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公开(公告)号：KR1020130059214A
公开(公告)日：2013-06-05
申请号：KR1020110125415
申请日：2011-11-28
Applicant: 오덱(주)
CPC classification number: H01M4/921 , Y02E60/50 , Y02E60/521
Abstract: PURPOSE: A manufacturing method of a catalyst for fuel cells is provided to replace a platinum catalyst with palladium with low costs, thereby reducing manufacturing costs of catalysts while maintaining performance of the platinum catalyst. CONSTITUTION: A manufacturing method of a catalyst for fuel cells comprises a step of manufacturing a platinum-palladium synthesis precursor; a step of manufacturing the catalyst for fuel cells. The first step comprises a step of reacting palladium and acetic acid to prepare palladium-acetate; a step of reacting gold and amine-based organic materials, to manufacture platinum-amide; and a step of mixing the palladium-acetate and platinum-amide. [Reference numerals] (AA) Start; (BB) Carbon pre-treatment step; (CC) Precursor dispersion step; (DD) Stabilization step; (EE) Filtration and washing step; (FF) Drying step; (GG) End
Abstract translation: 目的：提供一种用于燃料电池的催化剂的制造方法，以低成本代替铂催化剂，从而降低催化剂的制造成本，同时保持铂催化剂的性能。 构成：燃料电池用催化剂的制造方法包括制造铂 - 钯合成前体的工序; 制造燃料电池用催化剂的工序。 第一步包括使钯和乙酸反应制备乙酸钯的步骤; 使金和胺基有机材料反应的步骤，制造铂 - 酰胺; 以及将乙酸钯和铂 - 酰胺混合的步骤。 （附图标记）（AA）开始; （BB）碳预处理步骤; （CC）前体分散步骤; （DD）稳定步骤; （EE）过滤和洗涤步骤; （FF）干燥步骤; （GG）结束
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公开(公告)号：KR101241421B1
公开(公告)日：2013-03-11
申请号：KR1020100127654
申请日：2010-12-14
Applicant: 오덱(주)
Abstract: 본 발명은 비대칭 구조를 갖는 팔라듐계 가솔린 자동차용 촉매 및 그 제조방법에 관한 것으로, 더욱 상세하게는 담체, 전술한 담체의 외표면에 형성되는 제1코팅층 및 전술한 제1코팅층의 외표면에 형성되는 제2코팅층으로 이루어지며, 담체의 외표면에 제1코팅액을 도포하는 제1코팅단계, 전술한 제1코팅액 도포된 담체의 외표면에 제2코팅액을 도포하는 제2코팅단계 및 전술한 제2코팅액이 도포된 담체를 80 내지 120℃의 온도로 가열하여 수분을 제거하는 건조단계 및 전술한 건조단계를 거친 담체를 500 내지 600℃의 온도로 가열하여 소성하는 소성단계를 통해 제조된다.
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公开(公告)号：KR1020120085609A
公开(公告)日：2012-08-01
申请号：KR1020110007050
申请日：2011-01-24
Applicant: 오덱(주)
CPC classification number: B01J23/44 , B01J35/023
Abstract: PURPOSE: A palladium catalyst with the optimized particle sizes of noble metals is provided to improve the initial purifying efficiency of the catalyst after deterioration by optimizing interaction between aluminum oxide and noble metals. CONSTITUTION: A palladium catalyst includes a carrier(10), a first coating layer(20), and a second coating layer(30). The first coating layer is formed at the outer surface of the carrier. The first coating layer includes barium oxide and palladium. The second coating layer is formed at the outer surface of the first coating layer. The second coating layer includes barium oxide and palladium. The thickness of the first coating layer is between 100 and 110 g/L. The thickness of the second coating layer is between 130 and 140 g/L.
Abstract translation: 目的：提供具有优化的贵金属粒度的钯催化剂，以通过优化氧化铝和贵金属之间的相互作用来改善催化剂劣化后的初始净化效率。 构成：钯催化剂包括载体（10），第一涂层（20）和第二涂层（30）。 第一涂层形成在载体的外表面。 第一涂层包括氧化钡和钯。 第二涂层形成在第一涂层的外表面。 第二涂层包括氧化钡和钯。 第一涂层的厚度为100-110g / L。 第二涂层的厚度在130-140g / L之间。
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公开(公告)号：KR1020120066358A
公开(公告)日：2012-06-22
申请号：KR1020100127654
申请日：2010-12-14
Applicant: 오덱(주)
CPC classification number: B01J23/63 , B01D53/94 , B01J37/0027
Abstract: PURPOSE: The palladium-based catalyst of an asymmetric structure for gasoline vehicles and a method for manufacturing the same are provided to improve the efficiency of purification by asymmetrically forming two coating layers with different coating component contents on the surface of a carrier. CONSTITUTION: The palladium-based catalyst of an asymmetric structure for gasoline vehicles includes a carrier, a first coating layer formed on the outer surface of the carrier, and a second coating layer formed on the outer surface of the first coating layer(S101, S103). The first coating layer includes 70-71 parts by weight of aluminum, 4-4.5 parts by weight of strontium oxide, 24-25 parts by weight of cerium oxide, and 0.5-1 parts by weight of palladium. The second coating layer includes 54-55 parts by weight of aluminum, 10-11 parts by weight of strontium oxide, 32-33 parts by weight of cerium oxide, and 2-2.5 parts by weight of palladium. A drying process and a plasticizing process are implemented(S105, S107).
Abstract translation: 目的：提供用于汽油车辆的不对称结构的钯基催化剂及其制造方法，以通过在载体表面上不对称地形成具有不同涂层成分含量的两个涂层来提高净化效率。 构成：用于汽油车辆的不对称结构的钯基催化剂包括载体，形成在载体的外表面上的第一涂层和形成在第一涂层的外表面上的第二涂层（S101，S103 ）。 第一涂层包括70-71重量份的铝，4-4.5重量份的氧化锶，24-25重量份的氧化铈和0.5-1重量份的钯。 第二涂层包括54-55重量份的铝，10-11重量份的氧化锶，32-33重量份的氧化铈和2-2.5重量份的钯。 实施干燥处理和塑化处理（S105，S107）。
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Patent Agency Ranking
公开(公告)号：KR1020120135786A
公开(公告)日：2012-12-17
申请号：KR1020110054694
申请日：2011-06-07
Applicant: 오덱(주)
CPC classification number: H01M4/92 , H01M4/926 , H01M2008/1095 , Y02E60/521
Abstract: PURPOSE: A manufacturing method of electrode catalyst is provided to have excellent diffusion efficiency by applying the duster and ultrasonic device at the same time, and an excellent production efficiency by using the centrifuge step and washing process, thereby enabling the mass production. CONSTITUTION: A manufacturing method of electrode catalyst comprises the steps of: pre-processing a mixture of ethylene glycol and a support element(S101), injecting platinum precursor to the pre-processed mixture and performing mixing(S103), putting acid solution into the mixture for stabilization(S105), centrifugally separating the stabilized mixture to extract electrode catalyst(S107), washing the electrode catalyst(S109), and heating the washed electrode catalyst(S111). [Reference numerals] (AA) Start; (BB) End; (S101) Pretreatment step; (S103) Platinum precursor injection step; (S105) Stabilization step; (S107) Centrifugal step; (S109) Cleaning step; (S111) Heat treatment step
Abstract translation: 目的：提供电极催化剂的制造方法，通过同时施用除尘器和超声波装置具有优异的扩散效率，并且通过使用离心机步骤和洗涤工艺具有优异的生产效率，从而能够批量生产。 构成：电极催化剂的制造方法包括以下步骤：预处理乙二醇和载体元素的混合物（S101），将铂前体注入预处理混合物并进行混合（S103），将酸溶液加入到 用于稳定化的混合物（S105），离心分离稳定的混合物以提取电极催化剂（S107），洗涤电极催化剂（S109），并加热洗涤的电极催化剂（S111）。 （附图标记）（AA）开始; （BB）结束; （S101）预处理步骤; （S103）铂前体注入步骤; （S105）稳定化步骤; （S107）离心步骤 （S109）清洁步骤; （S111）热处理工序
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公开(公告)号：KR1020120134857A
公开(公告)日：2012-12-12
申请号：KR1020110054054
申请日：2011-06-03
Applicant: 오덱(주)
CPC classification number: H01M4/92 , H01M4/926 , Y02E60/50 , Y02E60/521
Abstract: PURPOSE: A manufacturing method of a highly dispersed platinum-supported catalyst is provided to provide a highly dispersed platinum-supported catalyst with excellent durability and activity by using materials such as carbon nanotubes, carbon fiber, carbon black which are not easily degradable even under oxidation atmosphere of a reduction electrode. CONSTITUTION: A manufacturing method of a highly dispersed platinum-supported catalyst comprises: a mixture preparation step(S101) mixing a platinum mixture, sodium hydroxide and an mine mixture; a pre-treatment step(S103) treating a carrier with ethylene glycol; a platinum dispersion step(S105) dispersing the mixture in the mixture preparation step into the carrier of the pre-treatment step; a stabilization step(S107) putting acid solution into the carrier passed through the platinum dispersion step; a filtering and washing step(S109) filtering and cleaning the stabilized carrier; a heat treatment step(S111) heating the cleaned carrier; and a pulverization step(S113) pulverizing the heat-treated carrier. [Reference numerals] (AA) Start; (BB) End; (S101) Mixture preparation step; (S103) Pre-treatment step; (S105) Platinum dispersion step; (S107) Stabilization step; (S109) Filtering and cleaning step; (S111) Heat treatment step; (S113) Pulverization step
Abstract translation: 目的：提供高度分散的铂负载催化剂的制造方法，通过使用碳纳米管，碳纤维，甚至在氧化时不易降解的碳黑等材料，提供高度分散的铂负载催化剂，具有优异的耐久性和活性 还原电极的气氛。 构成：高分散铂负载催化剂的制造方法包括：混合制备步骤（S101）将铂混合物，氢氧化钠和矿物混合物混合; 预处理步骤（S103）用乙二醇处理载体; 将混合物制备步骤中的混合物分散到预处理步骤的载体中的铂分散步骤（S105） 稳定化步骤（S107）将酸溶液放入通过铂分散步骤的载体中; 过滤和洗涤步骤（S109）过滤和清洁稳定的载体; 热处理步骤（S111）加热清洁的载体; 和粉碎工序（S113），对经热处理的载体进行粉碎。 （附图标记）（AA）开始; （BB）结束; （S101）混合物制备步骤; （S103）预处理步骤; （S105）铂分散步骤; （S107）稳定步骤; （S109）过滤清洗工序; （S111）热处理工序; （S113）粉碎步骤
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公开(公告)号：KR101186342B1
公开(公告)日：2012-09-26
申请号：KR1020110012948
申请日：2011-02-14
Applicant: 오덱(주)
Abstract: 본 발명은 백금 및 팔라듐을 이용한 디젤자동차용 촉매의 제조방법에 관한 것으로, 더욱 상세하게는 팔라듐이 고착된 지지체 분말을 제조하는 팔라듐고착분말제조단계, 전술한 팔라듐 분말이 고착된 지지체 분말, 증류수 및 백금용액을 혼합하여 백금팔라듐 예비혼합물을 제조하는 예비혼합물제조단계, 전술한 예비혼합물 및 백금용액으로 이루어진 혼합물에 질산을 첨가하는 질산첨가단계, 전술한 질산첨가단계를 거친 혼합물에 촉매지지체를 함침하고 교반하는 함침교반단계 및 함침교반단계를 거친 촉매혼합물을 소성하는 소성단계를 포함하여 이루어진다.
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公开(公告)号：KR100932295B1
公开(公告)日：2009-12-16
申请号：KR1020060069928
申请日：2006-07-25
Applicant: 오덱(주)
Abstract: A method for preparing an oxidizing catalyst for a diesel vehicle is provided to improve the performance in purification of CO and HC, by mixing vanadium and platinum into binders separately. An oxidizing catalyst is prepared by mixing V2O5 into a first binder, hardening the mixture of V2O5 and the first binder, mixing other binders and a platinum solution into the hardened mixture to regulate a pH value, pulverizing the resultant mixture, and coating and hardening the pulverized matters on a supporter. The first binder is titan dioxide, and the second binder is titan dioxide and alumina. Further, the pH is adjust to 4-5, and the hardening is performed at 500°C for 4 hrs.
Abstract translation: 提供一种用于制备用于柴油车辆的氧化催化剂的方法，以通过将钒和铂分别混合到粘合剂中来提高CO和HC的净化性能。 通过将V 2 O 5混合到第一粘合剂中，硬化V 2 O 5和第一粘合剂的混合物，将其它粘合剂和铂溶液混入硬化混合物中以调节pH值，粉碎所得混合物，并涂覆并硬化 粉碎的物质在支架上。 第一种粘合剂是二氧化钛，第二种粘合剂是二氧化钛和氧化铝。 此外，将pH调节至4-5，并且在500℃下进行硬化4小时。
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