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    OLEFIN POLYMERIZATION CATALYST SYSTEMS AND METHODS OF USE THEREOF
    12.
    发明申请
    OLEFIN POLYMERIZATION CATALYST SYSTEMS AND METHODS OF USE THEREOF 审中-公开
    烯烃聚合催化剂体系及其使用方法

    公开(公告)号：WO2017173079A1

    公开(公告)日：2017-10-05

    申请号：PCT/US2017/025021

    申请日：2017-03-30

    Applicant: DOW GLOBAL TECHNOLOGIES LLC

    Inventor： BAILEY, Brad C. ,  CHRISTIANSON, Matthew D. ,  SREEKUMAR, Sanil

    IPC: C08F210/16 ,  C08F4/642 ,  C08F2/38

    Abstract: An olefin polymerization catalyst system includes a procatalyst component chosen from metal-ligand complexes of Formula (I): In Formula (I), each X is independently a monodentate or polydentate ligand that is neutral, monoanionic, or dianionic; the metal-ligand complex of Formula (I) is overall neutral; each Y 1 -Y 4 and Y 7 -Y 10 independently is selected from C or N such that six membered diaza (N 2 ) or triaza (N 3 ) rings are formed; wherein each R 1 and R 10 independently are chosen from (C 1 -C 40 ) hydrocarbyl, substituted (C 1 -C 40 ) hydrocarbyl, (C 1 -C 40 ) heterohydrocarbyl, and substituted (C 1 -C 40 ) heterohydrocarbyl or is absent; each R 2 , R 3 , R 4 , R 7 , R 8 , and R 9 is chosen from hydrogen; (C 1 -C 40 ) hydrocarbyl; substituted (C 1 -C 40 ) hydrocarbyl; (C 1 -C 40 ) heterohydrocarbyl; substituted (C 1 -C 40 ) heterohydrocarbyl; halogen, nitro (NO 2 ) or is absent; each R 5 and R 6 independently is chosen from (C 1 -C 40 ) hydrocarbyl, substituted (C 1 -C 40 ) hydrocarbyl, (C 1 -C 40 ) heterohydrocarbyl, and substituted (C 1 -C 40 ) heterohydrocarbyl.

    Abstract translation: 烯烃聚合催化剂体系包括选自式（I）的金属 - 配体络合物的前催化剂组分：在式（I）中，每个X独立地为单齿或多齿配体，其为中性，单阴离子， 或双阴离子; 式（I）的金属 - 配体络合物是总体中性的; 每个Y 1 -Y 4和Y 7 -Y 10独立地选自C或N，使得六个 （N = 2）或三氮杂（N = 3）环形成; 其中每个R 1和R 10独立地选自（C 1 -C 40）烃基，取代的（C 1 -C 40） C 1 -C 40）烃基，（C 1 -C 40）杂烃基和取代的（C 1 -C 40） 低级亚甲基）杂烃基或不存在; 每个R 2，R 3，R 4，R 7，R 8，R 8，R 8，R 8， ，并且R 9选自氢; （C≡C-40）烃基; 取代的（C 1 -C 40）烃基; （C≡C-40）杂烃基; 取代的（C 1 -C 40）杂烃基; 卤素，硝基（NO 2）或不存在; 每个R 5和R 6独立地选自（C 1 -C 40）烃基，取代的（C （C 1 -C 40）杂烃基和取代的（C

    CATALYST SYSTEM FOR MULTI-BLOCK COPOLYMER FORMATION
    15.
    发明申请
    CATALYST SYSTEM FOR MULTI-BLOCK COPOLYMER FORMATION 审中-公开

    公开(公告)号：WO2018170138A1

    公开(公告)日：2018-09-20

    申请号：PCT/US2018/022454

    申请日：2018-03-14

    Applicant: DOW GLOBAL TECHNOLOGIES LLC

    Inventor： YOUNG, Andrew J. ,  DO, Hien Q. ,  BAILEY, Brad C. ,  CHRISTIANSON, Matthew D. ,  MUNRO, Jeffrey C. ,  CARNAHAN, Edmund M.

    IPC: C08F210/16 ,  C08F4/64

    Abstract: The present disclosure relates to a catalyst system for use in forming a multi-block copolymer, said copolymer containing therein two or more segments or blocks differing in chemical or physical properties, a polymerization process using the same, and the resulting polymers, wherein the composition comprises the admixture or reaction product resulting from combining: (A) a first olefin polymerization procatalyst, (B) a second olefin polymerization procatalyst capable of preparing polymers differing in chemical or physical properties from the polymer prepared by procatalyst (A) under equivalent polymerization conditions, (C) an activator, and (D) a chain shuttling agent.

    NON-CYCLOPENTADIENYL-BASED CHROMIUM CATALYSTS FOR OLEFIN POLYMERIZATION
    16.
    发明申请
    NON-CYCLOPENTADIENYL-BASED CHROMIUM CATALYSTS FOR OLEFIN POLYMERIZATION 审中-公开
    用于烯烃聚合的非环丙烯二酸的铬催化剂

    公开(公告)号：WO2012155022A1

    公开(公告)日：2012-11-15

    申请号：PCT/US2012/037462

    申请日：2012-05-11

    Applicant: DOW GLOBAL TECHNOLOGIES LLC ,  CHRISTIANSON, Matthew D. ,  DE VRIES, Timothy S. ,  FROESE, Robert D. ,  OBER, Matthias S. ,  PATTON, Jasson T. ,  ROMER, Duane R. ,  ROOF, Gordon R. ,  SUN, Lixin ,  SZUROMI, Endre ,  THERIAULT, Curt N. ,  WELSH, Dean M. ,  WENZEL, Timothy T. ,  MORAN, Paul H.

    Inventor： CHRISTIANSON, Matthew D. ,  DE VRIES, Timothy S. ,  FROESE, Robert D. ,  OBER, Matthias S. ,  PATTON, Jasson T. ,  ROMER, Duane R. ,  ROOF, Gordon R. ,  SUN, Lixin ,  SZUROMI, Endre ,  THERIAULT, Curt N. ,  WELSH, Dean M. ,  WENZEL, Timothy T. ,  MORAN, Paul H.

    IPC: C07F11/00 ,  C08F4/69 ,  C08F4/60

    CPC classification number: C08F4/78 ,  C07F11/00 ,  C08F10/00 ,  C08F110/02 ,  C08F110/06 ,  C08F210/06 ,  C08F4/69112 ,  C08F210/16 ,  C08F2500/15

    Abstract: Provided is a non-cyclopentadienyl-based chromium-ligand complex, preferably a chromium-ligand complex of formula (J): LCr(R A ) m (D) k (J), wherein L is a non-Cp monoanionic ligand; Cr (chromium) is in a formal oxidation state of +3 or +2; when Cr formally is Cr +3 , either m is 1 and R A is hydrocarbylene (a hydrocarbylene chromium-ligand complex of formula (J)) or m is 2 and each R A independently is hydrocarbyl (a dihydrocarbyl chromium-ligand complex of formula (J)), wherein each hydrocarbyl or hydrocarbylene of R A independently is unsubstituted or substituted by from 1 to 5 R AS ; each R AS independently is a neutral aprotic heteroalkyl, neutral aprotic heterocycloalkyl, neutral aprotic heteroaryl, or neutral aprotic aryl; when Cr formally is Cr +2 , m is 1 and R A is hydrocarbyl (a hydrocarbyl chromium-ligand complex of formula (J)); k is an integer of 0 or 1; D is absent when k is 0 or D is a neutral ligand when k is 1; wherein the chromium-ligand complex of formula (J) is overall neutral and lacks a cyclopentadienyl-based (Cp-based) moiety. Also provided is a chromium catalyst comprising or prepared from the complex. Also provided is a process of making the catalyst and a process employing the chromium catalyst for polymerizing the olefin monomer, especially a straight chain 1-alkene, to prepare the polyolefin, especially a partially chain-straightened poly( 1-alkene) or olefin block copolymer. Further provided is the partially chain- straightened poly( 1-alkene) or olefin block copolymer prepared thereby. Also provided is a high throughput workflow.

    Abstract translation: 提供非环戊二烯基铬配体络合物，优选式（J）的铬 - 配体络合物：LCr（RA）m（D）k（J），其中L是非-C 1单阴离子配体; Cr（铬）处于+3或+2的正式氧化态; 当Cr正式为Cr + 3时，m为1，RA为亚烃基（式（J））的亚烃基铬 - 配体配合物）或m为2，各RA独立地为烃基（式（J）的二烃基铬 - 配体络合物 ）），其中RA的各个烃基或亚烃基独立地未被取代或被1至5个RAS取代; 每个RAS独立地是中性非质子杂烷基，中性非质子杂环烷基，中性非质子杂芳基或中性非质子性芳基; 当Cr正式为Cr + 2时，m为1，RA为烃基（式（J））的烃基铬 - 配体络合物）; k是0或1的整数; 当k为0时，D不存在，或当k为1时D为中性配体; 其中式（J）的铬配体络合物是总体中性的，并且缺少基于环戊二烯基的（Cp-基）部分。 还提供了包含或由络合物制备的铬催化剂。 还提供了制备催化剂的方法和使用铬催化剂聚合烯烃单体，特别是直链1-烯烃的方法，以制备聚烯烃，特别是部分链改性的聚（1-烯烃）或烯烃嵌段 共聚物。 进一步提供由其制备的部分链直链化的聚（1-烯烃）或烯烃嵌段共聚物。 还提供了高吞吐量的工作流程。

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