16.
    发明专利
    未知

    公开(公告)号:DE4111827A1

    公开(公告)日:1992-10-15

    申请号:DE4111827

    申请日:1991-04-11

    Applicant: BASF AG

    Abstract: The preparation of 1-amino-2-phenoxy-4-hydroxyanthraquinone by reacting 1-amino-2-halo-4-hydroxyanthraquinone with phenol in aqueous suspension at a pH of from 9 to 13 and at a temperature of from 130 to 160 DEG C is carried out by adjusting the pH of a reaction mixture to between 9.5 and 11.5 when the reaction is complete, separating the reaction product from the liquid phase, and purifying 1-amino-2-phenoxy-4-hydroxyanthraquinone, which has been obtained by reacting 1-amino-2-halo-4-hydroxyanthraquinone with phenol, by washing the crude product with alkaline hypochlorite solution.

    17.
    发明专利
    未知

    公开(公告)号:DE4110458A1

    公开(公告)日:1992-10-01

    申请号:DE4110458

    申请日:1991-03-30

    Applicant: BASF AG

    Abstract: The invention concerns a method for the preparation of halogenated indigo by reacting indigo with bromine and/or chlorine, optionally using iodine as a catalyst, characterized in that thionyl chloride is used as the reaction medium.

    20.
    发明专利
    未知

    公开(公告)号:ES2107483T3

    公开(公告)日:1997-12-01

    申请号:ES92111596

    申请日:1992-07-08

    Applicant: BASF AG

    Abstract: A process for purifying indigo comprises stripping the as-synthesized aqueous alkaline indoxylate solution before its oxidation to indigo of impurities in the absence of oxygen by distillation or by passing in steam or an inert gas and then treating the indigo precipitated on oxidation of the stripped indoxylate solution with dilute hydrogen peroxide solution.

Patent Agency Ranking