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    Method and apparatus for optimizing gas-liquid interfacial contact
    141.
    发明授权
    Method and apparatus for optimizing gas-liquid interfacial contact 失效
    用于优化气 - 液界面接触的方法和装置

    公开(公告)号：US5529701A

    公开(公告)日：1996-06-25

    申请号：US492766

    申请日：1995-06-21

    Applicant: Thomas L. Grisham ,  Janet K. Peters ,  Keith W. Sharp ,  Edward E. Ebel

    Inventor： Thomas L. Grisham ,  Janet K. Peters ,  Keith W. Sharp ,  Edward E. Ebel

    IPC: B01J4/04 ,  B01J10/00 ,  B01J19/26 ,  B04C5/10 ,  B04C7/00 ,  B04C9/00 ,  B01D21/26

    CPC classification number: B04C9/00 ,  B01J19/26 ,  B01J4/04 ,  B04C5/10 ,  B04C7/00 ,  B01J2219/00051 ,  B01J2219/0011 ,  B01J2219/0013 ,  B01J2219/00162 ,  B01J2219/00164 ,  B01J2219/00166

    Abstract: Apparatus for optimizing gas-liquid interfacial contact for molecular mass transfer between gas and liquid comprises a gas-liquid contactor assembly including a hollow porous tube surrounded by an outer jacket defining a gas plenum between the jacket and the porous tube; a liquid feed assembly including a nozzle for injecting liquid into the porous tube in a spiraling flow pattern around and along the porous tube; a gas-liquid separator assembly at the first end of the porous tube including a nonporous degassing tube coaxially aligned with and connected to the porous tube, a gas outlet port coaxially aligned with the degassing tube to receive a first portion of gas flowing from the degassing tube, a first gas duct coaxially aligned with and connected to the gas outlet duct to convey the first portion of gas therefrom; a liquid collection assembly; and a second gas discharge assembly to collect and convey gas from the first end of the porous tube. A method of optimizing gas-liquid interfacial contact comprises the general steps of introducing a stream of liquid to the hollow interior of a cylindrical porous tube in a thin film following a spiral flow pattern around and along the wall of the tube; controlling the physical characteristics of the liquid film and the flow pattern followed by the film through the tube; sparging gas through the wall of the tube and into the liquid film at a preselected flow rate so as to create a two phase gas-liquid froth around the wall of the tube and a discrete column of gas in the central portion of the tube; maintaining the froth flow in a radial force field so as to prevent mixing of the froth and gas in the central column; removing gas forming the column from both ends of the tube; and removing liquid from the tube.

    Abstract translation: 用于优化用于气体和液体之间的分子质量传递的气 - 液界面接触的装置包括气 - 液接触器组件，其包括中空多孔管，所述中空多孔管被外护套围绕，所述外护套在所述护套和所述多孔管之间限定气室; 液体供给组件，包括用于沿着多孔管围绕和沿着多孔管以螺旋形流动图案将液体注入多孔管中的喷嘴; 在多孔管的第一端处的气液分离器组件包括与多孔管同轴对准并连接到其上的无孔脱气管，与脱气管同轴对准的气体出口，以接收从脱气流出的第一部分气体 管，与气体出口管道同轴对准并连接到气体出口管道的第一气体管道，以从其中输送气体的第一部分; 液体收集组件; 以及第二气体排出组件，用于从多孔管的第一端收集和输送气体。 优化气 - 液界面接触的方法包括以下步骤：在围绕并沿着管壁的螺旋流动模式之后将液体流引入到圆柱形多孔管的中空内部的薄膜中; 通过管子控制液膜的物理特性和随后的膜流动模式; 以预选的流量将气体喷射穿过管的壁并进入液膜，以在管的中心部分上形成围绕管的壁和分立的气体柱的两相气液泡沫; 将泡沫流维持在径向力场中，以防止中心塔中的泡沫和气体混合; 从管的两端去除形成塔的气体; 并从管中去除液体。

    Apparatus for uniform mixing of solutions
    143.
    发明授权
    Apparatus for uniform mixing of solutions 失效
    用于均匀混合溶液的装置

    公开(公告)号：US5424180A

    公开(公告)日：1995-06-13

    申请号：US996866

    申请日：1992-12-15

    Applicant: Mitsuo Saitou

    Inventor： Mitsuo Saitou

    IPC: B01F5/00 ,  B01F5/06 ,  B01J4/04 ,  G03C1/015

    CPC classification number: B01F5/0659 ,  B01F5/0602 ,  B01F5/0682 ,  B01J4/04 ,  G03C1/015 ,  B01F2005/0008

    Abstract: An apparatus for producing a highly uniform mixture of a first solution with two or more solute-containing solutions comprises a reaction vessel with a porous member located therein. The porous member, whic may be a membrane or a plurality of fine tubes, is located within the vessel below the surface of the first solution. One or more solute-containing solutions are rapidly and uniformly introduced into the first solution through the porous member. The solute containing solutions diffuse rapidly into the first solution through the openings in the porous member, mixing evenly to produce a uniform composition.

    Abstract translation: 用于生产具有两种或多种含溶质溶液的第一溶液的高度均匀混合物的装置包括具有位于其中的多孔构件的反应容器。 多孔构件可以是膜或多个细管，位于第一溶液表面下方的容器内。 通过多孔构件将一种或多种含溶质的溶液快速均匀地引入第一溶液中。 含有溶质的溶液通过多孔构件中的开口快速扩散到第一溶液中，混合均匀以产生均匀的组成。

    Oxidization of an oxidizable charge in the gaseous phase and a reactor for implementing this method
    146.
    发明授权
    Oxidization of an oxidizable charge in the gaseous phase and a reactor for implementing this method 失效
    气相中可氧化电荷的氧化和用于实施该方法的反应器

    公开(公告)号：US5037619A

    公开(公告)日：1991-08-06

    申请号：US507507

    申请日：1990-04-11

    Applicant: Jacques Alagy ,  Christian Busson

    Inventor： Jacques Alagy ,  Christian Busson

    IPC: B01J4/04 ,  B01J12/00 ,  B01J19/00 ,  B01J19/24 ,  C01B3/34 ,  C01B3/38

    CPC classification number: C01B3/34 ,  B01J12/005 ,  B01J19/2415 ,  B01J4/04 ,  B01J2219/00085 ,  B01J2219/00155 ,  B01J2219/00159 ,  B01J2219/0263

    Abstract: An oxidizable charge is oxidized in a gaseous phase reaction. The oxidizable charge and an oxidizing gas flow simultaneously and separately through a distribution zone made of a ceramic material. In at least a part of the distribution zone, the oxidizable charge and the oxidizing gas flow through a multiplicity of passages of a dimension so small that any flame resulting from oxidation of the oxidizable charge will be quenched. The oxidizable charge and oxidizing gas are then mixed in a mixing zone made from a ceramic material defining a multiplicity of spaces with passages having a dimension comparable to the dimension of the passages in the distribution zone. The mixture of gases then flows through a reaction zone made from a ceramic material defining another multiplicity of passages having dimensions comparable to those in the distribution zone. The distance between each of the distribution, mixing and reaction zones is also so small that any flame resulting from oxidation of the oxidizable charge will be quenched.

    Abstract translation: 可氧化的电荷在气相反应中被氧化。 可氧化的电荷和氧化性气体流动同时且分开地通过由陶瓷材料制成的分布区域。 在分配区域的至少一部分中，可氧化电荷和氧化气体流过多个尺寸小的通道，使得由可氧化电荷的氧化产生的任何火焰都将被淬灭。 然后将可氧化的电荷和氧化气体在由限定多个空间的陶瓷材料制成的混合区中混合，通道具有与分配区中的通道的尺寸相当的尺寸。 气体混合物然后流过由陶瓷材料制成的反应区，该反应区限定了与分配区相当的尺寸的多个通道。 分配，混合和反应区域之间的距离也很小，使得可氧化的电荷的氧化产生的任何火焰都将被淬火。

    Process involving oxidation reactor used oxidize a gaseous phase oxidizable feed
    147.
    发明授权
    Process involving oxidation reactor used oxidize a gaseous phase oxidizable feed 失效
    使用氧化反应器的方法氧化气相可氧化的进料

    公开(公告)号：US4971770A

    公开(公告)日：1990-11-20

    申请号：US264393

    申请日：1988-10-31

    Applicant: Jacques Alagy ,  Christian Busson

    Inventor： Jacques Alagy ,  Christian Busson

    IPC: C10J3/00 ,  B01J4/04 ,  B01J12/00 ,  B01J19/00 ,  B01J19/24 ,  C01B3/38 ,  C07C29/152 ,  B01J8/04

    CPC classification number: B01J19/2485 ,  B01J12/005 ,  B01J19/242 ,  B01J4/004 ,  B01J4/04 ,  C07C29/152 ,  B01J2219/00155 ,  B01J2219/00159 ,  B01J2219/00265 ,  B01J2219/0263

    Abstract: A new technique for oxidizing a gaseous phase oxidizable feed involves a process wherein a gas mixture containing at least one oxidizing gas is placed in contact with an oxidizable feed inside a mixing contact zone situated between at least one first zone passed through by the feed and at least one second zone passed through by the oxidation reaction products. The first and second zones define a multiplicity of multidirectional spaces exhibiting passages having, along at least one direction, a dimension at most equal to the jamming distance of the flame possibly resulting from oxidations of feed. The contact zone comprises an oxidizing gas mixture supply means comprising a plurality of parallel pipes with porous walls situated at a distance from the first and second zones which is at most equal to the jamming distance.

    Abstract translation: 用于氧化气相可氧化进料的新技术涉及一种方法，其中将含有至少一种氧化气体的气体混合物置于与位于至少由进料通过的至少一个第一区域之间的混合接触区域内， 至少一个第二区域被氧化反应产物穿过。 第一和第二区域限定多个多向空间，其显示通道，沿着至少一个方向具有最大等于可能由进料氧化引起的火焰的干扰距离的尺寸。 所述接触区包括氧化气体混合物供应装置，所述氧化气体混合物供应装置包括多个平行的管道，所述多个平行管道具有位于距离所述第一和第二区域一定距离的多孔壁，所述第一和第二

    Mobile atom insertion reaction, mobile atom transmissive membrane for carrying out the reaction, and reactor incorporating the mobile atom transmissive membrane
    148.
    发明授权
    Mobile atom insertion reaction, mobile atom transmissive membrane for carrying out the reaction, and reactor incorporating the mobile atom transmissive membrane 失效
    移动原子插入反应，用于进行反应的移动原子透射膜，以及并入移动原子透射膜的反应器

    公开(公告)号：US4908114A

    公开(公告)日：1990-03-13

    申请号：US117298

    申请日：1987-11-06

    Applicant: William Ayers

    Inventor： William Ayers

    IPC: B01J4/04 ,  B01J19/24 ,  C01B15/029 ,  C01B21/16 ,  C01C1/04 ,  C07C45/00 ,  C07C45/49 ,  C25B3/04 ,  C25B13/08

    CPC classification number: C25B3/04 ,  B01J19/2475 ,  B01J4/04 ,  C01B15/029 ,  C01B21/16 ,  C01C1/04 ,  C01C1/0405 ,  C07C45/00 ,  C07C45/49 ,  C25B13/08 ,  B01J2219/00177 ,  B01J2219/00186 ,  Y02P20/52

    Abstract: Disclosed is a method of carrying out a mobile atom insertion reaction, such as a hydrogen insertion reaction, for the synthesis of reduced, hydrogenated compounds. Such reactions include the production of ammonia and hydrazine from nitrogen, formic acid and methanol from carbon dioxide, and hydrogen peroxide from oxygen. The insertion reactions are carried out at a bipolar mobile atom transmissive membrane comprising a membrane formed of a mobile atom pump material, as a hydrogen pump material, conductive atom transmissive means on one surface of the membrane and conductive atom transmissive means on the opposite surface of the membrane. The mobile atom, such as hydrogen, diffuses across the membrane, to provide a source of hydrogen on the insertion reaction side of the membrane. The insertion reaction side of the membrane is positively biased with respect to a counterelectrode so that a reactant molecule, such as carbon dioxide, is electrosorbed on that surface of the membrane. The electrosorbed reactant molecular chemically reacts with the surface hydrogen by the insertion reaction to form a reduced, hydrogenated product such as formic acid. Also disclosed is a chemical reactor, containing the membrane, and several electrical field assisted chemical reactions utilizing the membrane and reactor.

    Abstract translation: 公开了用于合成还原的氢化化合物的进行诸如氢插入反应的可移动的原子插入反应的方法。 这样的反应包括从氮气中生成氨和肼，从二氧化碳生成甲酸和甲醇，以及从氧气生产过氧化氢。 插入反应在双极移动原子透射膜上进行，该双极移动原子透射膜包括由移动原子泵材料形成的膜，作为氢泵材料，在膜的一个表面上的导电原子透射装置和在膜的相对表面上的导电原子透射装置 膜。 诸如氢的移动原子扩散到膜上，以在膜的插入反应侧提供氢源。 膜的插入反应侧相对于反电极被正偏置，使得诸如二氧化碳的反应物分子在膜的表面上被电泳。 电泳反应物分子通过插入反应与表面氢化学反应形成还原的氢化产物如甲酸。 还公开了含有膜的化学反应器和利用膜和反应器的几个电场辅助化学反应。

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