公开(公告)号：JPH11140486A

公开(公告)日：1999-05-25

申请号：JP23327198

申请日：1998-08-19

Applicant: KAO CORP

Inventor： SAKUMA YASUMITSU ,  MIYOSHI KAZUHITO ,  TAKAHASHI HIROSHI

IPC: B01F17/00 ,  B01J13/00 ,  C07C303/44 ,  C07C305/06 ,  C11D1/29

Abstract: PROBLEM TO BE SOLVED: To provide a method for producing an anionic surfactant slurry having a reduced content of impurities in the surfactant slurry in a small state of energy burden and facility load (simplification of facilities). SOLUTION: In this method for producing an anionic surfactant slurry having a reduced content of impurities from an anionic surfactant slurry containing impurities, (A) the anionic surfactant slurry containing impurities is brought into contact with at least one or more inert gases under reduced pressure, (B) the contact product obtained by bringing the anionic surfactant slurry containing impurities into contact with the inert gas is expanded in volume, the impurities are accompanied by the inert gas and separated from the anionic surfactant slurry and (C) the anionic surfactant slurry having a reduced content of impurities is recovered.

公开(公告)号：JP2009102274A

公开(公告)日：2009-05-14

申请号：JP2007276702

申请日：2007-10-24

Applicant: Kao Corp ,  花王株式会社

Inventor： MIYAHARA TSUTOMU ,  SAKUMA YASUMITSU ,  HORIBATA TATSUYA

IPC: A61K8/34 ,  A61K8/33 ,  A61K8/40 ,  A61K8/73 ,  A61K8/84 ,  A61Q11/00

Abstract: PROBLEM TO BE SOLVED: To obtain a dentifrice granule finely and stably containing a non-cationic germicide and to provide a method for producing the dentifrice granule.
SOLUTION: The method for producing a dentifrice powder includes a process 1 for mixing 100 parts by mass of a 1-4C alcohol with 0-200 parts by mass of water and 6-110 parts by mass of a non-cationic germicide to give a mixed solution A, a process 2 for mixing an aqueous solution of a water-soluble polymer, obtained by mixing 100 parts by mass of water with 0.025-1 part by mass of a water-soluble polymer, with a water-insoluble inorganic binder and a water-insoluble powder material to give a slurry B and a process 3 for mixing the mixed solution A with the slurry B to give a slurry C. The dentifrice granule is obtained by the production method.
COPYRIGHT: (C)2009,JPO&INPIT

Abstract translation: 待解决的问题：获得精细稳定地含有非阳离子杀菌剂的洁齿剂颗粒，并提供一种制备洁齿剂颗粒的方法。 解决方案：洁牙粉的制造方法包括将100质量份的1-4C醇与0〜200质量份的水混合的方法1和6〜10质量份的非阳离子杀菌剂 得到混合溶液A，将通过将100质量份水与0.025-1质量份水溶性聚合物混合而获得的水溶性聚合物的水溶液与水不溶性的混合溶液A 无机粘合剂和水不溶性粉末材料，得到浆料B和将混合溶液A与浆料B混合的工序3，得到浆料C.通过该制造方法得到洁齿剂颗粒。 版权所有（C）2009，JPO＆INPIT

公开(公告)号：JP2009019194A

公开(公告)日：2009-01-29

申请号：JP2008131941

申请日：2008-05-20

Applicant: Kao Corp ,  花王株式会社

Inventor： HOSOYA SHINGO ,  SAKUMA YASUMITSU ,  MINE KOJI

IPC: C11D3/42 ,  A61K8/33 ,  A61K8/34 ,  A61K8/37 ,  A61Q5/02 ,  A61Q5/12 ,  A61Q19/10 ,  C11D1/14 ,  C11D1/52 ,  C11D1/68 ,  C11D1/72 ,  C11D3/20 ,  C11D11/00

Abstract: PROBLEM TO BE SOLVED: To provide a pearlescent composition having large turbidity, while maintaining strong pearlescence. SOLUTION: This pearlescent composition comprises fatty acid glycol ester and water, and further at least one kind of aliphatic compound selected from a group consisting of an aliphatic alcohol, fatty acid monoglyceride and aliphatic ether by 0.3-3 wt.%. The method for producing the pearlescent composition comprises a step of cooling a melt mixed liquid, comprising fatty acid glycol ester, water and at least one kind of aliphatic compound selected from a group consisting of an aliphatic alcohol, aliphatic acid monoglyceride and aliphatic ether, to a temperature lower than the melting point of the fatty acid glycol ester. COPYRIGHT: (C)2009,JPO&INPIT

Abstract translation: 待解决的问题：提供具有大浊度的珠光组合物，同时保持强烈的珠光。 解决方案：该珠光组合物包含脂肪酸乙二醇酯和水，还有至少一种选自脂肪醇，脂肪酸单甘油酯和脂族醚的脂族化合物的0.3-3重量％。 珠光组合物的制造方法包括：将包含脂肪酸乙二醇酯，水和选自脂肪族醇，脂肪酸单甘油酯和脂肪族醚的至少一种脂肪族化合物的熔融混合液冷却至 温度低于脂肪酸乙二醇酯的熔点。 版权所有（C）2009，JPO＆INPIT

公开(公告)号：JP2005270961A

公开(公告)日：2005-10-06

申请号：JP2005006268

申请日：2005-01-13

Applicant: Kao Corp ,  花王株式会社

Inventor： SAKUMA YASUMITSU ,  HORIBATA TATSUYA ,  MIYAKE TOSHIO

IPC: B01F3/08 ,  C11D3/04 ,  C11D11/00 ,  C11D17/08

Abstract: PROBLEM TO BE SOLVED: To provide a process for producing an emulsified material with a minute droplet diameter by which equipment load can be remarkably reduced in a process for producing an emulsion.
SOLUTION: The invention provides a process for producing the emulsion, including steps of continuously charging an aqueous solution (1) containing a water-soluble inorganic salt (a) and a mixture solution (2) containing a surfactant (b), a surfactant-emulsifying agent (c) and hydrophilic powder (d) into a mixer to obtain the emulsion in which the surfactant (b) is emulsified.
COPYRIGHT: (C)2006,JPO&NCIPI

Abstract translation: 要解决的问题：提供一种制造具有微小液滴直径的乳化材料的方法，在乳液的制备方法中可以显着降低设备负荷。 解决方案：本发明提供一种制备乳液的方法，包括连续加入含有水溶性无机盐（a）的水溶液（1）和含有表面活性剂（b）的混合溶液（2）的步骤， 表面活性剂 - 乳化剂（c）和亲水性粉末（d）混合到混合器中以获得其中表面活性剂（b）被乳化的乳液。 版权所有（C）2006，JPO＆NCIPI

公开(公告)号：JPH11315061A

公开(公告)日：1999-11-16

申请号：JP12246198

申请日：1998-05-01

Applicant: KAO CORP

Inventor： MIYOSHI KAZUHITO ,  SAKUMA YASUMITSU ,  YANAKA HIROO ,  KATAHATA YASUTAKA

IPC: C07B45/02 ,  C07C303/06

Abstract: PROBLEM TO BE SOLVED: To provide the production process for sulfates and the production apparatus that permit the efficient reaction of the starting compound with SO3 gas in the tubular reactor without contamination of individual parts of the production apparatus and can produce the sulfated product with improved operability. SOLUTION: In the sulfation reaction process in which the thin layer flow of a compound to be sulfated is brought into cocurrent contact with an SO3 gas, an inert gas is fed between the thin layer flow and the SO3 gas flow thereby feeding the starting compound to be sulfated from its staying part, as the starting material is overflowed from the staying part to the inner wall of the reactor tube. This production apparatus is equipped with the tubular reactor, the starting compound feeder, the SO3 gas feeder and the inert gas feeder and has a mechanism that starting compound feeder can feed the compound into the inner wall of the reactor by its overflowing.

公开(公告)号：JPH09227424A

公开(公告)日：1997-09-02

申请号：JP4087296

申请日：1996-02-28

Applicant: KAO CORP

Inventor： SAKUMA YASUMITSU ,  MIYOSHI KAZUHITO ,  TERASAKA MICHIO

IPC: B01J23/755 ,  C07B61/00 ,  C07C29/34 ,  C07C31/125

Abstract: PROBLEM TO BE SOLVED: To remarkably shorten filtering time and obtain a branched dimerized alcohol hardly containing a by-product such as soap in high yield by carrying out condensation reaction of an alcohol by combinedly using oxide consisting essentially of SiO2 . SOLUTION: (D) A primary alcohol (e.g. stearyl alcohol) of the formula (R1 and R2 are each H or a 1-24C alkyl) alone or mixed alcohol comprising two or more kinds of primary alcohols is subjected to heat condensation in the presence of (A) an alkaline substance (e.g. potassium hydroxide) or the component A and (B) a dehydrating catalyst (e.g. copper-nickel) and (C) an oxide consisting essentially of SO2 . Furthermore, a mineral oxide such as diatomaceous earth is especially used as the component C and the component C is preferably added in an amount of 0.001-1wt.% to the component D.

公开(公告)号：JP2009062305A

公开(公告)日：2009-03-26

申请号：JP2007230388

申请日：2007-09-05

Applicant: Kao Corp ,  花王株式会社

Inventor： HORIBATA TATSUYA ,  SAKUMA YASUMITSU ,  NORO HIROSHI

IPC: A61K8/33 ,  A61K8/23 ,  A61Q11/00

Abstract: PROBLEM TO BE SOLVED: To provide a method for producing dentifrice granules finely and stably containing a non-cationic microbicide. SOLUTION: The method for producing the dentifrice granules comprises a step 1 of obtaining a powder containing the non-cationic microbicide by dissolving the non-cationic microbicide in a 1-4C alcohol, and mixing a porous inorganic powder having 50-500 m 2 /g specific surface area therewith, a step 2 of obtaining slurry by mixing water, a water-insoluble inorganic binder, a water-insoluble powder material and the non-cationic microbicide-containing powder obtained at the step 1, and a step 3 of obtaining granules by drying the slurry obtained at the step 2. COPYRIGHT: (C)2009,JPO&INPIT

Abstract translation: 待解决的问题：提供一种精细且稳定地含有非阳离子杀微生物剂的洁齿剂颗粒的制备方法。 解决方案：制备洁齿剂颗粒的方法包括步骤1，通过将非阳离子杀微生物剂溶解在1-4℃的醇中获得含有非阳离子杀微生物剂的粉末，并混合具有50-500的多孔无机粉末 m 2 / SP / g比表面积;步骤2，通过混合水，水不溶性无机粘合剂，水不溶性粉末材料和非阳离子杀微生物剂粉末获得浆料， 步骤1和通过干燥步骤2获得的浆料获得颗粒的步骤3。版权所有：（C）2009，JPO＆INPIT

公开(公告)号：JP2009051831A

公开(公告)日：2009-03-12

申请号：JP2008198281

申请日：2008-07-31

Applicant: Kao Corp ,  花王株式会社

Inventor： UMEHARA MASAHIRO ,  SAKUMA YASUMITSU ,  HORIBATA TATSUYA ,  INOMATA YUKIO

IPC: A61K8/27 ,  A61K8/19 ,  A61K8/29 ,  A61K8/34 ,  A61K8/89 ,  A61Q17/04

Abstract: PROBLEM TO BE SOLVED: To provide an ultraviolet shielding inorganic particle dispersion containing at high concentration, inorganic particles having ultraviolet shielding ability, low in viscosity of the dispersion, and excellent in dispersion stability of the inorganic particle having ultraviolet shielding ability, to provide a production method of the dispersion, and to provide ultraviolet shielding cosmetics containing the dispersion.
SOLUTION: The ultraviolet shielding inorganic particle dispersion contains a 1-4C lower alcohol and a silicone oil, wherein inorganic particles and a polymer dispersant are dispersed in a solvent containing the lower alcohol of 10-80 wt.% which inorganic particles are covered with an organic substance and have ≤0.1 μm primary average particle diameter and ultraviolet shielding ability, and the concentration of the inorganic particles is 7.5-18 vol.%, and wherein the secondary volume-average particle diameter of the inorganic particle after being dispersed is ≤0.2 μm and the dispersion weight average particle diameter of the polymer dispersant is 0.01-0.7 time of the average distance between inorganic particles, and a production method of the dispersion is provided. And the ultraviolet shielding cosmetics containing the dispersion is provided.
COPYRIGHT: (C)2009,JPO&INPIT

Abstract translation: 解决问题的方案：为了提供高浓度的紫外线屏蔽无机粒子分散体，具有紫外线屏蔽性，分散性粘度低，无机粒子具有紫外线屏蔽能力的分散稳定性优异的无机粒子， 提供分散体的制备方法，并提供含有该分散体的紫外线屏蔽化妆品。 解决方案：紫外线屏蔽无机颗粒分散体含有1-4C低级醇和硅油，其中无机颗粒和聚合物分散剂分散在含有10-80重量％的低级醇的溶剂中，该无机颗粒是 覆盖有机物质，一次平均粒径≤0.1μm，紫外线屏蔽能力，无机粒子的浓度为7.5〜18vol。％，分散后的无机粒子的二次体积平均粒径 ≤0.2μm，聚合物分散剂的分散重量平均粒径为无机粒子间平均距离的0.01-0.7倍，提供了分散液的制造方法。 并提供含有分散体的紫外线屏蔽化妆品。 版权所有（C）2009，JPO＆INPIT

公开(公告)号：JP2008255110A

公开(公告)日：2008-10-23

申请号：JP2008063020

申请日：2008-03-12

Applicant: Kao Corp ,  花王株式会社

Inventor： HOSOYA SHINGO ,  SAKUMA YASUMITSU ,  NAKAI TAKESHI ,  MINE KOJI

IPC: A61K8/37 ,  A61K8/39 ,  A61K8/42 ,  A61K8/46 ,  A61Q5/02

Abstract: PROBLEM TO BE SOLVED: To provide a pearl gloss composition which maintains strong pearl gloss and is simultaneously large in turbidity. SOLUTION: Provided are a pearl gloss composition comprising a fatty acid glycol ester, an alkyl sulfate salt, a polyoxyalkylene type nonionic surfactant and water, characterized by further containing 0.3 to 3 wt.% of a fatty acid, and a method for producing the same. COPYRIGHT: (C)2009,JPO&INPIT

Abstract translation: 要解决的问题：提供一种保持强烈的珍珠光泽并同时具有大浊度的珍珠光泽组合物。 解决方案：提供包含脂肪酸二醇酯，烷基硫酸盐，聚氧化烯型非离子表面活性剂和水的珍珠光泽组合物，其特征在于还含有0.3至3重量％的脂肪酸​​，以及用于 生产相同。 版权所有（C）2009，JPO＆INPIT

公开(公告)号：JP2007161708A

公开(公告)日：2007-06-28

申请号：JP2006312700

申请日：2006-11-20

Applicant: Kao Corp ,  花王株式会社

Inventor： INOMATA YUKIO ,  KAMISAKA TOSHIO ,  SUGAWARA SATOSHI ,  SAKUMA YASUMITSU ,  UMEHARA MASAHIRO

IPC: A61K8/894 ,  A61K8/06 ,  A61K8/19 ,  A61K8/27 ,  A61K8/29 ,  A61K8/34 ,  A61K8/37 ,  A61K8/42 ,  A61K8/73 ,  A61K8/81 ,  A61K8/89 ,  A61K8/891

Abstract: PROBLEM TO BE SOLVED: To provide an O/W emulsified cosmetic containing stably ultraviolet-blocking powder of high specific gravity even if being low in viscosity, and giving fresh and refreshing touch feeling.
SOLUTION: The O/W emulsified cosmetic comprises (A) a nonionic or cationic polymer composed of hydrophobic monomer units and hydrophilic monomer units, wherein the content of the hydrophilic groups is 40-80 mass%, (B) a dispersion comprising (a) powder having ultraviolet-blocking ability with the surface being hydrophobicized, (b) a polymer composed of hydrophobic monomer units and hydrophilic monomer units, (c) a silicone oil and (d) a 1-3C alcohol in the mass ratio (a):(b):(c):(d)=(25-65):(0.1-5):(10-50):(10-50) and (C) water.
COPYRIGHT: (C)2007,JPO&INPIT

Abstract translation: 待解决的问题：即使粘度低，也提供含有稳定的高比重的稳定的紫外线阻隔粉末的O / W乳化化妆品，并且具有清新和清爽的触感。 解决方案：O / W乳化化妆品包含（A）由疏水单体单元和亲水性单体单元组成的非离子或阳离子聚合物，其中亲水基团的含量为40-80质量％，（B）包含 （a）具有紫外线阻断能力的表面被疏水化的粉末，（b）由疏水性单体单元和亲水性单体单元构成的聚合物，（c）硅油和（d）质量比为1〜 a）:( b）:( c）:( d）=（25-65）：（0.1-5）:( 10-50）:( 10-50）和（C）水。 版权所有（C）2007，JPO＆INPIT