PROCESS FOR PRODUCING A PARTIALLY BALANCED ACID SOLUTION
    11.
    发明申请
    PROCESS FOR PRODUCING A PARTIALLY BALANCED ACID SOLUTION 审中-公开
    生产部分平衡酸溶液的方法

    公开(公告)号:US20160060460A1

    公开(公告)日:2016-03-03

    申请号:US14786651

    申请日:2014-04-15

    Inventor: Robert J. WELCH

    Abstract: A process for producing a partially balanced acid solution that involves metering dicarboxylic acid powder, based on weight, from a loss-in-weight feeder to a feeding conduit that transfers the dicarboxylic acid powder at a low variability feed rate into an in-line disperser, adding a first feed stream of diamine to the in-line disperser in an amount sufficient to form the partially balanced acid solution having a solids content of less than 60%, and storing the partially balanced acid solution at a temperature to maintain the dissolved dicarboxylic acid and to prevent formation of a slurry. The partially balanced acid solution may be used as a feed solution to prepare a nylon salt solution. Process controls for the process are also disclosed.

    Abstract translation: 一种制备部分平衡的酸溶液的方法,其涉及将二羧酸粉末以重量计从重量损失进料器计量到以低变异性进料速率将二羧酸粉末转移到在线分散器中的进料管道 将二胺的第一进料流以足以形成固体含量小于60%的部分平衡的酸溶液的量向在线分散器中加入,并将部分平衡的酸溶液储存在保持溶解的二羧酸的温度 酸,并防止淤浆的形成。 部分平衡的酸溶液可以用作进料溶液以制备尼龙盐溶液。 还公开了该方法的过程控制。

    SEPARATING A SOLVENT FROM A NICKEL CATALYST BY DISTILLATION
    12.
    发明申请
    SEPARATING A SOLVENT FROM A NICKEL CATALYST BY DISTILLATION 审中-公开
    通过蒸馏从镍催化剂分离溶剂

    公开(公告)号:US20160168081A1

    公开(公告)日:2016-06-16

    申请号:US14904726

    申请日:2014-07-16

    Abstract: A solvent is at least partially separated from a catalyst. The catalyst comprises nickel and a bidentate phosphorus-containing ligand. The method for separation involves distilling a catalyst solution. The ratio of 2-pentenenitrile to 3-pentenenitrile in distillation column bottoms is controlled to reduce the amount of 3-pentenenitrile which is isomerized to form 2-methyl-3-butenenitrile. Isomerization of 3-pentenenitrile to 2-methyl-3-butenenitrile and subsequent isomerization of 2-methyl-3-butenenitrile to 2-methyl-2-butenenitrile, and/or hydrocyanation of 2-methyl-3-butenenitrile to methylglutaronitrile represents a loss in adiponitrile yield in a process for making adiponitrile.

    Abstract translation: 溶剂至少部分地与催化剂分离。 该催化剂包括镍和二齿含磷配体。 分离方法包括蒸馏催化剂溶液。 控制蒸馏柱底部中2-戊烯腈与3-戊烯腈的比例,以减少异构化形成2-甲基-3-丁烯腈的3-戊烯腈的量。 3-戊烯腈异构化为2-甲基-3-丁烯腈,随后将2-甲基-3-丁烯腈异构化为2-甲基-2-丁烯腈,和/或2-甲基-3-丁烯腈氢化为甲基戊二烯代表损失 在己二腈的制备方法中的己二腈产率。

    EFFLUENT OFF-GAS TREATMENT
    13.
    发明申请
    EFFLUENT OFF-GAS TREATMENT 审中-公开
    有效的关闭气体处理

    公开(公告)号:WO2016055542A1

    公开(公告)日:2016-04-14

    申请号:PCT/EP2015/073184

    申请日:2015-10-07

    Abstract: The present invention provides a process for the production of an aromatic dicarboxylic acid comprising the catalytic oxidation of a hydrocarbon precursor in an organic solvent, wherein off-gas generated by the oxidation reaction is vented to the atmosphere after treatment to remove HBr and/or Br 2 , wherein said process comprises scrubbing in a scrubbing column a gas stream derived from off-gas generated by said oxidation reaction and comprising HBr and/or Br 2 , characterised in that: (i) the gas stream is irrigated with liquid phase water and a wash stream comprising alkali metal ions within said scrubbing column; (ii) the scrubbed gas stream is withdrawn from a vent located in an upper region of the scrubbing column; and (iii)a stream comprising water, said alkali metal ions and bromide ions is withdrawn from an effluent outlet located in a lower region of the scrubbing column. The present invention further provides a scrubbing column for carrying out the process.

    Abstract translation: 本发明提供一种生产芳族二羧酸的方法,其包括在有机溶剂中催化氧化烃前体,其中通过氧化反应产生的废气在处理后排放到大气中以除去HBr和/或Br 2 其中所述方法包括在洗涤塔中洗涤源自由所述氧化反应产生的废气并包含HBr和/或Br 2的气流,其特征在于:(i)气流用液相水和洗涤液 在所述洗涤塔内包含碱金属离子; (ii)洗涤气流从位于洗涤塔上部区域的排气口排出; 和(iii)包含水的流,所述碱金属离子和溴离子从位于洗涤塔的下部区域的流出物出口排出。 本发明还提供一种用于进行该方法的洗涤塔。

    STRETCH CIRCULAR KNIT FABRICS WITH MULTIPLE ELASTIC YARNS
    14.
    发明申请
    STRETCH CIRCULAR KNIT FABRICS WITH MULTIPLE ELASTIC YARNS 审中-公开
    带多根弹性纱线的圆形针织面料

    公开(公告)号:WO2015057697A1

    公开(公告)日:2015-04-23

    申请号:PCT/US2014/060473

    申请日:2014-10-14

    CPC classification number: D04B1/18 D10B2403/0114 Y02P70/633

    Abstract: An article comprising a knit fabric having a surface side and a base side, and including a set of ground yarns and a layer of effect yarns, wherein the ground yarns and effect yarns are knit through intermesh points in a predetermined arrangement wherein the effect yarns are alternately arranged with the ground yarns and wherein the ground yarns comprise at least one elastic fiber and optionally at least one hard fiber, and the effect yarns comprise at least one hard fiber and optionally an elastic fiber.

    Abstract translation: 一种制品,包括具有表面侧和底侧的针织织物,并且包括一组研磨纱线和一层效果纱线,其中所述研磨纱线和效果纱线以预定布置编织穿过相互间的点,其中所述效果纱线是 交替地布置有研磨纱线,并且其中所述研磨纱线包括至少一种弹性纤维和任选的至少一种硬质纤维,并且所述效果纱线包括至少一种硬质纤维和任选的弹性纤维。

    SEPARATING A SOLVENT FROM A NICKEL CATALYST BY DISTILLATION
    16.
    发明申请
    SEPARATING A SOLVENT FROM A NICKEL CATALYST BY DISTILLATION 审中-公开
    通过蒸馏从镍催化剂分离溶剂

    公开(公告)号:WO2015009847A1

    公开(公告)日:2015-01-22

    申请号:PCT/US2014/046881

    申请日:2014-07-16

    Abstract: A solvent is at least partially separated from a catalyst. The catalyst comprises nickel and a bidentate phosphorus-containing ligand. The method for separation involves distilling a catalyst solution. The ratio of 2-pentenenitrile to 3-pentenenitrile in distillation column bottoms is controlled to reduce the amount of 3-pentenenitrile which is isomerized to form 2-methyl-3-butenenitrile. Isomerization of 3-pentenenitrile to 2- methyl-3-butenenitrile, and subsequent isomerization of 2-methyl-3-butenenitrile to 2- methyl-2-butenenitrile, and/or hydrocyanation of 2-methyl-3-butenenitrile to methylglutaronitrile represents a loss in adiponitrile yield in a process for making adiponitrile.

    Abstract translation: 溶剂与催化剂至少部分分离。 催化剂包括镍和二齿磷含量配体。 分离方法包括蒸馏催化剂溶液。 控制蒸馏塔底馏分中2-戊烯腈与3-戊烯腈的比例,以减少异构化形成2-甲基-3-丁烯腈的3-戊烯腈的量。 3-戊烯腈异构化为2-甲基-3-丁烯腈,随后将2-甲基-3-丁烯腈异构化为2-甲基-2-丁烯腈,和/或2-氰基-3-丁烯腈氢化为甲基戊二烯代表 在制造己二腈的方法中己二腈产率的损失。

    PROCESS FOR PRODUCING A PARTIALLY BALANCED ACID SOLUTION
    17.
    发明申请
    PROCESS FOR PRODUCING A PARTIALLY BALANCED ACID SOLUTION 审中-公开
    生产部分平衡酸溶液的方法

    公开(公告)号:WO2014179066A1

    公开(公告)日:2014-11-06

    申请号:PCT/US2014/034224

    申请日:2014-04-15

    Inventor: WELCH, Robert J.

    Abstract: A process for producing a partially balanced acid solution that involves metering dicarboxylic acid powder, based on weight, from a loss-in-weight feeder to a feeding conduit that transfers the dicarboxylic acid powder at a low variability feed rate into an in-line disperser, adding a first feed stream of diamine to the in-line disperser in an amount sufficient to form the partially balanced acid solution having a solids content of less than 60%, and storing the partially balanced acid solution at a temperature to maintain the dissolved dicarboxylic acid and to prevent formation of a slurry. The partially balanced acid solution may be used as a feed solution to prepare a nylon salt solution. Process controls for the process are also disclosed.

    Abstract translation: 一种制备部分平衡的酸溶液的方法,其涉及将二羧酸粉末以重量计从重量损失进料器计量到以低变异性进料速率将二羧酸粉末转移到在线分散器中的进料管道 将二胺的第一进料流以足以形成固体含量小于60%的部分平衡的酸溶液的量向在线分散器中加入,并将该部分平衡的酸溶液储存在一定温度以保持溶解的二羧酸 酸,并防止淤浆的形成。 部分平衡的酸溶液可以用作进料溶液以制备尼龙盐溶液。 还公开了该方法的过程控制。

    INTEGRATED PROCESS FOR DIAMINE PRODUCTION
    18.
    发明申请
    INTEGRATED PROCESS FOR DIAMINE PRODUCTION 审中-公开
    DIAMINE生产的综合工艺

    公开(公告)号:WO2014099610A1

    公开(公告)日:2014-06-26

    申请号:PCT/US2013/074668

    申请日:2013-12-12

    Abstract: Described is a process for the integrated production of hexamethylenediamine. The process includes integrating an HCN production process, a dinitrile compound production process, and a diamine production process. The HCN production process provides HCN for hydrocyanating butadiene to form a dinitrile compound and a hydrogen stream for hydrogenating the dinitrile compound to form a diamine. The HCN production process includes forming a crude hydrogen cyanide product and separating the crude hydrogen cyanide product to form an off-gas stream and a hydrogen cyanide product stream. The off-gas stream is further separated to recover hydrogen. The hydrogen cyanide product stream is further processed to recover hydrogen cyanide.

    Abstract translation: 描述了一体化生产六亚甲基二胺的方法。 该方法包括将HCN生产过程,二腈化合物生产过程和二胺生产过程相结合。 HCN生产方法提供用于氢化氰化丁二烯的HCN以形成二腈化合物和用于氢化二腈化合物形成二胺的氢气流。 HCN生产方法包括形成粗制氰化氢产物并分离粗制氰化氢产物以形成废气流和氰化氢产物流。 进一步分离废气流以回收氢气。 进一步处理氰化氢产物流以回收氰化氢。

    STRETCH WOVENS WITH A CONTROL YARN SYSTEM
    19.
    发明申请
    STRETCH WOVENS WITH A CONTROL YARN SYSTEM 审中-公开
    具有控制纱线系统的拉链车身

    公开(公告)号:WO2013148659A1

    公开(公告)日:2013-10-03

    申请号:PCT/US2013/033848

    申请日:2013-03-26

    Abstract: An article including a woven fabric comprising warp yarns and weft yarns, wherein at least one of either the warp yarns or the weft yarns includes: (a) a corespun elastic base yarn having a denier and including staple fiber and an elastic fiber core; and (b) a separate control yarn selected from the group consisting of a single filament yarn, a multiple filament yarn, a composite yarn, and combinations thereof; having a denier greater than zero to about 0.8 times the denier of the corespun elastic base yam; wherein the woven fabric includes (1 ) a ratio of corespun base yarn ends to control yarn ends of up to about 6:1; or (2) a ratio of corespun base yarn picks to control yarn picks of up to about 6:1; or (3) both a ratio of corespun base yarn ends to control yarn ends of up to about 6:1; and a ratio of corespun base yarn picks to control yarn picks of up to about 6:1.

    Abstract translation: 一种包括经纱和纬纱的织物的制品,其中经纱或纬纱中的至少一种包括:(a)具有旦尼尔并包括短纤维和弹性纤维芯的芯绒弹性基纱; 和(b)选自单丝纱,多丝纱,复合纱及其组合的单独对照丝; 具有大于零至约0.8倍核心弹性基础纱线的丹尼尔的旦尼尔; 其特征在于,所述机织织物包括:(1)芯纱基纱线端部的比例,以控制纱线末端高达约6:1; 或(2)芯绒纱线选择的比例控制高达约6:1的纱线挑选; 或者(3)两芯纱线的纱线端部之间的比例控制纱线端部高达约6:1; 以及芯绒纱线的纱线比例控制在6:1左右。

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