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公开(公告)号:CA2202525A1
公开(公告)日:1996-05-17
申请号:CA2202525
申请日:1995-10-20
Applicant: CONOCO INC
Inventor: ROMINE H ERNEST , SOUTHARD W MARK , CAREL MARK W , NANNI EDWARD J
Abstract: The present invention provides a process for obtaining a very clean mesophase pitch from isotropic pitch. This invention utilizes a solvent fractionation process which does not involve the process steps, yield loss and waste generation associated with fluxing and filtering the isotropic pitch. Additionally, this invention provides a liquid/liquid extraction process that avoids the solids handling and the high temperatures and pressures of supercritical fluid extraction. Finally, this invention controls the hardness of the mesophase product.
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公开(公告)号:NO932257L
公开(公告)日:1993-06-18
申请号:NO932257
申请日:1993-06-18
Applicant: CONOCO INC
Inventor: KALBACK WALTER M , ROMINE H ERNEST , BOURRAT XAVIER M
Abstract: This invention relates to low melting solvated mesophase pitches which are suitable for spinning into carbon fibers. The solvated mesophase pitches have a lower melting point than conventional mesophase pitch but remain substantially anisotropic. The solvated mesophase can be produced as an intermediate during solvent fractionation or supercritical solvent fractionation of mesogen-containing isotropic pitches. The process is enhanced through the ability to recover pseudomesogens with an increased average molecular weight which, in combination with the solvent content, provides a fusible mesophase capable of being spun directly into infusible oriented anisotropic carbon fibers.
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公开(公告)号:FI932772A
公开(公告)日:1993-06-16
申请号:FI932772
申请日:1993-06-16
Applicant: CONOCO INC
Inventor: KALBACK WALTER M , ROMINE H ERNEST , BOURRAT XAVIER M
Abstract: This invention relates to low melting solvated mesophase pitches which are suitable for spinning into carbon fibers. The solvated mesophase pitches have a lower melting point than conventional mesophase pitch but remain substantially anisotropic. The solvated mesophase can be produced as an intermediate during solvent fractionation or supercritical solvent fractionation of mesogen-containing isotropic pitches. The process is enhanced through the ability to recover pseudomesogens with an increased average molecular weight which, in combination with the solvent content, provides a fusible mesophase capable of being spun directly into infusible oriented anisotropic carbon fibers.
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54.
公开(公告)号:CA2055155A1
公开(公告)日:1993-05-08
申请号:CA2055155
申请日:1991-11-07
Applicant: CONOCO INC
Inventor: ROMINE H ERNEST
Abstract: An improved process is disclosed for producing a metals containing anisotropic pitch product suitable for carbon fiber manufacture. Soluble-aromatic, organometallic compounds are added to a carbonaceous feedstock substantially free of mesophase pitch and the resulting composition is heat soaked preferably with gas sparge to produce a metals containing mesophase pitch.
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公开(公告)号:ES2185718T3
公开(公告)日:2003-05-01
申请号:ES95936316
申请日:1995-10-20
Applicant: CONOCO INC
Inventor: ROMINE H ERNEST , SOUTHARD W MARK , CAREL MARK W , NANNI EDWARD J
Abstract: The present invention provides a process for obtaining a very clean mesophase pitch from isotropic pitch. This invention utilizes a solvent fractionation process which does not involve the process steps, yield loss and waste generation associated with fluxing and filtering the isotropic pitch. Additionally, this invention provides a liquid/liquid extraction process that avoids the solids handling and the high temperatures and pressures of supercritical fluid extraction. Finally, this invention controls the hardness of the mesophase product.
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56.
公开(公告)号:CA2055155C
公开(公告)日:2002-09-17
申请号:CA2055155
申请日:1991-11-07
Applicant: CONOCO INC
Inventor: ROMINE H ERNEST
Abstract: An improved process is disclosed for producing a metals containing anisotropic pitch product suitable for carbon fiber manufacture. Soluble-aromatic, organometallic compounds are added to a carbonaceous feedstock substantially free of mesophase pitch and the resulting composition is heat soaked preferably with gas sparge to produce a metals containing mesophase pitch.
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公开(公告)号:DE69132940D1
公开(公告)日:2002-04-04
申请号:DE69132940
申请日:1991-12-05
Applicant: CONOCO INC
Inventor: KALBACK M , ROMINE H ERNEST , BOURRAT M
Abstract: This invention relates to low melting solvated mesophase pitches which are suitable for spinning into carbon fibers. The solvated mesophase pitches have a lower melting point than conventional mesophase pitch but remain substantially anisotropic. The solvated mesophase can be produced as an intermediate during solvent fractionation or supercritical solvent fractionation of mesogen-containing isotropic pitches. The process is enhanced through the ability to recover pseudomesogens with an increased average molecular weight which, in combination with the solvent content, provides a fusible mesophase capable of being spun directly into infusible oriented anisotropic carbon fibers.
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公开(公告)号:DE69518836T2
公开(公告)日:2001-01-11
申请号:DE69518836
申请日:1995-07-31
Applicant: CONOCO INC
Inventor: SOUTHARD W MARK , ROMINE H ERNEST , NANNI EDWARD J , CAREL MARK W
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公开(公告)号:AU721796B2
公开(公告)日:2000-07-13
申请号:AU1129099
申请日:1999-01-12
Applicant: CONOCO INC
Inventor: KALBACK WALTER M , ROMINE H ERNEST , BOURRAT XAVIER M
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公开(公告)号:NO994914A
公开(公告)日:1999-10-08
申请号:NO994914
申请日:1999-10-08
Applicant: CONOCO INC
Inventor: ZIMMERMANN ANDREA K , RODGERS JOHN A , ROMINE H ERNEST , MCCONAGHY JAMES R , DAVIS LORITA
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