公开(公告)号：US09370677B2

公开(公告)日：2016-06-21

申请号：US14760567

申请日：2014-01-20

Applicant: Commissariat a l'energie atomique et aux energies alternatives

Inventor： Jean Christophe Ruiz ,  Hubert-Alexandre Turc ,  Frederic Charton

IPC: A62D3/38 ,  B09B3/00 ,  B01J19/18 ,  B01J3/00 ,  B01J3/02 ,  A62D101/20

CPC classification number: A62D3/38 ,  A62D2101/20 ,  B01J3/008 ,  B01J3/02 ,  B01J19/1812 ,  B01J19/1843 ,  B01J2208/00761 ,  B01J2219/00083 ,  B01J2219/00087 ,  B01J2219/0009 ,  B01J2219/00135 ,  B01J2219/00761 ,  Y02P20/544

Abstract: A hydrothermal oxidation device for treatment of a material in a supercritical medium includes a main body, an internal tube installed inside the main body to form an annular zone along the main body, a stirring mechanism installed in an internal zone of the internal tube and actuated by a rotating shaft, a cooling mechanism to cool the treated material located in the internal zone of the internal tube, an inlet for water and oxidant mix, an effluents outlet, an inlet for material to be treated, located at one end of the main body, this inlet opening up into the internal tube. The oxidation device includes an inlet for a diluted effluent, located in the flange and connected to a preheating coil arranged along an internal wall of the main body and extending from its first end to its second end, the preheating coil opening up into the internal tube.

Abstract translation: 用于处理超临界介质中的材料的水热氧化装置包括主体，安装在主体内部的内管，以沿着主体形成环形区域;搅拌机构，安装在内管的内部区域中并致动 通过旋转轴，用于冷却位于内管内部区域中的处理过的材料的冷却机构，用于水和氧化剂混合物的入口，排出物出口，待处理材料的入口，位于主体的一端 身体，这个入口打开进入内管。 氧化装置包括用于稀释流出物的入口，其位于凸缘中并且连接到沿着主体的内壁布置并且从其第一端延伸到其第二端的预热线圈，预热线圈开口进入内管 。

公开(公告)号：US09192901B2

公开(公告)日：2015-11-24

申请号：US13699774

申请日：2011-05-17

Applicant: Jawwad Darr ,  Christopher James Tighe ,  Robert Gruar

Inventor： Jawwad Darr ,  Christopher James Tighe ,  Robert Gruar

IPC: B01J19/00 ,  B01J8/00 ,  B01D11/04 ,  B01F5/04 ,  B01F13/00 ,  B01J3/00 ,  B01J3/02 ,  B01F5/00 ,  B82Y99/00

CPC classification number: B01J8/005 ,  B01D11/0411 ,  B01F5/045 ,  B01F13/0059 ,  B01F2005/0034 ,  B01J3/008 ,  B01J3/02 ,  B01J19/0093 ,  B01J2219/00889 ,  B82Y99/00 ,  Y02P20/544

Abstract: A high pressure tubular reactor for production of nanoparticles by precipitation has unidirectional fluid flows of precursor and supercritical water directed from inner and outer coaxial inlets to an outlet via a reaction zone immediately downstream of the inlets. The inner inlet is for supercritical fluid, and the outer inlet is for a precursor.

Abstract translation: 用于通过沉淀生产纳米颗粒的高压管式反应器具有从内部和外部同轴入口经由入口紧邻下游的反应区引导到出口的前体和超临界水的单向流体流。 内部入口用于超临界流体，外部入口用于前体。

公开(公告)号：US09056294B2

公开(公告)日：2015-06-16

申请号：US13043486

申请日：2011-03-09

Applicant: Jens Fink ,  Niels Nielsen Poulsen

Inventor： Jens Fink ,  Niels Nielsen Poulsen

IPC: B65G53/48 ,  B01J8/00 ,  B65G53/00 ,  B65G53/34 ,  B65G53/40 ,  B65G51/00 ,  B65G51/04 ,  B65G51/08 ,  B65G51/10 ,  B65G51/14 ,  B01J8/08 ,  B01J8/18 ,  B01J19/00

CPC classification number: B01J8/002 ,  B01J3/02 ,  B01J8/0015 ,  B01J8/0035 ,  B01J2208/00743 ,  B01J2208/00752 ,  B01J2208/00761 ,  B01J2208/00769 ,  B65G53/48 ,  C12P2201/00 ,  Y02E50/32 ,  Y10T137/87917

Abstract: Methods and devices are provided for transfer of particulate material, such as biomass feedstocks, into and out of pressurized reactors. Improved sluice devices have an L-shaped sluice chamber having an upper, vertical component in communication with a horizontal loading chamber and a lower component in communication with a vertical reactor inlet or outlet. Piston valves seal the sluice inlet and outlet by axial displacement across the vertical component of the sluice chamber and across the vertical reactor inlet or outlet. Relative to other methods for reactor unloading, these devices consume less steam and significantly reduce furfural content of unloaded, pretreated biomass. An optional hybrid plug/sluice method of biomass feeding using the devices permits biomass loading at sluice pressures intermediate between atmospheric and reactor pressure, thereby reducing “pump cycle” time and increasing biomass throughput capacity.

Abstract translation: 提供的方法和装置用于将诸如生物质原料的颗粒材料转移到加压反应器中和从加压反应器中排出。 改进的闸门装置具有L形闸门室，其具有与垂直反作用器入口或出口连通的水平加载室和下部构件连通的上部垂直部件。 活塞阀通过在闸室垂直部件和垂直反应器入口或出口的轴向位移来密封闸门入口和出口。 相对于反应堆卸载的其他方法，这些装置消耗较少的蒸汽并显着减少未加载的预处理生物质的糠醛含量。 使用这些装置的生物质进料的可选的混合塞/水闸方法允许在大气压和反应堆压力之间的闸门压力下生物质负载，从而减少“泵循环”时间并增加生物量通过能力。

公开(公告)号：US09005537B1

公开(公告)日：2015-04-14

申请号：US14205177

申请日：2014-03-11

Applicant: George Francis Cudahy

Inventor： George Francis Cudahy

IPC: B01J3/02 ,  C10G1/06 ,  B01J19/00 ,  B01J19/20

CPC classification number: B01J3/02 ,  B01J19/004 ,  B01J19/20 ,  C10G1/06

Abstract: A continuous high capacity system for converting a combination of natural gas and coal into liquid fuel, using a pug for blending less than 200 micron diameter particulate with a plasticizing agent; a sealing auger for forming an agglomerated material and sealing, a cutting device, a vacuum chamber to remove air from the cut material, a second sealing auger for forming a de-aerated agglomerated material and sealing, a second cutting device, a gas injection chamber for impregnating the de-aerated cut material with natural gas, an extruder forming an extrudate, a heating chamber to evolve at least one gas; a pressure sensor and temperature sensors in the heating chamber, a cooling chamber providing controlled pressure and controlled temperature cooling of the evolved gasses, wherein the cooling chamber liquefies sequentially at least 50 percent of the evolved gasses forming a liquid.

Abstract translation: 用于将天然气和煤的组合转化为液体燃料的连续高容量系统，使用用于将小于200微米直径的颗粒与增塑剂混合的哈巴狗; 用于形成附聚材料并密封的密封螺旋钻，切割装置，用于从切割材料去除空气的真空室;用于形成脱气附聚材料和密封的第二密封螺旋钻;第二切割装置;气体喷射室 用于用天然气浸渍脱气的切割材料，形成挤出物的挤出机，加热室以放出至少一种气体; 加热室中的压力传感器和温度传感器，提供受控压力并且对放出的气体进行受控温度冷却的冷却室，其中冷却室顺序地液化至少50％的形成液体的放出气体。

公开(公告)号：US08443724B2

公开(公告)日：2013-05-21

申请号：US12838041

申请日：2010-07-16

Applicant: Murray J. Burke

Inventor： Murray J. Burke

IPC: B30B11/24 ,  B01J19/20 ,  B01J4/00

CPC classification number: B01J8/002 ,  B01J3/02 ,  B01J8/0045 ,  B01J2208/0007 ,  B01J2208/0061 ,  B01J2208/00699 ,  B01J2208/00752 ,  B01J2219/00198 ,  B01J2219/00231 ,  B30B11/241 ,  B30B11/265 ,  C10L5/44 ,  Y02E50/10 ,  Y02E50/30

Abstract: An apparatus is provided for treating a loose fibrous solid organic feedstock. The apparatus includes a reactor vessel and a compressor operable to introduce feedstock at elevated pressure into the reactor chamber. The apparatus includes means for controlling and modulating moisture level within the reactor. The apparatus includes an outflow or discharge assembly that has its own feeder or drive for packing feedstock into a discharge accumulator. The discharge accumulator feeds an outflow valve, in this case a uni-directional rotation ball valve operated by a servo motor. Discharge from the valve may be carried through a diffuser into a settling cyclone. In operation the ball valve is rotated to open and close the outflow passageway, the rate of rotation being variable in real time. The rate of rotation may be a function of the pressure or other parameters sensed in the reaction vessel, and, particularly, in the accumulator immediately upstream of the ball valve, and of proxy sensed values such as discharge feeder motor current.

Abstract translation: 提供了一种用于处理松散纤维状固体有机原料的设备。 该装置包括反应器容器和可操作以将进料以升高的压力引入反应器室中的压缩机。 该装置包括用于控制和调节反应器内的水分含量的装置。 该装置包括具有其自己的进料器或驱动器的排出或排出组件，用于将原料包装到排放蓄能器中。 排放蓄能器供给流出阀，在这种情况下是由伺服电动机操作的单向旋转球阀。 来自阀的排出物可以通过扩散器进入沉降旋风分离器。 在操作中，球阀旋转以打开和关闭流出通道，旋转速率实时变化。 旋转速率可以是反应容器中感测的压力或其他参数的函数，特别是在紧邻球阀上游的蓄能器中，以及代理感测值，例如放电给电机电流。

公开(公告)号：US20120076706A1

公开(公告)日：2012-03-29

申请号：US13244409

申请日：2011-09-24

Applicant: Bernd BONSO

Inventor： Bernd BONSO

IPC: B01J7/00

CPC classification number: B01J19/24 ,  B01J3/02 ,  B01J3/03 ,  B01J4/002 ,  B01J19/0006 ,  B01J19/0013 ,  B01J2204/005 ,  B01J2204/007 ,  B01J2219/00162 ,  B01J2219/00164 ,  B01J2219/00247 ,  B01J2219/00252 ,  C10L3/108

Abstract: An apparatus for making a gaseous clathrate has a closed reaction vessel to which are fed a reaction gas and a reaction liquid while an interior of the vessel is maintained at a predetermined pressure and a predetermined temperature so that the gaseous clathrate is formed in the vessel. An outlet nozzle on the vessel defines a flow passage opening into the vessel and having an inner wall surface extending between an inner inlet end inside the vessel and an outer outlet end. The passage extends along an axis, is rotation-symmetrical about the axis, and is of decreasing flow cross section from its inner end to its outer end. The inner wall surface is curved in an S-shape from the inner end to the outer end so that pressure in the vessel forces the formed clathrate out through the passage with increasing compression as the flow cross section decreases.

Abstract translation: 用于制备气态包合物的装置具有封闭的反应容器，在容器的内部保持在预定的压力和预定的温度下供给反应气体和反应液体，从而在容器中形成气态包合物。 容器上的出口喷嘴限定了通向容器的流动通道，并且具有在容器内的内部入口端和外部出口端之间延伸的内壁表面。 通道沿着轴线延伸，围绕轴线旋转对称，并且从其内端到其外端具有减小的流动横截面。 内壁表面从内端到外端弯曲成S形，使得当流动横截面减小时，容器中的压力迫使形成的包合物通过通道增加压缩。

公开(公告)号：US20110197992A1

公开(公告)日：2011-08-18

申请号：US13062522

申请日：2010-08-27

Applicant: Jens Fink ,  Niels Nielsen Poulsen

Inventor： Jens Fink ,  Niels Nielsen Poulsen

IPC: B65B31/00

CPC classification number: B01J8/002 ,  B01J3/02 ,  B01J8/0015 ,  B01J8/0035 ,  B01J2208/00743 ,  B01J2208/00752 ,  B01J2208/00761 ,  B01J2208/00769 ,  B65G53/48 ,  C12P2201/00 ,  Y02E50/32 ,  Y10T137/87917

Abstract: Methods and devices are provided for transfer of particulate material, such as biomass feedstocks, into and out of pressurized reactors. Improved sluice devices have an L-shaped sluice chamber having an upper, vertical component in communication with a horizontal loading chamber and a lower component in communication with a vertical reactor inlet or outlet. Piston valves seal the sluice inlet and outlet by axial displacement across the vertical component of the sluice chamber and across the vertical reactor inlet or outlet. Relative to other methods for reactor unloading, these devices consume less steam and significantly reduce furfural content of unloaded, pretreated biomass. An optional hybrid plug/sluice method of biomass feeding using the devices permits biomass loading at sluice pressures intermediate between atmospheric and reactor pressure, thereby reducing “pump cycle” time and increasing biomass throughput capacity.

Abstract translation: 提供的方法和装置用于将诸如生物质原料的颗粒材料转移到加压反应器中和从加压反应器中排出。 改进的闸门装置具有L形闸门室，其具有与垂直反作用器入口或出口连通的水平加载室和下部构件连通的上部垂直部件。 活塞阀通过在闸室垂直部件和垂直反应器入口或出口的轴向位移来密封闸门入口和出口。 相对于反应堆卸载的其他方法，这些装置消耗较少的蒸汽并显着减少未加载的预处理生物质的糠醛含量。 使用这些装置的生物质进料的可选的混合塞/水闸方法允许在大气压和反应堆压力之间的闸门压力下生物质负载，从而减少“泵循环”时间并增加生物量通过能力。

公开(公告)号：US20110162741A1

公开(公告)日：2011-07-07

申请号：US13043486

申请日：2011-03-09

Applicant: Jens Fink ,  Niels Nielsen Poulsen

Inventor： Jens Fink ,  Niels Nielsen Poulsen

IPC: G05D16/06

CPC classification number: B01J8/002 ,  B01J3/02 ,  B01J8/0015 ,  B01J8/0035 ,  B01J2208/00743 ,  B01J2208/00752 ,  B01J2208/00761 ,  B01J2208/00769 ,  B65G53/48 ,  C12P2201/00 ,  Y02E50/32 ,  Y10T137/87917

Abstract: Methods and devices are provided for transfer of particulate material, such as biomass feedstocks, into and out of pressurized reactors. Improved sluice devices have an L-shaped sluice chamber having an upper, vertical component in communication with a horizontal loading chamber and a lower component in communication with a vertical reactor inlet or outlet. Piston valves seal the sluice inlet and outlet by axial displacement across the vertical component of the sluice chamber and across the vertical reactor inlet or outlet. Relative to other methods for reactor unloading, these devices consume less steam and significantly reduce furfural content of unloaded, pretreated biomass. An optional hybrid plug/sluice method of biomass feeding using the devices permits biomass loading at sluice pressures intermediate between atmospheric and reactor pressure, thereby reducing “pump cycle” time and increasing biomass throughput capacity.

公开(公告)号：US20110021592A1

公开(公告)日：2011-01-27

申请号：US12441308

申请日：2007-09-16

Applicant: Shlomo Magdassi ,  Hadas Netivi ,  Katrin Goshen

Inventor： Shlomo Magdassi ,  Hadas Netivi ,  Katrin Goshen

IPC: A61K31/415 ,  C07D231/12 ,  C07D309/30 ,  A61K31/351

CPC classification number: B01J3/02 ,  A61K9/1075 ,  A61K9/5123 ,  A61K9/5138 ,  A61K9/5192

Abstract: The present invention provides a process for preparing a redispersible powder of nanoparticles of a water-insoluble organic compound, the process including the steps of: (i) preparing an oil-in-water microemulsion comprising a water-insoluble organic compound, a volatile water-immiscible organic solvent, water, and at least one surfactant; and (ii) removing the volatile water-immiscible organic solvent and the water so as to form the redispersible powder comprising said nanoparticles, wherein the nanoparticle are in a particulate form, and wherein the solubility of the water-insoluble organic compound is at least about 5 times greater than the solubility of the water-insoluble organic compound in unprocessed form. Step (i) can further include the addition of co-solvent or polymer. The water-insoluble organic compound can be a pharmaceutically active agent (in particular a statin), a cosmetic active agent, an anti oxidant, a preservative, a colorant, a food additive, an agriculturally active compound and a fragrance.

Abstract translation: 本发明提供一种制备水不溶性有机化合物纳米颗粒的可再分散粉末的方法，该方法包括以下步骤：（i）制备包含水不溶性有机化合物，挥发性水的水包油微乳液 可混溶的有机溶剂，水和至少一种表面活性剂; 和（ii）除去挥发性的与水不混溶的有机溶剂和水，以便形成包含所述纳米颗粒的可再分散粉末，其中所述纳米颗粒是颗粒形式，并且其中所述水不溶性有机化合物的溶解度为至少约 比未加工形式的水不溶性有机化合物的溶解度大5倍。 步骤（i）可以进一步包括加入共溶剂或聚合物。 水不溶性有机化合物可以是药物活性剂（特别是他汀类），美容活性剂，抗氧化剂，防腐剂，着色剂，食品添加剂，农业活性化合物和香料。

公开(公告)号：US20080102025A1

公开(公告)日：2008-05-01

申请号：US11576952

申请日：2005-10-13

Applicant: Volker Kurth ,  Attila Jambor ,  Richard Rau ,  Christian Ringelhan

Inventor： Volker Kurth ,  Attila Jambor ,  Richard Rau ,  Christian Ringelhan

IPC: C01B39/04

CPC classification number: B01J29/70 ,  B01J3/02 ,  B01J3/04 ,  B01J19/18 ,  B01J35/006 ,  B01J2219/00162

Abstract: The invention relates to a reaction vessel comprising at least:a pressure-resistant main tank (1);a turbulence-reduction tank (2) connected to the main tank (1);wherein the turbulence-reduction tank (2) has a pressure-regulating valve (9) through which gaseous products can be discharged from the turbulence-reduction tank (2) to the outside. The invention further relates to a process for producing molecular sieves, in particular zeolites, which can be carried out in the reaction vessel of the invention.

Abstract translation: 本发明涉及至少包括：耐压主罐（1）的反应容器; 连接到主箱（1）的湍流减少箱（2）; 其中，所述湍流减压罐（2）具有压力调节阀（9），气体产物可以通过所述压力调节阀从所述湍流还原罐（2）排出到外部。 本发明还涉及可在本发明的反应容器中进行的分子筛特别是沸石的制备方法。