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    PROCESS FOR PREPARING ALPHA-BIS-OXIME OF HIGH PURITY
    35.
    发明专利
    PROCESS FOR PREPARING ALPHA-BIS-OXIME OF HIGH PURITY 未知

    公开(公告)号：CZ315597A3

    公开(公告)日：1998-04-15

    申请号：CZ315597

    申请日：1996-03-25

    Applicant: BASF AG

    Inventor： MULLER RUTH DR ,  BENOIT REMY DR ,  BAYER HERBERT DR ,  GOTZ NORBERT DR ,  SAUTER HUBERT DR

    IPC: C07D231/12 ,  C07B61/00 ,  C07C249/04 ,  C07C249/12 ,  C07C249/14 ,  C07C251/38 ,  C07C251/48 ,  C07C255/62 ,  C07D261/08

    Abstract: PCT No. PCT/EP96/01306 Sec. 371 Date Oct. 7, 1997 Sec. 102(e) Date Oct. 7, 1997 PCT Filed Mar. 25, 1996 PCT Pub. No. WO96/32373 PCT Pub. Date Oct. 17, 1996A process for the preparation of largely isomerically pure alpha -bisoximes of the formula IaR1O-N=CR2-CR3=N-OR4Iawhere the groups R1O- and R2 on the N=C bond are cis to one another and where the radicals have the following meanings: R1 and R4 are hydrogen or a C-organic radical; R2 is hydrogen, cyano, nitro, hydroxyl, amino, halogen or an organic radical which can be bonded to the structure directly or via an oxygen, sulfur or nitrogen atom; R3 is hydrogen, cyano, nitro, hydroxyl, amino, halogen, alkyl, haloalkyl, alkoxy, haloalkoxy, alkylthio, alkylamino, dialkylamino or cycloalkyl, from a mixture of the isomers of the a-bisoximes Ia and Ib is described.

    39.
    发明专利
    未知

    公开(公告)号：DE59307141D1

    公开(公告)日：1997-09-25

    申请号：DE59307141

    申请日：1993-04-01

    Applicant: BASF AG

    Inventor： BENOIT REMY DR ,  SAUTER HUBERT DR

    IPC: C07C253/30 ,  C07C249/12 ,  C07C251/60 ,  C07C255/17 ,  C07C255/57 ,  C07C255/61 ,  C07C259/04 ,  C07C259/12 ,  C07C259/14 ,  C07C259/18 ,  C07C317/24 ,  C07C323/47 ,  C07C323/63 ,  C07D209/14 ,  C07D209/48 ,  C07D213/53 ,  C07D213/57 ,  C07D239/26 ,  C07D277/20 ,  C07D277/38 ,  C07D333/24 ,  C07D333/36

    Abstract: Process for the preparation of an o-iminooxymethylbenzoic acid of the general formula I in which m denotes an integer from 0 to 3, X denotes alkyl, alkoxy, nitro, cyano, or halogen, R1 and R2 denote hydrogen, cyano, hydroxyl, alkyl, cycloalkyl, alkenyl, cycloalkenyl, alkynyl, alkoxy, alkylthio, benzylthio, benzylamino, alkylcarbonyl, optionally substituted phenylcarbonyl, optionally substituted benzylcarbonyl, alkoxycarbonyl, optionally substituted phenoxycarbonyl, optionally substituted benzyloxycarbonyl, optionally substituted aryl, optionally substituted aryloxy, optionally substituted arylthio, optionally substituted arylalkyl, optionally substituted arylalkenyl, optionally substituted aryloxyalkyl, optionally substituted arylthioalkyl, optionally substituted hetaryl, optionally substituted hetaryloxy, optionally substituted hetarylthio, optionally substituted heteroarylalkyl, optionally substituted hetarylalkenyl, optionally substituted hetaryloxyalkyl, hetarylthioalkyl, optionally substituted heterocyclyl, optionally substituted heterocyclyloxy, or denote N(R )2, where R denotes H, alkyl or phenyl, or denote -CO-N(R )2, where R denotes H, alkyl or phenyl, or R and R together with the C atom which they substitute can form a carbo- or heterocyclic ring, or R or R denotes halogen or the group denotes the radical where n denotes the integers 1 to 4 and the radicals R denote H, halogen, cyano, nitro; alkyl, alkoxy, aryl, aryloxy, benzyloxy, hetaryl and hetaryloxy, by reacting an oxime of the general formula II in which R1 and R2 have the abovementioned meanings, with a lactone of the general formula III in which X and m have the abovementioned meaning, if appropriate in the presence of a base or of a diluent, and o-iminooxymethylbenzoic acids of the abovementioned formula.

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