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公开(公告)号：KR1020140071158A
公开(公告)日：2014-06-11
申请号：KR1020120139184
申请日：2012-12-03
Applicant: 한국전기연구원
Abstract: The present invention relates to a manufacturing method of an organic-inorganic hybrid adhesive material using nanoparticle-dispersed monomer. The manufacturing method of an organic-inorganic hybrid adhesive material using nanoparticle-dispersed monomer comprises: a first step of providing a reactive functional group by modifying the surface of nanoparticles with organic silane; a second step of forming nanoparticle-dispersed monomer by dispersing the nanoparticles surface-modified at the first step in functional monomer having a reactive functional group reacting with the reactive functional group of the nanoparticles; a third step of forming mixed monomer by adding and mixing soft monomer and hard monomer in the nanoparticle-dispersed monomer manufactured at the second step; a fourth step of manufacturing an adhesive syrup by adding an initiator to the mixed monomer, mixing, and irradiating light; and a fifth step of forming an organic-inorganic hybrid adhesive material by mixing functional micro particles to the adhesive syrup formed at the fourth step. As such, the present invention has an advantage of improving physical properties of materials by firstly forming monomer dispersed with nanoparticles, adding the monomer dispersed with nanoparticles in the synthesis process of an organic-inorganic hybrid material, and maintaining the homogeneous and stable dispersion.
Abstract translation: 本发明涉及使用纳米粒子分散单体的有机 - 无机杂化粘合剂材料的制造方法。 使用纳米粒子分散单体的有机 - 无机混合粘合剂材料的制造方法包括：通过用有机硅烷改性纳米粒子的表面来提供反应性官能团的第一步骤; 通过将在第一步骤表面改性的纳米颗粒分散在具有与纳米颗粒的反应性官能团反应的反应性官能团的官能单体中形成纳米颗粒分散单体的第二步骤; 通过在第二步骤制造的纳米颗粒分散单体中加入和混合软单体和硬单体形成混合单体的第三步骤; 通过在混合单体中加入引发剂，混合和照射光来制造粘合剂浆料的第四步骤; 以及通过将功能性微粒子与第四步骤形成的粘合剂浆料混合形成有机 - 无机混合粘合剂材料的第五步骤。 因此，本发明通过首先形成分散有纳米颗粒的单体，在有机 - 无机混合材料的合成过程中加入分散有纳米颗粒的单体，并保持均匀和稳定的分散体，具有改善材料的物理性能的优点。
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