公开(公告)号：US5374148A

公开(公告)日：1994-12-20

申请号：US40025

申请日：1993-03-30

Applicant: Reijo Kilpelainen ,  Risto Laukkanen ,  Matti Virolainen

Inventor： Reijo Kilpelainen ,  Risto Laukkanen ,  Matti Virolainen

IPC: B01J3/02 ,  B01J8/00 ,  C10J3/30 ,  F23K3/00

CPC classification number: C10J3/30 ,  B01J3/02 ,  B01J8/0035 ,  C10J2200/154 ,  C10J2200/158

Abstract: The invention relates to a procedure and an apparatus for feeding solid material into a pressurized space. According to the invention, the apparatus comprises a feed chamber (12) communicating with the pressurized space (1) via a gate (13), a piston cylinder (8) adjoining the feed chamber (12) and provided with an aperture (28) in its wall for the intake of solid material, and a piston (9) which consists of an inner and an outer piston (11,10), moves within the piston cylinder (8) and closes the feed chamber (12) tightly when in its front position. The inner piston (11) moves inside the outer piston (10) and in the feed chamber (12) to insert the solid material into the pressurized space (1). In the procedure of the invention, the solid material is supplied into the feed chamber (12) through the piston cylinder (8) and the aperture (28) in its wall while the piston (9) is in its rear position, the piston (9) is thrust into its front position so that the feed chamber (12) is tightly closed, a pressure corresponding to that in the pressurized space (1) is formed in the feed chamber (12), the gate (13) between the pressurized space (1) and the feed chamber (12) is opened and the inner piston (11) is thrust into its front position.

Abstract translation: 本发明涉及一种用于将固体材料进料到加压空间中的方法和装置。 根据本发明，该装置包括通过门（13）与加压空间（1）连通的进料室（12），与进料室（12）相邻并设有孔（28）的活塞缸（8） 在其壁上用于吸收固体材料，并且由内活塞和外活塞（11,10）组成的活塞（9）在活塞缸（8）内移动，并且当进入 其前置位置 内活塞（11）在外活塞（10）内和进料室（12）内移动，将固体材料插入加压空间（1）。 在本发明的方法中，当活塞（9）处于其后部位置时，固体材料通过活塞缸（8）和其壁中的孔（28）供应到进料室（12）中，活塞 9）被推入其前部位置，使得进料室（12）被紧密地关闭，在进料室（12）中形成与加压空间（1）中的压力相对应的压力，加压 空间（1）和进料腔（12）打开，内活塞（11）推入其前位置。

公开(公告)号：US5325603A

公开(公告)日：1994-07-05

申请号：US957153

申请日：1992-11-16

Applicant: Donald H. Eastham ,  James W. Reeves

Inventor： Donald H. Eastham ,  James W. Reeves

IPC: F26B3/08 ,  B01J3/02 ,  B01J4/00 ,  B01J8/00 ,  B01J8/24 ,  C22B1/10 ,  C22B5/14 ,  C22B34/12 ,  F26B17/00 ,  F26B17/10 ,  F26B25/00

CPC classification number: B01J8/0025 ,  B01J3/02 ,  B01J8/0015 ,  B01J8/003 ,  B01J8/0055 ,  C22B1/10 ,  F26B25/002 ,  F26B3/08 ,  B01J2208/00672 ,  B01J2208/00752 ,  B01J2208/00769 ,  C22B5/14

Abstract: The invention provides an improved method and apparatus for feeding solids to a fluidized bed reactor. A back pressure control valve regulates the pressure drop between the pressure above a solids column in a standpipe and the pressure in the reactor. Solids are fed from the standpipe via a conduit without valve means, the conduit contains a bend of an angle greater than the angle of repose of the solids.

Abstract translation: 本发明提供了一种用于将固体输送到流化床反应器的改进的方法和装置。 背压控制阀调节立管中的固体柱上方的压力与反应器中的压力之间的压降。 固体通过没有阀装置的导管从立管进料，导管包含大于固体的休止角的弯曲。

公开(公告)号：US5272880A

公开(公告)日：1993-12-28

申请号：US822179

申请日：1992-01-16

Applicant: Hiroshi Nishizato ,  Hirofumi Ono

Inventor： Hiroshi Nishizato ,  Hirofumi Ono

IPC: C23C16/44 ,  B01F3/02 ,  B01J3/02 ,  C23C16/448 ,  C23C16/455 ,  H01L21/205 ,  H01L21/31 ,  F17C13/00

CPC classification number: B01J3/02 ,  B01F3/022 ,  C23C16/4481

Abstract: A liquid vaporizer-feeder has a unitary housing structure for both a control valve for controlling the amount of a liquid passing therethrough and a vaporization valve for causing the liquid from the control valve to be vaporized and transported out by a carrier gas. The housing structure has a throughhole through which the two valves are connected. The throughhole is short and narrow, and has a portion made even narrower such that the pressure in the liquid passing therethrough is increased, preventing bubbles from forming in the throughhole. As a result, vaporized liquid can be supplied at a steadier rate, for example, to a reaction chamber.

Abstract translation: 液体蒸发器给料器具有用于控制通过其中的液体量的控制阀和用于使来自控制阀的液体被载气气化并输出的汽化阀的整体外壳结构。 壳体结构具有连接两个阀的通孔。 通孔短而窄，并且具有更窄的部分，使得通过其中的液体中的压力增加，防止在通孔中形成气泡。 结果，蒸发的液体可以以更稳定的速率供应到例如反应室。

公开(公告)号：US5073348A

公开(公告)日：1991-12-17

申请号：US549666

申请日：1990-07-09

Applicant: Charles M. DeWoody

Inventor： Charles M. DeWoody

IPC: B01J3/02 ,  B01J4/00 ,  B01L99/00

CPC classification number: B01L99/00 ,  B01J3/02 ,  B01J4/001

Abstract: A pressure equalizing liquid addition funnel for a closed system reactor is described. The funnel includes an internal valve stem which seats in the outlet port and extends therethrough and which defines a lumen which extends axially from below the outlet port upwardly to a port in the valve stem in the upper portion of said flask. The valve stem then terminates in a valve cap which is threadedly mounted on the funnel whereby rotation of the cap will cause the valve to engage or disengage a valve seat at the outlet.

Abstract translation: 描述了用于封闭系统反应器的均压液体加料漏斗。 漏斗包括内部阀杆，其位于出口端口并延伸穿过其中，并且限定了从出口端口的下方向上延伸到所述烧瓶的上部中的阀杆中的端口的内腔。 阀杆然后终止于螺纹安装在漏斗上的阀盖，由此盖的旋转将导致阀在出口处接合或脱离阀座。

公开(公告)号：US5009849A

公开(公告)日：1991-04-23

申请号：US372095

申请日：1989-06-28

Applicant: Jerry R. Ebner ,  John T. Gleaves

Inventor： Jerry R. Ebner ,  John T. Gleaves

IPC: B01J3/00 ,  B01J3/02 ,  B01J3/03 ,  B01J8/00 ,  B01J8/02 ,  B01J8/06 ,  G01N31/10

CPC classification number: B01J8/001 ,  B01J3/006 ,  B01J3/02 ,  B01J3/03 ,  B01J8/0278 ,  B01J8/067 ,  G01N31/10 ,  B01J2208/00061 ,  B01J2208/0007 ,  B01J2208/00132 ,  B01J2208/00176 ,  B01J2208/00212 ,  B01J2208/00345 ,  B01J2208/00407 ,  B01J2208/00415

Abstract: Disclosed are an apparatus adapted for use in a temporal analysis of products (TAP) system for studying catalytic reactions, a catalytic reactor provided with heat exchange capability and useful in the TAP system, and an apparatus for use in gas processing which can also be used in a TAP system. The gas processing apparatus includes a manifold for introduction of a plurality of gases into a gas processing system. The manifold comprises a plurality of channels through which gas may flow toward the gas processing system, and a mixing chamber having an inlet in communication with the plurality of channels and an outlet in communication with the gas processing system. At least one of the channels has a rapidly operable feed valve at the terminus of the channel at which it communicates with the chamber inlet. The mixing chamber has a void volume that is small relative to the working volume of the gas processing system. The catalytic reactor comprises any of several novel combinations of catalytic reaction chamber and constructions providing for transfer of heat to the chamber. The novel TAP system apparatus includes a housing and, within the housing, a catalytic reactor, a collimating slit or the like for providing a resolved pulse of product gas, an analytical device for real time analysis of the product pulse, and circuitry for coordinating the product pulse with scanning of the analytical device. The TAP apparatus may also include a cryogenic surface surrounding the product pulse path, a low residence time mixing zone ahead of the reactor, and/or a manifold of the type described above.

Abstract translation: 公开了一种适用于时间分析用于研究催化反应的产物（TAP）系统的设备，具有热交换能力并且在TAP系统中有用的催化反应器的设备，以及也可用于气体处理的设备 在TAP系统中。 气体处理装置包括用于将多种气体引入气体处理系统的歧管。 歧管包括多个通道，气体可以通过该通道流向气体处理系统，以及具有与多个通道连通的入口和与气体处理系统连通的出口的混合室。 至少一个通道在通道的末端具有快速可操作的进料阀，在该通道的端部与腔室入口连通。 混合室具有相对于气体处理系统的工作容积小的空隙体积。 催化反应器包括催化反应室的几种新型组合和提供将热量传递到室的结构的任何一种。 该新型TAP系统装置包括壳体，并且在壳体内部具有催化反应器，准直缝隙等，用于提供产物气体的分辨脉冲，用于产物脉冲的实时分析的分析装置和用于协调 产品脉冲与扫描分析装置。 TAP设备还可以包括围绕产物脉冲路径的低温表面，反应器前面的低停留时间混合区域和/或上述类型的歧管。

公开(公告)号：US4942972A

公开(公告)日：1990-07-24

申请号：US327449

申请日：1989-03-22

Applicant: Eiichi Hiraoka ,  Toshio Akagi ,  Kiyotaka Yano ,  Junji Onaka

Inventor： Eiichi Hiraoka ,  Toshio Akagi ,  Kiyotaka Yano ,  Junji Onaka

IPC: F16J12/00 ,  B01J3/02 ,  F16J13/00 ,  F16J13/02

CPC classification number: F16J13/00 ,  B01J3/02

Abstract: A pressure vessel includes a cylindrical, fixed body which is closed at the two ends thereof, the central portion of the body forming a sample accommodating space, and a drum body provided in such a manner as to be rotatable relative to the outer periphery of the body. The body has an opening in a lateral portion thereof, and the drum body 3 has an opening at a position which faces the opening formed in the body at one rotated position.

公开(公告)号：US4912078A

公开(公告)日：1990-03-27

申请号：US208935

申请日：1988-06-20

Applicant: Pieter Krijgsman

Inventor： Pieter Krijgsman

IPC: C01F11/04 ,  B01J3/02 ,  B01J3/04 ,  B01J19/18 ,  C01B20060101 ,  C01B13/18 ,  C01B13/36 ,  C01B33/24 ,  C01F20060101 ,  C01F11/00 ,  C01G23/00 ,  C01G25/00

CPC classification number: C01B13/185 ,  B01J19/1862 ,  B01J3/02 ,  B01J3/04 ,  C01B13/366 ,  C01F11/00 ,  C01F7/162 ,  C01G23/006 ,  C01G25/00 ,  B01J2219/00065 ,  B01J2219/0009 ,  B01J2219/00103 ,  B01J2219/00779 ,  B01J2219/185 ,  B01J2219/1943 ,  C01P2002/32 ,  C01P2002/34 ,  C01P2002/54 ,  Y10S502/524 ,  Y10T137/0396 ,  Y10T137/313 ,  Y10T137/86187

Abstract: Composite powders for spinels, MgO.nAl.sub.2 O.sub.3 (n=1 and 2), are synthesized hydrothermally using commercially available hydroxide reactants. The synthesis is carried out in an aqueous suspension within an autoclave under a pressure of 4 Mega-Pascals (MPa) and at a corresponding saturated steam temperature of 523.degree. K. Powder characterization has shown that the particle size ranges from 2 to 10 .mu.m. Sintering of preformed green bodies comprising compressed powder, without the use of additives, is then carried out at 1873.degree. K. in one atmosphere, resulting in a spinel having a density 94% of theorietical. Structure and microstructure have been studied by X-ray diffraction and scanning electron microscopy, and compressive strength of the resulting spinels has been determined.

Abstract translation: 使用市售氢氧化物反应物水热合成尖晶石的复合粉末，MgO.nAl 2 O 3（n = 1和2）。 该合成在高压釜内在4兆帕（MPa）的压力和相应的饱和蒸汽温度为523℃下在水性悬浮液中进行。粉末表征显示，粒度范围为2-10μm 。 然后在1873°K下在一个大气压下进行包含压缩粉末的预制坯体的烧结，而不使用添加剂，得到密度为94％的尖晶石。 已经通过X射线衍射和扫描电子显微镜研究了结构和微观结构，并确定了所得尖晶石的抗压强度。

公开(公告)号：US4830233A

公开(公告)日：1989-05-16

申请号：US73995

申请日：1987-07-16

Applicant: Hubert Thelen ,  Menrad Wesp

Inventor： Hubert Thelen ,  Menrad Wesp

IPC: B01D35/16 ,  B01J3/02 ,  B65G53/46

CPC classification number: B65G53/4691 ,  B01D35/16 ,  B01J3/02

Abstract: A sluice type apparatus for discharging batches of material from a pressurized enclosure has a container with an upper inlet and a lower outlet each closable by a slide gate. Preferably, each slide gate has two slide gate members driven by respective piston cylinder devices so that one gate is closed while the other gate is open and vice versa. At least the slide gate members for opening and closing the inlet are withdrawn from their inlet closing position into a respective outwardly closed or sealed chamber for making it easier to keep the container pressurized. The seals between the chamber entrance slots and the respective slide gate member are not required to be precision seals because any material that may pass into these outwardly closed or sealed chambers is easily removed again.

Abstract translation: 用于从加压外壳排出批料的闸阀式装置具有容器，其具有可由滑动门关闭的上入口和下出口。 优选地，每个滑动门具有由相应的活塞气缸装置驱动的两个滑动门构件，使得一个门关闭，而另一个门打开，反之亦然。 至少用于打开和关闭入口的滑动门构件从其入口关闭位置被抽出到相应的向外关闭或密封的室中，以使得容易保持容器的加压。 腔室入口槽和相应的滑动门构件之间的密封件不需要是精密密封件，因为可以再次进入这些向外关闭或密封的腔室中的任何材料。

公开(公告)号：US4413977A

公开(公告)日：1983-11-08

申请号：US328693

申请日：1981-12-08

Applicant: Motoharu Takano ,  Minoru Hoshino

Inventor： Motoharu Takano ,  Minoru Hoshino

IPC: A23L3/00 ,  B01J3/02 ,  F27D19/00 ,  A45B9/00

CPC classification number: B01J3/02 ,  A23L3/001

Abstract: An apparatus for taking a material to be treated into and out of a treating high pressure tank such as a heating sterilization tank comprises a conveyor passage interconnecting the high pressure tank and a water tank and constituted by two or more partially cylindrical casings connected in a side-by-side relation and each rotatably accomodating a rotary closure member having 2 to 6 blades adapted to make a sliding contact with the inner peripheral surface of the casing. Due to a specific phase difference between the blades of adjacent rotary closure members, the conveyor passage is always closed by some of the blades. A pair of endless conveyor chains, carrying a plurality of treating vessels accomodating the material, are adapted to run along both side surfaces of the conveyor passage through the high pressure tank and the water tank in a timed relation to the rotation of the rotary closure members. Means are provided for returning the leaked liquid back to the high pressure tank from the water tank.

Abstract translation: 用于将待处理的材料进出处理高压罐例如加热灭菌罐的装置包括将高压罐和水箱相互连接的输送通道，由两个或更多个部分圆筒形的壳体连接在一起 并且每个可旋转地容纳具有2至6个叶片的旋转关闭构件，其适于与壳体的内周表面滑动接触。 由于相邻的旋转关闭构件的叶片之间的特定相位差，输送通道总是被一些叶片关闭。 携带多个处理容器的一对环形输送机链条，适用于材料，适于沿着与旋转闭合件的旋转定时关系的高压罐和水箱的输送通道的两个侧表面延伸 。 提供了用于将泄漏的液体从水箱返回到高压罐的装置。

公开(公告)号：US4398852A

公开(公告)日：1983-08-16

申请号：US235195

申请日：1981-02-17

Applicant: John D. Milligan

Inventor： John D. Milligan

IPC: B01J3/02 ,  B01J8/00 ,  B65G53/30

CPC classification number: B01J3/02 ,  B01J8/003

Abstract: A method for adding and removing fine particles from a pressurized reactor is provided, which comprises connecting the reactor to a container, sealing the container from the reactor, filling the container with particles and a liquid material compatible with the reactants, pressurizing the container to substantially the reactor pressure, removing the seal between the reactor and the container, permitting particles to fall into or out of the reactor, and resealing the container from the reactor. An apparatus for adding and removing particles is also disclosed.

Abstract translation: 提供了一种从加压反应器中加入和除去细颗粒的方法，其包括将反应器连接到容器，将容器与反应器密封，用容器填充容器和与反应物相容的液体材料，将容器加压至基本上 反应器压力，去除反应器和容器之间的密封，允许颗粒落入或离开反应器，并将反应器重新密封容器。 还公开了一种用于添加和除去颗粒的装置。