公开(公告)号：WO2010062162A2

公开(公告)日：2010-06-03

申请号：PCT/MY2009000200

申请日：2009-11-25

Applicant: MIMOS BERHAD ,  AHMAD MOHD RAIS

Inventor： AHMAD MOHD RAIS

IPC: C25D3/64 ,  C25C1/20 ,  C25D17/12 ,  C25D21/18 ,  G01N27/30

CPC classification number: C25B1/00 ,  C25D11/34 ,  G01N27/301 ,  Y02P20/542

Abstract: The present invention relates to a method for chlorination of silver materials in the forms of wire, thick film paste and metallic sheet/disc. The method is environmentally friendly since the process does not produce hazardous chemicals or flammable gas. The electrochemical setup includes position the electrode containing silver materials in the anode and a platinum wire at the cathode. A DC voltage supply between 1 to 5 volts oxidizes the silver surface which receives chloride from imidazolium chloride solution to produce silver chloride on silver wire, film or disc. The imidazolium chloride reagent can be in aqueous solution or polar organic solvents or naturally exists in ionic liquid form. The imidazolium radical cation decomposes to produce a stabilized organic radical and an imidazole molecule. The stabilized radical recombines to produce volatile organic compound that can be recovered by simple distillation. The chlorination reagent can be regenerated by re-introducing the stabilized group at N1.

Abstract translation: 本发明涉及一种以线材，厚膜糊料和金属片/盘的形式氯化银材料的方法。 该方法是环保的，因为该方法不产生有害化学物质或易燃气体。 电化学装置包括在阳极中含有银材料的电极和阴极处的铂丝线的位置。 1至5伏之间的直流电压电压使从氯化咪唑鎓溶液中接收氯化物的银表面氧化，以在银线，薄膜或圆盘上产生氯化银。 咪唑氯化物试剂可以在水溶液或极性有机溶剂中或天然以离子液体形式存在。 咪唑鎓阳离子分解产生稳定的有机基团和咪唑分子。 稳定化的基团重新组合以产生可通过简单蒸馏回收的挥发性有机化合物。 氯化试剂可以通过在N1上重新引入稳定化的基团来再生。

公开(公告)号：WO2010005280A3

公开(公告)日：2010-05-20

申请号：PCT/MY2009000095

申请日：2009-07-06

Applicant: MIMOS BERHAD ,  AHMAD MOHD RAIS ,  RASHID NORA ZAH ABDUL

Inventor： AHMAD MOHD RAIS ,  RASHID NORA ZAH ABDUL

IPC: C07F7/14 ,  C07F7/12 ,  G01N27/414

CPC classification number: C07F7/1892 ,  C07F7/1852 ,  G01N27/3335 ,  G01N27/414

Abstract: Lipophilic bromobenzene compounds substituted at the para position with long-chain hydrocarbon or fluorinated. carbon and terminal hydroxy group can be prepared from 4-bromophenylmagnesium bromide and other reagents. When converted to its Grignard derivative, the 4-hydroxyalkyI bromobenzene are reactive towards boron trihalides or boranes to give borates having sterically shielded negative charge with loosely bound metal cation suitable for creating anionic sites in chemical sensor membrane.

Abstract translation: 在对位被长链烃或氟化取代的亲油性溴苯化合物。 碳和末端羟基可以由4-溴苯基溴化镁等试剂制备。 当转化为其格氏衍生物时，4-羟基烷基溴苯对三卤化硼或硼烷硼反应，得到具有空间屏蔽负电荷的硼酸盐，其松散结合的金属阳离子适于在化学传感器膜中产生阴离子位点。

公开(公告)号：WO2009082187A2

公开(公告)日：2009-07-02

申请号：PCT/MY2008000191

申请日：2008-12-19

Applicant: MIMOS BERHAD ,  AHMAD MOHD RAIS ,  ABD AZIZ AIMAN SAJIDAH

Inventor： AHMAD MOHD RAIS ,  ABD AZIZ AIMAN SAJIDAH

IPC: G01N27/30 ,  G01N27/26

CPC classification number: G01N27/301

Abstract: The present invention relates to the method of manufacturing of maintenance-free silver-silver chloride reference electrode wherein the immobilized gel internal electrolyte (5) is made of fluorinated quaternary ammonium chloride salts immobilized to the acrylic hydrogel polymer backbone. Migration and loss of chloride ion is prevented and thus results in negligible variation of chloride ion concentration, and prolonged life of the reference electrode.

Abstract translation: 本发明涉及无维护银氯化银参比电极的制造方法，其中固定化的凝胶内部电解质（5）由固定在丙烯酸类水凝胶聚合物主链上的氟化季铵盐形成。 防止氯离子的迁移和损失，从而导致氯离子浓度的变化可以忽略不计，延长了参比电极的寿命。

公开(公告)号：WO2009157755A2

公开(公告)日：2009-12-30

申请号：PCT/MY2009000085

申请日：2009-06-26

Applicant: MIMOS BERHAD ,  AHMAD MOHD RAIS ,  RAHMAN AIRUL AZHA ABDUL ,  RASHID NORAZAH ABDUL ,  SAMAN RAHIMAH MOHD ,  ZAINI KHAIRIL MAZWAN MOHD ,  AZIZ AIMAN SAJIDAH ABD

Inventor： AHMAD MOHD RAIS ,  RAHMAN AIRUL AZHA ABDUL ,  RASHID NORAZAH ABDUL ,  SAMAN RAHIMAH MOHD ,  ZAINI KHAIRIL MAZWAN MOHD ,  AZIZ AIMAN SAJIDAH ABD

IPC: G01N27/333 ,  G01N33/24

CPC classification number: G01N27/333 ,  G01N33/24 ,  G01N2033/245

Abstract: An apparatus for detecting and analysing soil macronutrients using ion- selective electrode comprises a porous metal casing (1), micro porous polymeric layer (2), conductive hydrogel (3), sensor module (4), electronics connection system (5) and PCB with a readout circuit (6).

Abstract translation: 用于使用离子选择性电极检测和分析土壤营养素的装置包括多孔金属壳体（1），微孔聚合物层（2），导电水凝胶（3），传感器模块（4），电子连接系统（5）和PCB 具有读出电路（6）。

公开(公告)号：WO2009088281A3

公开(公告)日：2009-10-15

申请号：PCT/MY2009000011

申请日：2009-01-07

Applicant: MIMOS BERHAD ,  AHMAD MOHD RAIS

Inventor： AHMAD MOHD RAIS

IPC: C07C13/00

CPC classification number: G01N27/3335 ,  C07D319/06 ,  C07D323/00

Abstract: Novel lipophilic metal cation ionophore comprising two cyclic polyether substituents having the following molecular formula is disclosed. wherein n = 0, 1, 2 which along with 2n number of methylene (CH2) units, of each of the cyclic polyether substituent is varied to derive an ionophore having specif?c affinity to any one of lithium (Li+), sodium (Na+) and potassium (K+) cations. Apart from intermediate compounds, a process is also disclosed for synthesizing the ionophore from pentaerythritol by first converting it to a protected diol with 2 tosylate leaving groups, converting it to a lipophilic protected diol with Grignard reaction before deprotecting the diol. A diol silyl ether is synthesized into cyclic polyether with a tosylate leaving group which is then reacted with the deprotected diol to give the desired lipophilic metal cation ionophore.

Abstract translation: 公开了包含具有以下分子式的两个环状聚醚取代基的新型亲脂性金属阳离子离子载体。 其中n = 0,1,2与每个环状聚醚取代基的2n个亚甲基（CH 2）单元一起改变以得到对锂（Li +），钠（Na +）， ）和钾（K +）阳离子。 除了中间体化合物之外，还公开了一种从季戊四醇合成离子载体的方法，首先将其转化为带有2个甲苯磺酸酯离去基团的受保护的二醇，在将二醇脱保护之前将其转化成具有格利雅反应的亲脂保护的二醇。 二醇甲硅烷基醚与甲苯磺酸酯离去基团合成环状聚醚，然后与脱保护的二醇反应，得到所需的亲脂性金属阳离子离子载体。

公开(公告)号：WO2009057989A3

公开(公告)日：2009-10-15

申请号：PCT/MY2008000123

申请日：2008-10-22

Applicant: MIMOS BERHAD ,  WAN JAMIL WAN ADIL ,  AHMAD MOHD RAIS ,  ABDUL RAHMAN AIRUL AZHA ,  RAZALI NABIHAH

Inventor： WAN JAMIL WAN ADIL ,  AHMAD MOHD RAIS ,  ABDUL RAHMAN AIRUL AZHA ,  RAZALI NABIHAH

IPC: H02J17/00 ,  H02M7/04

CPC classification number: H02J50/00 ,  H02J17/00

Abstract: This invention relates to a device for harvesting energy from ubiquitous radio waves and more particularly an adaptive rectifier device (8) designed as power harvesting circuit which is to harvest electrical energy by tapping the commercially available radio waves. The device (10) comprises of an antenna (1), a high frequency transformer (2), an automatic tuning circuit (3), a capacitors bank (4), a rectifier (5), a threshold limit circuit (6) and an adaptive circuit (7). The threshold limit circuit (6) is configured having a predetermined output voltage and when an output voltage is below than the predetermined voltage, the automatic tuning circuit (3) starts searching for new source of radio frequency (RF) energy by changing its capacitance by feeding a distinctive voltage into the automatic tuning circuit (3) via the adaptive circuit (7). The searching for RF energies stops when the output voltage level resumes to the predetermined voltage.

Abstract translation: 本发明涉及一种用于从普遍存在的无线电波收集能量的装置，更具体地说，涉及一种被设计为功率收集电路的自适应整流装置（8），该电力收集电路通过点击市售无线电波来收获电能。 设备（10）包括天线（1），高频变压器（2），自动调谐电路（3），电容器组（4），整流器（5），阈值限制电路（6）和 自适应电路（7）。 阈值限制电路（6）被配置为具有预定的输出电压，并且当输出电压低于预定电压时，自动调谐电路（3）通过改变其电容开始寻找新的射频（RF）能量源 通过自适应电路（7）向自动调谐电路（3）馈送独特的电压。 当输出电压电平恢复到预定电压时，RF能量的搜索停止。

公开(公告)号：WO2010024661A3

公开(公告)日：2010-06-24

申请号：PCT/MY2009000126

申请日：2009-08-21

Applicant: MIMOS BERHAD ,  AHMAD MOHD RAIS ,  SAMAN RAHIMAH MOHD

Inventor： AHMAD MOHD RAIS ,  SAMAN RAHIMAH MOHD

IPC: C07F5/02 ,  G01N27/327

CPC classification number: C07F5/027 ,  G01N27/3335

Abstract: The present invention relates to preparation of immobilized lipophilic ammonium borate salts, wherein the salt can form covalent bond with the monomer of sensing membrane and thus immobilized to the matrix backbone. The sterically shielded ammonium and borate ions create equal number of lipophilic cationic and anionic sites that are loosely bound and when in contact with silver-silver electrode can function as planar reference electrode.

Abstract translation: 本发明涉及固定的亲脂性硼酸铵盐的制备，其中盐可以与感测膜的单体形成共价键并因此固定在基质主链上。 空间屏蔽的铵和硼酸根离子产生相等数量的松散结合的亲脂阳离子和阴离子位点，并且当与银 - 银电极接触时可以起到平面参考电极的作用。

公开(公告)号：WO2009075561A3

公开(公告)日：2009-12-10

申请号：PCT/MY2008000186

申请日：2008-12-12

Applicant: MIMOS BERHAD ,  AHMAD MOHD RAIS ,  ABD AZIZ AIMAN SAJIDAH

Inventor： AHMAD MOHD RAIS ,  ABD AZIZ AIMAN SAJIDAH

IPC: C07C231/08 ,  C07C233/89

CPC classification number: C07C231/12 ,  C07C213/08 ,  C07C219/08 ,  C07C233/89

Abstract: The present invention relates to the syntheses fluorinated quaternary ammonium salts with active fluorinated acrylamide or acrylate group for polymerization. The fluorinated quaternary ammonium salts can be used as a component for the preparation of immobilized internal electrolyte in maintenance-free reference electrode, lipophilic agents in anion chemical sensor membranes and ionic dopants for conductive hydrogels.

Abstract translation: 本发明涉及用于聚合的具有活性氟化丙烯酰胺或丙烯酸酯基团的合成氟化季铵盐。 氟化季铵盐可用作制备免维护参比电极中的固定化内电解质，阴离子化学传感器膜中的亲脂剂和导电水凝胶的离子掺杂剂的组分。

公开(公告)号：WO2009066987A3

公开(公告)日：2009-10-15

申请号：PCT/MY2008000153

申请日：2008-11-24

Applicant: MIMOS BERHAD ,  AHMAD MOHD RAIS ,  MOHD SAMAN RAHIMAH ,  MOHD ZAINI KHAIRIL MAZWAN

Inventor： AHMAD MOHD RAIS ,  MOHD SAMAN RAHIMAH ,  MOHD ZAINI KHAIRIL MAZWAN

IPC: G01N33/24 ,  G01N30/04

CPC classification number: G01N33/24 ,  G01N1/02 ,  G01N1/38 ,  G01N35/085 ,  G01N2001/383 ,  G01N2033/245

Abstract: The present invention relates to the use of an apparatus for filtering, extracting and analyzing soil nutrient. The apparatus comprises spray head (1), sampling filter (2), inert tubing (3), flow injection analysis (FIA) system (4), extractant supply (5), rinse supply (6), waste output (7), micro sampling platform (8), sensor cell (9) and/or analyzer (10).

Abstract translation: 本发明涉及用于过滤，提取和分析土壤养分的设备的用途。 该设备包括喷头1，采样过滤器2，惰性管3，流动注射分析系统4，萃取剂供应5，漂洗供应6，废物输出7， 微量采样平台（8），传感器单元（9）和/或分析器（10）。

公开(公告)号：WO2009075560A2

公开(公告)日：2009-06-18

申请号：PCT/MY2008000185

申请日：2008-12-12

Applicant: MIMOS BERHAD ,  AHMAD MOHD RAIS ,  ABD AZIZ AIMAN SAJIDAH

Inventor： AHMAD MOHD RAIS ,  ABD AZIZ AIMAN SAJIDAH

IPC: C07C231/02

CPC classification number: C07C231/02 ,  C07C213/06 ,  C07C219/08 ,  C07C233/09

Abstract: The present invention relates to the syntheses of fluorinated acrylamides and amino acrylates. The fluorinated acrylamide IV, fluorinated acrylamide V and fluorinated amino acrylate VI can be used as precursor molecules for the preparation of fluorinated quaternary ammonium salts. The fluorinated quaternary ammonium salts can be used as immobilized internal electrolyte in maintenance-free reference electrode, immobilized lipophilic agents in anion chemical sensor membranes and ionic dopants for moisture- retaining conductive hydrogels.

Abstract translation: 本发明涉及氟化丙烯酰胺和氨基丙烯酸酯的合成。 氟化丙烯酰胺IV，氟化丙烯酰胺V和氟化氨基丙烯酸酯VI可用作制备氟化季铵盐的前体分子。 氟化季铵盐可用作免维护参比电极中的固定内部电解质，阴离子化学传感器膜中的固定亲脂性试剂和用于保湿导电水凝胶的离子掺杂剂。