Method of Sulfonation of Block Polymers
    201.
    发明申请
    Method of Sulfonation of Block Polymers 有权
    块状聚合物的磺化方法

    公开(公告)号:US20100048817A1

    公开(公告)日:2010-02-25

    申请号:US12498778

    申请日:2009-07-07

    Abstract: Improved methods for preparing sulfonated block polymers with acyl sulfates in non-halogenated aliphatic solvents are provided. The methods include the sulfonation of a precursor block polymer with an acyl sulfate in a reaction mixture further comprising at least one non-halogenated aliphatic solvent to form a sulfonated block polymer, wherein the initial concentration of the precursor block polymer is in the range of from about 0.1 wt % to a concentration that is below the limiting concentration of the precursor block polymer based on the total weight of the reaction mixture. A sulfonation degree of greater than about 1.0 milliequivalent sulfonic acid per gram sulfonated block polymer can be achieved substantially free of polymer precipitation and free of disabling gelation.

    Abstract translation: 提供了在非卤代脂族溶剂中制备具有酰基硫酸盐的磺化嵌段聚合物的改进方法。 所述方法包括在还含有至少一种非卤代脂族溶剂的反应混合物中使用酰基硫酸酯磺化前体嵌段聚合物以形成磺化嵌段聚合物,其中前体嵌段聚合物的初始浓度范围为 约0.1重量%至低于前体嵌段聚合物的极限浓度的浓度,基于反应混合物的总重量。 可以实现大于约1.0毫当量磺酸/克磺化嵌段聚合物的磺化度,基本上不含聚合物沉淀并且没有失效的凝胶化。

    LIGNIN COMPOSITION
    206.
    发明公开
    LIGNIN COMPOSITION 审中-公开

    公开(公告)号:US20230304222A1

    公开(公告)日:2023-09-28

    申请号:US18326593

    申请日:2023-05-31

    Abstract: The present invention relates to a process for producing a lignin composition, which process comprises:



    providing a lignin slurry comprising water and a water miscible organic solvent;
    subjecting the lignin slurry to extraction at an extraction temperature of less than 100° C. for an extraction time of at least 1 minute to provide an extracted slurry;
    removing liquid from the extracted slurry to provide an extracted lignin; and
    suspending the extracted lignin in a polar organic solvent to provide a lignin composition having a dry matter content of at least 30% by weight.




    The present invention also relates to a lignin composition comprising hardwood Kraft lignin and a polar organic solvent, which composition has a dry matter content of at least 30% by weight. The present invention also relates to use of the lignin composition as a fuel.

Patent Agency Ranking