公开(公告)号：DE2156602A1

公开(公告)日：1973-05-24

申请号：DE2156602

申请日：1971-11-15

Applicant: BASF AG

Inventor： EILINGSFELD HEINZ DR ,  SCHWANTJE GERD DR ,  KRALLMANN REINHOLD

IPC: C09B5/16 ,  D06P1/16 ,  D06P1/52 ,  D06P1/62 ,  D06P1/651 ,  D06P3/79 ,  D06P5/00

Abstract: The dyestuffs usd are of formula (I): (where one X is OH and the other is 1-4C alkylamino in which one H atom may be substd. by 1-3C alkoxy, cyano, carbonamide, alkoxycarbonyl with a total of 2-5C atoms, phenyl or pyrrolidon-2-yl-1, or phenylamino in which 1 or 2 H atoms may be substd. by Cl, Br, OH, CH3, NO2, alkoxycarbonyl with a total of 2-5C atoms, alkyl and/or alkoxy with 1 or 2 C atoms, or in which one H atom may be substd. by the gps -CONR1R2 or - SO2NR1R2, or aliphatic acylamino with 2-8C atoms in the acyl gp. in which one or two H atoms may be substd. by Cl, Br, or 1-2C alkoxy, or cycloaliphatic acyl amino with 7-8C atoms in the acyl gp. or benzoylamino in which one or two H atoms may be substd. by Cl, Br, alkoxy and/or alkyl with 1 or 2 C atoms; R1 is H opt. branched 1-8C alkyl, 6-8C cycloalkyl, 2-4C hydroxyalkyl or alkoxyalkyl with a total of 3-5C atoms; R2 is H 1-8C alkyl, 2-4C hydroxyalkyl or 3-5C alkoxyalkyl. Cpds. (I) where one X is opt. substd. phenyl and the other X is OH are esp., suitable.

公开(公告)号：DE2041565A1

公开(公告)日：1972-02-24

申请号：DE2041565

申请日：1970-08-21

Applicant: BASF AG

Inventor： SCHWANTJE GERD DR

IPC: C09B1/514

Abstract: Polyesters, esp. polyethylene glycol terephthalate textiles, are dyed to fast blue shades with dyes of formula: (where one X is OH and the other is -NO2), esp. used in equimolar ratio.

公开(公告)号：DE3374932D1

公开(公告)日：1988-01-28

申请号：DE3374932

申请日：1983-02-16

Applicant: BASF AG

Inventor： MUELLER JOSEF DR ,  WIERSDORFF WALTER-WIELANT DR ,  KIRSCHENLOHR WERNER DR ,  SCHWANTJE GERD DR

IPC: C07C231/00 ,  C07C67/00 ,  C07C231/02 ,  C07C231/12 ,  C07C233/02 ,  C07C233/13 ,  C07C103/375

Abstract: 1. A process for the preparation of an o-acylaminomethylbenzyl halide of the formula (I) see diagramm : EP0087676,P5,F3 where X is halogen and R**1 is an aliphatic or aromatic radical, wherein an o-aminomethylbenzyl alkyl ether of the formula (II) see diagramm : EP0087676,P5,F4 where R**2 is alkyl, is reacted with an acylating agent to give the corresponding acylaminomethylbenzyl alkyl ether, and the latter is reacted with an aqueous hydrohalic acid to give the halide (I).

公开(公告)号：CH602588A5

公开(公告)日：1978-07-31

申请号：CH1568173

申请日：1973-11-08

Applicant: BASF AG

Inventor： ELSER WOLFGANG DR ,  SCHWANTJE GERD DR

IPC: C07C227/12 ,  C07C229/74 ,  C07D265/12 ,  C09B1/22 ,  C07C101/80

Abstract: The production of 1-amino-4-nitroanthraquinone-2-carboxylic esters by reaction of 1,2-dihydro-6-nitro-7,8-diphthaloyl-3,1,4H-benzoxazone-4 with an alcohol in the presence of an acid catalyst. Pure carboxylic esters are immediately obtained in a high yield previous isolation of the carboxylic acid.

公开(公告)号：CH601194A5

公开(公告)日：1978-06-30

申请号：CH1568273

申请日：1973-11-08

Applicant: BASF AG

Inventor： SCHUHMACHER ALFRED DR ,  SCHWANTJE GERD DR

IPC: C07C67/00 ,  C07C231/00 ,  C07C231/02 ,  C07C235/84 ,  C07C237/30 ,  C07C237/48 ,  C07D265/12 ,  C09B1/22 ,  C09B1/28 ,  C07C103/76 ,  C07C103/28 ,  C09B1/20

Abstract: Production of amides of 1-aminoanthraquinone-2-carboxylic acid which bear hydrogen, cyclohexylamino, chloro, bromo or nitro as substituent in the 4-position by reaction of 1,2-dihydro-7,8-diphthaloyl-3,1,4H-benzoxazone-4:

公开(公告)号：DE2254813A1

公开(公告)日：1974-05-22

申请号：DE2254813

申请日：1972-11-09

Applicant: BASF AG

Inventor： ELSER WOLFGANG DR ,  SCHWANTJE GERD DR

IPC: C07C227/12 ,  C07C229/74 ,  C07D265/12 ,  C09B1/22 ,  C07D87/16

Abstract: The production of 1-amino-4-nitroanthraquinone-2-carboxylic esters by reaction of 1,2-dihydro-6-nitro-7,8-diphthaloyl-3,1,4H-benzoxazone-4 with an alcohol in the presence of an acid catalyst. Pure carboxylic esters are immediately obtained in a high yield previous isolation of the carboxylic acid.

公开(公告)号：DE2247347A1

公开(公告)日：1974-03-28

申请号：DE2247347

申请日：1972-09-27

Applicant: BASF AG

Inventor： SCHWANTJE GERD DR ,  SCHUHMACHER ALFRED DR

IPC: C07C227/12 ,  C07C20060101 ,  C07C229/74 ,  C09B1/22 ,  C07C101/78

Abstract: An improvement in the process for the production of 1-amino-4-nitroanthraquinone-2-carboxylic acid from 1-aminoanthraquinone-2-carboxylic acid by reaction with formaldehyde in concentrated sulfuric acid and nitration of the reaction product into 1,2-dihydro-6-nitro-7,8-diphthaloyl-3,1,4H-benzoxazone-4 followed by hydrolysis of the same. The improvement consists in precipitating the benzoxazone derivative by adding a precipitant, hydrolyzing the isolated benzoxazone derivative in aqueous solution and precipitating the 1-amino-4-nitro-anthraquinone-2-carboxylic acid from the alkaline solution by acidification. 1-amino-4-nitroanthraquinone-2-carboxylic acid is obtained in a purity of 95 percent by weight or more.

公开(公告)号：DE2227401A1

公开(公告)日：1973-12-20

申请号：DE2227401

申请日：1972-06-06

Applicant: BASF AG

Inventor： SCHWANTJE GERD DR

IPC: C07D209/48 ,  C09B1/51 ,  C09B1/514 ,  C09B1/50

Abstract: A disperse dye of the formula (I):