DESUBLIMER FOR THE RECOVERY OF SUBLIMED PRODUCTS FROM REACTION GASES

    公开(公告)号:DE3160439D1

    公开(公告)日:1983-07-21

    申请号:DE3160439

    申请日:1981-07-09

    Applicant: BASF AG

    Abstract: Desublimator for isolating sublimation products from reaction gases, which consists of a closed housing and a plurality of rows of finned tubes accommodated horizontally and superposedly therein, successive superposed finned tubes being supported, and mutually spaced, with limited adjustability, by means of cage-like perforated sliding shoes surrounding them in a box-like manner, the sliding shoes of the individual finned tubes being directly stacked one above the other and resting loosely on common supporting girders anchored to the housing, and the supporting girders having, in cross-section, the outline of a triangle with its apex pointing downward.

    14.
    发明专利
    未知

    公开(公告)号:DE1618136A1

    公开(公告)日:1971-03-11

    申请号:DEB0092089

    申请日:1967-04-15

    Applicant: BASF AG

    Abstract: 1,180,117. Distillation columns; purification of phthalic anhydride. BADISCHE ANILIN-& SODA-FABRIK A.G. 19 May, 1967 [21 May, 1966; 15 April, 1967], No. 23398/67. Heading BIB. [Also in Division. C2] Phthalic anhydride is purified by distillation in a plant comprising two fractionating columns 1, 5 of the tray-type connected as shown to two evaporators 2, 8 each containing a vertically-disposed bundle of tubes, the arrangement being such that the distilland flows down as a thin film on the inside of the tubes. The material to be purified is introduced about half-way up column 1, which is maintained under reduced pressure. Vapours comprising about 37% of the feed, including all the low-boiling impurities, leave the head of column 1, and are condensed; and part of the condensate is refluxed to the column. Highboiling impurities are withdrawn from the system through line 9. Purified phthalic anhydride is obtained at the head of column 5.

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