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公开(公告)号：KR100888467B1
公开(公告)日：2009-03-12
申请号：KR1020070118880
申请日：2007-11-21
Applicant: 한국화학연구원
CPC classification number: B01J29/85 , B01J29/40 , B01J37/036 , B01J37/08 , C10G11/00
Abstract: A method for preparing a composite catalyst for a light olefin obtained from an oxygenated compound is provided to control a selectivity ratio of propylene/ethylene so as to control a composition ratio of a reaction product. A method for preparing a composite catalyst for a light olefin obtained from an oxygenated compound comprises the following steps. A ZSM-5 basic solution is prepared by mixing ZSM-5 and alkaline solution. An alumina basic solution for SAPO-34 is prepared by mixing an alumina precursor and a tetraethyl ammonium hydroxide. An aluminium phosphate solution for SAPO-34 is prepared by mixing the alumina basic solution, phosphoric acid, and water.
Abstract translation: 提供了制备由含氧化合物得到的轻质烯烃复合催化剂的方法，以控制丙烯/乙烯的选择比，从而控制反应产物的组成比。 制备由含氧化合物得到的轻质烯烃复合催化剂的方法包括以下步骤。 通过混合ZSM-5和碱性溶液制备ZSM-5碱性溶液。 通过混合氧化铝前体和四乙基氢氧化铵来制备SAPO-34的氧化铝碱性溶液。 通过混合氧化铝碱性溶液，磷酸和水，制备SAPO-34的磷酸铝溶液。
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公开(公告)号：KR100881279B1
公开(公告)日：2009-02-03
申请号：KR1020080068404
申请日：2008-07-15
Abstract: A high purity refining method of acetone is provided to refine acetone containing organic impurity and inorganic metallic impurity through an ion exchange resin tower and a batch type distillation tower containing zeolite 4A. A high purity refining method of acetone comprises (1) a step for obtaining refined acetone by injecting the collected acetone containing organic impurity, inorganic metallic impurity and moisture to the top of a tower having ion-exchange resin at a flow rate of 10~100 cc /minute . g (the flow rate of the collected acetone per the ion-exchange resin gram); and (2) a step for obtaining acetone by injecting the first refined acetone in a batch type distillation tower continuously and distilling it at a distillation temperature of 60~80 °C with the reflux ratio of 2~6. The batch type distillation tower contains 1~5 % of zeolite 4A based on the weight of the collected acetone.
Abstract translation: 提供丙酮的高纯度精制方法，通过离子交换树脂塔和含沸石4A的间歇式蒸馏塔来提炼含丙酮的有机杂质和无机金属杂质。 丙酮的高纯度精炼方法包括：（1）通过将收集到的含丙酮的有机杂质，无机金属杂质和水分注入到具有离子交换树脂的塔顶部以10〜100的流速获得精制丙酮的步骤 cc /分钟。 g（离子交换树脂克收集的丙酮的流量）; 和（2）通过在间歇式蒸馏塔中连续注入第一精制丙酮并在60〜80℃的蒸馏温度下以2〜6的回流比蒸馏得到丙酮的步骤。 基于收集的丙酮的重量，间歇式蒸馏塔含有1〜5％的沸石4A。
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公开(公告)号：KR1020170127085A
公开(公告)日：2017-11-21
申请号：KR1020160056888
申请日：2016-05-10
Applicant: 한국화학연구원
IPC: B01J23/44 , B01J23/40 , B01J23/755 , B01J32/00 , B01J37/02 , B01J37/16 , B01J37/12 , C07C1/207 , C07C7/20 , C07C9/22
CPC classification number: B01J23/44 , B01J23/40 , B01J23/755 , B01J32/00 , B01J37/0201 , B01J37/12 , B01J37/16 , C07C1/207 , C07C7/20 , C07C9/22
Abstract: 본발명은 3 차원구조의규칙적인메조다공성탄소(Ordered Mesoporous Carbon, OMC) 담체에촉매활성금속이담지된지방산으로부터탈산소화화합물제조용촉매를제공한다. 본발명에따른 3 차원구조의메조다공성탄소담체(Ordered Mesoporous Carbon, OMC)에촉매활성금속이담지된촉매이되, 상기담체의구조는 3 차원막대형또는 3 차원튜브형인지방산으로부터탈산소화합물제조용촉매를제공함으로써, 기존의촉매에비하여촉매활성이높아선택도와생성속도를향상시킬수 있을뿐만아니라촉매안정성이높아촉매수명을크게증가시키는장점이있다. 또한, 본발명에따른지방산으로부터탈산소화화합물제조용촉매의제조방법은 3 차원적인메조세공구조를유지하는표면산화법을사용하여촉매활성금속이담지된 3 차원구조의메조세공촉매를제조할수 있다.
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Patent Agency Ranking
公开(公告)号：KR101732121B1
公开(公告)日：2017-05-08
申请号：KR1020100029421
申请日：2010-03-31
Applicant: 한국화학연구원 , 동양하이테크산업주식회사
Abstract: 본발명은백금, 레늄, 및로듐으로이루어진군에서선택된 2 종이상의복합금속이메조다공성탄소로이루어진담체에담지된수상개질반응의촉매에관한것이다. 수상개질반응시안정적인담체로서, 균일한기공을갖는메조다공성탄소물질을사용하며, 또한단독금속이아닌복합금속을사용하여수상개질반응내에서수소의전환율및 생성속도를크게향상시킨것에본 기술의특징이있다.
Abstract translation: 本发明涉及一种用于水重整反应的催化剂，其中将由铂，铼和铑组成的组中选择的两种或更多种复合金属负载在由介孔碳制成的载体上。 如在水的重整反应，在本领域中，以使用具有均匀的细孔与复合金属的中孔碳材料，和鞋底金属极大地提高了转化率和氢的在内部水相中的生产速率重整，不能稳定的支撑 它的特点。
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公开(公告)号：KR101652467B1
公开(公告)日：2016-09-01
申请号：KR1020100029422
申请日：2010-03-31
Applicant: 한국화학연구원 , 동양하이테크산업주식회사
Abstract: 본발명은메조세공체알루미나를담체로하여백금을담지한수상개질반응의촉매및 그의제조방법에관한것이다. 또한본 발명은상기촉매를활용하여수상개질반응에서수소의수율과반응속도를향상시키는방법에관한발명이다. 본발명의촉매는구조적으로안정하면서도, 수소의수율이높고, 반응속도가빠르게증가하므로, 본촉매를활용하여바이오매스의수상개질반응을실행할시 수소의생성속도및 수소의수율등 반응의효율이높아는효과가있어친환경녹색성장기술이다.
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58.发明授权다환 방향족 탄화수소로부터 벤젠, 톨루엔, 에틸벤젠, 자일렌의 혼합물과 중간 유분을 제조하는 선택적 개환 반응을 위한 제올라이트 촉매 및 이의 제조방법 有权用于合成苯甲苯乙苯二甲苯BTEX和中间馏分与聚芳烃的混合物的沸石催化剂及其制备方法
公开(公告)号：KR101621307B1
公开(公告)日：2016-05-17
申请号：KR1020140119230
申请日：2014-09-05
Applicant: 한국화학연구원
IPC: B01J29/076 , B01J37/02 , B01J37/20 , C07C15/02
Abstract: 본발명은적어도 1종의 VIB족금속이함침된 beta 제올라이트로써,SiO/Al2O의몰비는 35 내지 70이고, 다환방향족탄화수소로부터 BTEX(Benzene(벤젠), Toluene(톨루엔), ethylbenzene(에틸벤젠), Xylene(자일렌)) 및중간유분으로전환을위한 Beta 제올라이트촉매를제공한다. 또한본 발명은 SiO/Al2O의몰비가 35 내지 70인 beta 제올라이트를제조하는단계 (단계 1); 상기단계 1에서제조된제올라이트에 VIB족금속을담지하는단계 (단계 2)을포함하는 beta 제올라이트촉매의제조방법을제공한다. 더나아가본 발명에따른 Beta 제올라이트촉매를이용하여, 다환방향족탄화수소의선택적개환반응을통해중간유분및 BTEX (벤젠, 톨루엔, 에틸벤젠및 자일렌)을제조하는단계;를포함하는다환방향족탄화수소의 BTEX 제조방법을제공한다. 또한상기제조방법을통해방향족탄화수소로부터전환된 BTEX를제공한다.
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公开(公告)号：KR101578469B1
公开(公告)日：2015-12-17
申请号：KR1020140056798
申请日：2014-05-12
Applicant: 한국화학연구원
IPC: B01J29/06 , B01J29/068 , B01J29/74 , B01J37/08
Abstract: 본발명은제올라이트분말, 매트릭스, 바인더및 산용액을포함하는혼합슬러리를분무건조시키고소성하여제조한미소구형담체에, 아연또는/및란탄이소정량함친된제올라이트계성형촉매및 이의제조방법에관한것이다. 구체적으로, 본발명의제1 성형촉매제조방법은 (ⅰ) (a) MFI 구조타입제올라이트분말, (b) 매트릭스, (c) 바인더및 (d) 산용액을포함하는혼합슬러리를분무건조시키고소성하여미소구형담체를제조하는단계; 및 (ⅱ) 상기미소구형담체에 (e) 아연, 또는아연및 란탄을포함하는금속을함침하고건조시킨후 소성하여미소구형의제올라이트계성형촉매를제조하는단계;를포함한다. 또한본 발명의제2 성형촉매제조방법은 (a) MFI 구조타입제올라이트분말, (b) 매트릭스, (c) 바인더, (d) 산용액, 및 (e) 아연또는아연및 란탄을포함하는금속을포함하는혼합슬러리를분무건조시키고소성하여미소구형의제올라이트계성형촉매를제조하는단계;를포함한다.
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公开(公告)号：KR101364691B1
公开(公告)日：2014-02-27
申请号：KR1020120156969
申请日：2012-12-28
Abstract: Disclosed is a high-pressure reaction apparatus. The disclosed high-pressure reaction apparatus comprises a first reactant compositional factor accommodation part for accommodating a first reactant compositional factor formed of one among solid, gaseous and liquid phases; a first reactant compositional factor transfer pump for transferring the first reactant compositional factor of the first reactant compositional factor accommodation part by pumping the first reactant compositional factor with high pressure; a second reactant compositional factor accommodation part for accommodating a second reactant compositional factor in a liquid phase; a second reactant compositional factor transfer pump for transferring the second reactant compositional factor of the second reactant compositional factor accommodation part by pumping the second reactant compositional factor with high pressure; and a high-pressure reactor for introducing, with pressure, the first reactant compositional factor and the second reactant compositional factor being transferred by the first and second reactant compositional factor transfer pumps together and compressing the introduced first and second reactant compositional factors with high pressure while mixing the introduced first and second reactant compositional factors.
Abstract translation: 公开了一种高压反应装置。 所公开的高压反应装置包括用于容纳由固相，气相和液相之一形成的第一反应物组成因子的第一反应物组成因子容纳部分; 第一反应物组分因子转移泵，用于通过以高压泵送第一反应物组成因子来转移第一反应物组分因子调节部分的第一反应物组成因子; 第二反应物组分因子调节部分，用于容纳液相中的第二反应物组分因子; 第二反应物组分因子转移泵，用于通过以高压泵送第二反应物组分因子来转移第二反应物组分因子调节部分的第二反应物组成因子; 以及高压反应器，用于将第一和第二反应物组分因子转移泵一起转移的第一反应物组成因子和第二反应物组成因子加压引入，并以高压压缩引入的第一和第二反应物组成因子，同时 混合引入的第一和第二反应物组成因子。
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