32.
    发明专利
    未知

    公开(公告)号:DE60327567D1

    公开(公告)日:2009-06-18

    申请号:DE60327567

    申请日:2003-12-29

    Abstract: The present invention relates to a process for the preparation of pure high quality 3,3', 4,4'-tetraminobiphenyl (TAB) in high yields. The present invention also discloses a process for the preparation of 3,3',4,4' tetraminobiphenyl (TAB) comprising a three step process: (1) oxidation 3,3'-dichloro 4,4'-diaminobiphenyl (DCB) with 50% aq. H2O2, (2) ammonolysis of the resulting 3,3'-dinitro 4,4'-dinitrobiphenyl (DCDNB) and (3) reduction of 3,3'-diamino-4,4'-dinitrobiphenyl (DADNB) with stannous chloride and concentrated hydrochloric acid.

Patent Agency Ranking