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    53.
    发明专利
    未知

    公开(公告)号：NO994914D0

    公开(公告)日：1999-10-08

    申请号：NO994914

    申请日：1999-10-08

    Applicant: CONOCO INC

    Inventor： ZIMMERMANN ANDREA K ,  RODGERS JOHN A ,  ROMINE H ERNEST ,  MCCONAGHY JAMES R ,  DAVIS LORITA

    IPC: C10C3/00 ,  C10C3/04 ,  D01F9/145 ,  D01F11/10 ,  D01F11/16 ,  C10G

    Abstract: The present invention provides a process for thermosetting pitch fibers in reduced times, at low concentrations of oxygen and at higher temperatures than previously possible. Additionally, the present invention provides a pitch fiber which has an oxygen diffusion rate to the center of the fiber which is competitive with the rate of oxidation at the fiber's surface. Further, the present invention provides a high density pitch fiber batt which thermosets without loss of fiber structure.

    54.
    发明专利
    未知

    公开(公告)号：BR9609163A

    公开(公告)日：1999-05-18

    申请号：BR9609163

    申请日：1996-12-05

    Applicant: CONOCO INC

    Inventor： RODGERS JOHN A ,  ROSSILLON DANIEL F ,  ROSS RODGER A

    IPC: D01F9/14 ,  C01B31/00 ,  D01D4/02 ,  D01F9/12 ,  D01F9/133 ,  D01F9/145

    Abstract: The present invention provides a blow spinning die particularly suited for spinning solvated pitch into fibers having a random cross-sectional structure. Additionally, the present invention provides a process for blow spinning fibers from solvated pitches. The present invention also provides pitch fibers having a high energy internal molecular structure. Finally, the present invention provides carbon fibers which have a non-radial internal structure.

    Organometallic containing mesophase pitches for spinning into pitch carbon fibres
    56.
    发明专利
    Organometallic containing mesophase pitches for spinning into pitch carbon fibres 未知

    公开(公告)号：GB2319780A

    公开(公告)日：1998-06-03

    申请号：GB9126474

    申请日：1991-12-13

    Applicant: CONOCO INC

    Inventor： ROMINE HUGH E ,  MCCONAGHY JAMES RICHARD ,  RODGERS JOHN A

    IPC: C10C3/02 ,  C10C3/08 ,  C10C3/10 ,  D01F9/145 ,  C08L95/00

    Abstract: A metals containing anisotropic pitch suitable for carbon fiber manufacture is produced by adding a soluble aromatic-organometallic compound to a carbonaceous feedstock which is substantially free of mesophase pitch and the resulting composition is heat soaked to produce an isotropic pitch product containing mesogens and soluble, aromatic-organometallic compounds. The pitch product is solvent fractionated to separate mesogens which contain metals from the organometallic compounds and is then heat-treated. In another method, the carbonaceous feedstock is heat soaked to produce an isotropic pitch product containing mesogens and the organometallic compounds are added to the mesogen containing isotropic pitch product prior to solvent fractionation. Alternatively, the solvent fractionation or separation is conducted under supercritical extraction conditions to produce a metals-containing mesophase pitch. Organometallic compounds may be added to the carbonaceous feedstock either prior to or after the heat soak step. The organometallic compound is preferably macrocyclic and most preferably porphyrin derived.

    57.
    发明专利
    未知

    公开(公告)号：NO975697D0

    公开(公告)日：1997-12-05

    申请号：NO975697

    申请日：1997-12-05

    Applicant: CONOCO INC

    Inventor： RODGERS JOHN A ,  ROSSILLON DANIEL F ,  ROSS ROGER A

    IPC: D01F9/14 ,  C01B31/00 ,  D01D4/02 ,  D01F9/12 ,  D01F9/133 ,  D01F9/145 ,  D01F

    Abstract: The present invention provides a blow spinning die particularly suited for spinning solvated pitch into fibers having a random cross-sectional structure. Additionally, the present invention provides a process for blow spinning fibers from solvated pitches. The present invention also provides pitch fibers having a high energy internal molecular structure. Finally, the present invention provides carbon fibers which have a non-radial internal structure.

    Solvating component and solvent system for mesophase pitch
    60.
    发明专利
    Solvating component and solvent system for mesophase pitch 未知

    公开(公告)号：SK442003A3

    公开(公告)日：2003-09-11

    申请号：SK442003

    申请日：2001-06-07

    Applicant: CONOCO INC

    Inventor： ROMINE H ERNEST ,  RODGERS JOHN A ,  SOUTHARD W MARK ,  NANNI EDWARD J

    IPC: C10C3/02 ,  C10C3/00 ,  C10C3/08 ,  C10G9/00 ,  C10G21/00 ,  D01F9/145 ,  C08L95/00

    Abstract: A solvating component for a solvated mesophase pitch. The solvated component includes a mixture of aromatic hydrocarbons having boiling points in the atmospheric equivalent boiling point range of about 285° to about 500° C. (about 550° F.-932° F.). At least 80% of the carbon atoms of the hydrocarbons are aromatic as characterized by carbon 13 NMR. The aromatic hydrocarbons are selected from a group consisting of aromatic compounds having 2 to 5 aromatic rings, substituted aromatic compounds having 2 to 5 aromatic rings wherein said substituents are alkyl groups having 1 to 3 carbons, hydroaromatic compounds having 2 to 5 rings, substituted aromatic compounds having 2 to 5 rings wherein said substituents are alkyl groups having 1 to 3 carbons, and mixtures thereof.

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