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    POLYMER, PROCESS AND COMPOSITION
    13.
    发明公开
    POLYMER, PROCESS AND COMPOSITION 审中-公开
    聚合物，工艺和组成

    公开(公告)号：EP2809693A1

    公开(公告)日：2014-12-10

    申请号：EP13702638.1

    申请日：2013-02-04

    Applicant: DSM IP Assets B.V.

    Inventor： NABUURS, Tijs ,  OVERBEEK, Gerardus, Cornelis ,  STUBBS, Jeffrey ,  GEBHARD, Matthew, Stewart

    IPC: C08F222/14 ,  C08F222/04 ,  C09D135/02 ,  C08L35/02

    Abstract: There is described a method of preparing a post-modified polymer the method comprising the steps of: (1) polymerising a monomer composition comprising from 2.5 to 75% by weight of the total monomer composition of at least one itaconic anhydride, precursor thereof and/or derivative thereof in a polymerisation method to obtain an itaconate Polymer A; (2) reacting in a post modification step at least 10 mole-% of the anhydride groups, anhydride precursor groups and/or anhydride derived groups of the Polymer A obtained from step (1) with a Nucleophile B to form a post-modified Polymer C, and optionally using said polymer C as seed or stabiliser in a further step (3) to form a sequential Polymer D.

    Abstract translation: 描述了包含重均分子量为1000至150,000g / mol（通过GPC测量）的低聚物组合物O的低聚物 - 聚合物组合物[任选地基本上不含苯乙烯（<1.5wt-％共聚物））和聚合物组合物 所述低聚物组合物O和所述聚合物组合物P各自独立地包含共聚物组合物，所述共聚物组合物包含：（a）至少8.5重量％，优选≥8重量％的至少80,000g / mol的重均分子量（通过GPC测量） 20重量％的较高的衣康酸二酯（优选衣康酸二丁酯-DBI）; （b）小于23重量％的酸单体，但也足以具有小于150mg KOH / g聚合物的酸值，（c）任选地具有小于50重量％的其他衣康酸单体，和（d）任选 （a）至（c）中少于77重量％的其他单体。 DBI可能是生物可再生的。 一个实施方案是两相的乙烯基序列聚合物的水分散体：A）40至90重量％的Tg为-50至30℃的乙烯基聚合物A; 和B）10至60重量％的Tg为50至130℃的乙烯基聚合物B; 其中DBI用于制备A和/或B，并且聚合物A具有0.1至10重量％的至少一种酸官能烯属不饱和单体。 另一个实施方案是Mw为1,000至150,000g / mol且酸值> 5mgKOH / g的乙烯基低聚物C的含水聚合物涂料组合物; 和乙烯基聚合物D，Mw> = 80,000g / mol，酸值<10mgKOH / g，其中D由DBI获得，用于形成C和D的单体的量分别落入聚合物重量比5-70 对于聚合物D为95至30。另一实施方案为由烯属不饱和单体和自由基引发剂制备乙烯基聚合物珠粒的水性悬浮聚合方法，其中至少10重量％的单体为DBI。

    AQUEOUS EMULSION
    16.
    发明公开
    AQUEOUS EMULSION 有权
    水性乳液

    公开(公告)号：EP2513176A1

    公开(公告)日：2012-10-24

    申请号：EP10800919.2

    申请日：2010-12-17

    Applicant: DSM IP Assets B.V.

    Inventor： NABUURS, Tijs ,  OVERBEEK, Gerardus Cornelis ,  STUBBS, Jeffrey

    IPC: C08F265/04 ,  C08F267/06 ,  C08L35/02

    CPC classification number: C09D135/02 ,  C08F212/08 ,  C08F220/18 ,  C08F222/14 ,  C08F265/04 ,  C08F267/06 ,  C08F2220/1808 ,  C08F2220/1825 ,  C08F2220/1833 ,  C08L35/02 ,  Y10T428/31935 ,  C08L2666/04 ,  C08L2666/02

    Abstract: The invention relates to an aqueous emulsion comprising at least a vinyl polymer, said vinyl polymer comprising: a) 45 to 99 wt % of itaconate ester monomers having formula (I), wherein R and R′ are independently an alkyl or an aryl group; b) 0.1 to 15 wt % of ionic or potentially ionic unsaturated monomers; c) 0 to 54 wt % of unsaturated monomers, different from a) and b); and 0.9 to 54.9 wt % by weight of total monomers of a chaser monomer composition added subsequently and polymerized after the polymerization of monomers a), b) and c); wherein a)+b)+c) and the chaser monomer composition add up to 100%; and wherein the aqueous emulsion contains less than 0.5 wt % free itaconate ester monomers of formula I based on the total weight of the aqueous emulsion.

    Abstract translation: 本发明涉及包含至少一种乙烯基聚合物的水性乳液，所述乙烯基聚合物包含：a）45-99wt％的具有式（I）的衣康酸酯单体，其中R和R'独立地为烷基或芳基; b）0.1至15重量％的离子型或潜在离子型不饱和单体; c）0至54重量％的不同于a）和b）的不饱和单体; 和随后加入的并且在单体a），b）和c）的聚合之后聚合的追加单体组合物的总单体的0.9至54.9重量％。 其中a）+ b）+ c）和追加单体组成加起来为100％; 并且其中所述水性乳液含有基于所述水性乳液的总重量的小于0.5重量％的式I的游离衣康酸酯单体。

    USE OF A POLYMER COMPOSITION
    18.
    发明公开
    USE OF A POLYMER COMPOSITION 审中-公开
    使用的聚合物组合物

    公开(公告)号：EP2809720A1

    公开(公告)日：2014-12-10

    申请号：EP13702235.6

    申请日：2013-02-04

    Applicant: DSM IP Assets B.V.

    Inventor： NABUURS, Tijs ,  OVERBEEK, Gerardus Cornelis ,  STUBBS, Jeffrey ,  GEBHARD, Matthew Stewart

    IPC: C08L35/02 ,  C08F222/14 ,  A61K8/81 ,  C09D135/02

    CPC classification number: C08F222/12 ,  A61K8/8152 ,  A61K8/8158 ,  A61K2800/10 ,  A61Q19/00 ,  C08F220/10 ,  C08F222/14 ,  C08F2220/1825 ,  C08L33/12 ,  C08L35/02 ,  C08F220/14 ,  C08F220/06

    Abstract: There is described use of a biorenewable copolymers in one or more of: in a topical and/or personal care composition, as a binder for toner, as an encapsulating agent for a colorant, as a hybrid colorant, as additive for sheet moulding compounds, as a plastic pigment, as a filler for composite materials such as concrete, as a filler for coatings and/or waxes; and/or as a spacer in a display; where the biorenewable copolymer comprises (a) at least 8. 5 wt-% preferably >=20 wt-% of a higher itaconate diester (preferably dibutyl itaconate -DBI); (b) less than 23 wt-% acid monomer but also sufficient to have an acid value less than 150 mg KOH/g of polymer, (c) optionally with less than 50 wt-% of other itaconate monomers, and (d) optionally less than 77 wt-%of other monomers not (a) to (c). The DBI may be biorenewable. One embodiment is an aqueous dispersion of vinyl sequential polymer of two phases: A) 40 to 90 wt-% of a vinyl polymer A with Tg from -50 to 30°C; and B) 10 to 60 wt-% of a vinyl polymer B with Tg from 50 to 130°C; where DBI is used to prepare A and/or B and polymer A has from 0.1 to 10 wt-% of at least one acid-functional olefinically unsaturated monomer.

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