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    The production of durable creases in keratinic fibre-containing textile materials
    52.
    发明专利
    The production of durable creases in keratinic fibre-containing textile materials 未知

    公开(公告)号：GB1101628A

    公开(公告)日：1968-01-31

    申请号：GB773266

    申请日：1966-02-22

    Applicant: OREAL

    Inventor： ZVIAK CHARLES ,  VIOUT ANDRE

    IPC: A61K8/81 ,  A61Q5/04 ,  A61Q5/06 ,  C08F8/00 ,  C08F8/34 ,  D06M15/273 ,  D06M15/285 ,  D06P1/52

    Abstract: A composition suitable for treating keratinous fibre fabrics comprises a solution of a polysulph-hydryl polymer which is a polymer in which the backbone consists of saturated carbon atoms or saturated carbon atoms and oxygen, nitrogen or sulphur atoms which contains one or, at more or less regular intervals, more -SH radicals either joined directly to the polymer chain or via intermediate groupings, e.g. amide and ester groupings. The solution may contain 1-20% by weight of the polysulph-hydryl polymer and may be adjusted to a pH of 3.5-10 by, for example, the addition of ammonia or monoethanolamine. Specified polymers are those obtained by the reaction of b -mercapto ethylamine with a styrene/maleic anhydride copolymer or maleic anhydride/ethylene copolymer, by the reaction of N-(b -aminoethyl)thioglycolamide with an ethylene/maleic anhydride copolymer, by the reaction of b -mercaptoethylamine and N,N-diethylpropylene diamine with an ethylene/maleic anhydride copolymer, by the reaction of b -mercaptoethylamine and n-butylamine with a vinyl acetate/maleic anhydride copolymer, by the reaction of b -mercaptoethylamine or N(b -aminoethyl)-thioglycolamide with a vinyl acetate/maleic anhydride copolymer or by the reaction of b -mercaptoethylamine alone or in admixture with butylamine with poly-(maleic anhydride). The composition may be in the form of an aerosol composition the propellant being dichlorodifluoromethane, trichloromonofluoromethane or butane, and optionally containing an anti-foam silicone, a fatty alcohol polyethyoxyether or alkyl phenol polyethoxyether, or may be applied by means of a rotating ball liquid dispenser bottle.ALSO:An aerosol composition suitable for treating keratinous fibre fabrics comprises a solution of a polysulph-hydryl polymer which is a polymer in which the backbone consists of saturated carbon atoms or saturated carbon atoms and oxygen, nitrogen or sulphur atoms which contains one or, at more or less regular intervals, more -SH radicals either joined directly to the polymer chain or via intermediate groupings, e.g. amide and ester groupings. The solution may contain 1-20% by weight of the polysulph-hydryl polymer and may be adjusted to a pH of 3.5-10 by, for example, the addition of ammonia or monoethanolamine. The propellent may be dichlorodifluoromethane, trichloromonofluoro-methane or butane and the composition may optionally contain an anti-foam silicone, a fatty alcohol polyethoxyether or alkyl phenolpolyethoxyether, specified polymers are those obtained by the reaction of b -mercapto ethylamine with a styrene/maleic anhydride copolymer or maleic anhydride/ethylene copolymer, by the reaction of N-(b -aminoethyl) thioglycolamide with an ethylene/maleic anhydride copolymer, by the reaction of b -mercaptoethylamine and N,N-diethylpropylene diamine with an ethylene/maleic anhydride copolymer, by the reaction of b -mercaptoethylamine and n-butylamine with a vinyl acetate/maleic anhydride copolymer, by the reaction of b -mercaptoethylamine or N-(b -aminoethyl)-thioglycolamide with a vinyl acetate/maleic anhydride copolymer or by the reaction of b -mercaptoethylamine alone or in admixture with butylamine with poly (maleic anhydride).ALSO:Durable creases are imparted to fabrics comprising keratinic fibres, e.g. wool, alpaca, camel hair or mohair, by treating them with a solution of a polysulph-hydryl polymer at the location where it is desired to form the crease and forming the crease by applying heat and pressure, e.g. by means of a hot iron or clothes press, to the impregnated fabric while it is arranged in the form of a crease. The polysulph-hydryl polymer is a polymer in which the backbone consists of saturated carbon atoms or saturated carbon atoms and oxygen, nitrogen or sulphur atoms which contains one or, at more or less regular intervals, more -SH radicals either joined directly to the polymer chain or via intermediate groupings, e.g. amide and ester groupings. An aqueous solution containing 1-20% by weight of the polysulph - hydryl polymer and having a pH of 3.5-10 adjusted by, for example, the addition of ammonia or monoethanol amine may be used. Polysulph-hydryl polymers obtained by the reaction of b -mercapto ethylamine with a styrene/maleic anhydride copolymer or maleic anhydride/ethylene copolymer, by the reaction of N-(b -aminoethyl) thioglycolamide with an ethylene/maleic anyhydride copolymer by the reaction of b -mercapto ethylamine and N,N-diethylpropylene diamine with an ethylene/maleic anhydride copolymer, by the reaction of b -mercapto ethylamine and n-butylamine with a vinyl acetate/maleic anhydride copolymer by the reaction of b -mercaptoethylamine or N-(b -aminoethyl)-thioglycolamide with a vinyl acetate/maleic anhydride copolymer or by the reaction of b -mercaptoethylamine alone or in admixture with butylamine with poly(maleic anhydride) are examples of numerous suitable polymers indicated. The treating composition may be used in the form of an aerosol composition, the propellent being dichlorodifluoromethane, trichloromonofluoromethane or butane, and optionally containing an anti-foam silicone, a fatty alcohol polyethoxyether or alkylphenol polyethoxyether, or may be applied by means of a rotating ball liquid dispenser bottle. The fabric may be a woven or knitted fabric, lace or felt.

    Improvements in or relating to the treatment of keratinic fibres
    53.
    发明专利
    Improvements in or relating to the treatment of keratinic fibres 未知

    公开(公告)号：GB1067065A

    公开(公告)日：1967-05-03

    申请号：GB1588364

    申请日：1964-04-16

    Applicant: OREAL

    Inventor： KALOPISSIS GREGOIRE ,  VIOUT ANDRE

    IPC: A45D7/06 ,  A61K8/46 ,  A61K8/81 ,  A61Q5/04 ,  C08F8/34 ,  D06M15/273

    Abstract: A composition for treating keratinic fibres comprises an aqueous solution of a polymer containing thiol groups and of an organic disulphide. Preferably the polymer containing thiol groups has the general formula in which R is an alkylene radical, preferably of 2 to 4 carbon atoms, which may be unsubstituted or substituted by alkyl of 1 to 4 carbon atoms, carboxyl or carbalkoxy; R1 is hydrogen or alkyl of 1 to 4 carbon atoms; R11 and R111, which may be the same or different, each represents hydrogen, alkyl of 1 to 4 carbon atoms, phenyl or alkoxy of 1 to 4 carbon atoms; and n is an integer greater than 1 and less than 25 obtained by the process described in Specification 1,002,455. The disulphide is of the formula R1SSR2 in which R1 and R2 which may be the same or different, each represents an alkyl radical of 1 to 4 carbon atoms having a water-solubilizing substituent. The composition may also contain ammonia or an organic amine.ALSO:A method of treating keratine fibres comprises (a) applying to the fibres an aqueous solution of a polymer containing thiol groups and of an organic disulphide, said polymer and said disulphide being such that they are capable of reacting together under the conditions of use, to reduce said disulphide to the corresponding mocaptan and to oxidise said polymer to the corresponding polysulphide; (b) shaping the keratinic fibres after reduction of their disulphide linkages by said mercaptan is substantially complete; (c) allowing said reduced linkages to oxidise to the disulphide form. The polymer is preferably that described in Specification 1,002,455 (see Division C3). The solution is preferably applied at a pH of from 8.5 to 9.5. Hair is permanently waved to applying the solution to the locks of the hair, winding the locks of hair on rollers, again impregnating the locks with the solution, leaving the air rolled while the solution reacts, removing the hair from the rollers, and rinsing and drying the hair. The rollers in which the hair is wound are preferably heated. The solution may also contain swelling and penetrating agents.

    Magnesium salts of succinic esters and emulsions containing the same
    54.
    发明专利
    Magnesium salts of succinic esters and emulsions containing the same 未知

    公开(公告)号：GB1066758A

    公开(公告)日：1967-04-26

    申请号：GB4226765

    申请日：1965-10-05

    Applicant: OREAL

    Inventor： LACHAMPT FELIX ,  VIOUT ANDRE ,  VANLERBERGHE GUY

    IPC: A61K8/06 ,  A61K8/39 ,  A61Q1/02 ,  A61Q1/08 ,  A61Q3/00 ,  A61Q5/06 ,  A61Q19/00 ,  C09K23/00

    Abstract: The magnesium salt of a succinic ester of formula in which m is 12 or greater, preferably 12-18, n and p are each from 0 to 12 inclusive, the sum of n and p being from 2 to 12 inclusive, which is prepared by reacting a fatty alcohol of formula CmH2m+1OH with butylene or propylene oxide in the presence of an alkaline catalyst at 100-150 DEG C., washing the product, esterifying with succinic anhydride in presence of pyridine at from 90-100 DEG C. for three hours, neutralizing with potassium hydroxide at about 80 DEG C., and finally precipitating the magnesium salt by adding an excess of magnesium chloride in aqueous solution is used as an emulsifier in water-in-oil emulsions.ALSO:Emulsifiers for water-in-oil type medicinal and cosmetic compositions comprise magnesium salts of a succinic ester of formula: in which m is an integer of 12 or greater, preferably 12-18, and n and p are each from 0 to 12 inclusive, the sum of n and p being from 2 to 12 inclusive (see Division C2). Oil in the emulsion may be paraffin, petrolatum, perhydrosqualene, or a solution of a microcrystalline wax in paraffin oil; an animal or vegetable oil such as horse oil, lard, sweet almond or calaphyllum; saturated esters such as isopropyl palmitate or myristate, and ethyl palmitate and silicone oils. Other additives may be cetyl, stearyl, or lanolin alcohols, fatty alcohols from beeswax, cholesterol and magnesium stearate. Examples describe the preparation of a moisturising lotion and cream, a foundation, hand, and cuticle cream, a brilliantine and a cream for treating burns of the water-in-oil type using the emulsifying agent and other ingredients mentioned above.

    55.
    发明专利
    未知

    公开(公告)号：FR87224E

    公开(公告)日：1966-07-01

    申请号：FR2339

    申请日：1965-01-18

    Applicant: OREAL

    Inventor： KALOPISSIS GREGOIRE ,  ZVIAK CHARLES ,  VIOUT ANDRE

    IPC: A61K8/81 ,  A61Q5/06 ,  C08F8/30 ,  C08F8/32 ,  C08F8/34 ,  C08F228/00 ,  C08G59/18

    Abstract: A polymer has a recurring structural unit of formula in which R1 and R11 are -H, a C1- 4 alkyl or alkoxy radical or a phenyl radical, R111 is -H, -OCOCH3, -COOCH3 or -CN, Y is Q or Q1, where is where R1 is -H or -CH3, R2 is -H or -COOH, q is 1-5, q1 and p are 0 or 1 and Q1 is where R3 is -H, or a C1- 4 alkyl radical, R4 is R3 or where the r's are a C1- 4 alkyl radical or, together with the N-atom to which they are attached, form a heterocyclic ring, and m is 2-4; the polymer containing both Q and Q1. The polymer may be produced by condensing an amino-thiol and an alkylamine with a copolymer having the repeating unit where the symbols in the formulae are as above. In examples, methyl acrylate, methyl methacrylate, acrylonitrile, vinyl acetate, ethylene or styrene-maleic an hydrid copolymer was condensed with b -mercapto ethylamine, cysteine or N - (b - aminoethyl) thioglycolamide and N,N - diethylpropylene diamine, n-butyl-amine or N-(b -aminoethyl) morpholine. The polymers may be compounded with (A) a vinyl pyrrolidone/vinyl acetate copolymer, water, ethyl alcohol, the tetrasodium salt of ethylene diamine tetracetic acid and 2-amino-2-methyl-1-propanol, triethanolamine or N,N-dimethyl ethanolamine, or (B) a cetyl-stearyl alcohol/ethylene oxide condensate and an aerosol propellant, e.g. a fluorinated hydrocarbon.ALSO:Human hair is set and the receptivity of textile keratinic fibres towards reactive dyes is improved by treatment with a polymer having the repeating unit where R1 and R11 are -H, a C1-4 alkyl or alkoxy radical or a phenyl radical, R111 is -H, -OCOCH3, -COOCH3 or -CN, Y is Q or Q1 where Q is where R1 is -H or -CH3, R2 is -H or -COOH, q is 1-5, q1 and p are 0 or 1 and Q1 is where R3 is -H or a C1-4 alkyl radical, R4 is R3 or where the r's are a C1-4 alkyl radical 2 or 1 together with the N-atom to which they are attached, form a heaterocyclic ring, and m is 2-4; the polymer containing both Q and Q1. In examples the polymer resulting from the condensation of b -mercaptoethylamine or N-(b -aminoethyl)thioglycolamide and N,N-diethylpropylenediamine or butylamine with an ethylene vinyl acetate, methyl methacrylate or acrylonitrile and maleic anhydride copolymer was compounded with water ethanol, the tetrasodium salt of ethylene diamine tetracetic acid and 2-amino-2-methyl-1-propanol, triethanolamine or N,N-dimethyl ethanolamine to form a setting lotion for human hair and with a cetyl-stearyl alcohol/ethylene oxide condensate and a fluorinated hydrocarbon to form an aerosol foam for hair.ALSO:A setting lotion or aerosol foam for human hair contains a polymer having a recurring structural unit of formula (I) in which R1 and R11 are -H, a C1-4 alkyl or alkoxy radical or a phenyl radical R111 is -H, -OCOCH3, -COOCH3 or -CN, Y is Q or Q1 where Q is (II) where R1 is -H or -CH3, R2 is -H or -COOH, q is 1-5, q and p are 0 or 1 and Q1 is (III) where R3 is -H, or a C1-4 alkyl radical, R4 is R3 or where the r's are a C1-4 alkyl radical or, together with the N-atom to which they are attached, form a heterocyclic ring, and m is 2-4; the polymer containing both Q and Q1. In examples the polymer resulting from the condensation of b -mercapto-ethylamine or N-(b -aminoethyl) thioglycolamide and N,N-diethylpropylene-diamine or butylamine with an ethylene, vinyl acetate, methyl methacrylate or acrylonitrile and maleic anhydride copolymer was compounded with a vinyl pyrrolidone vinyl acetate copolymer, water, ethyl alcohol, the tetrasodium salt of ethylene diamine tetracetic acid and 2-amino-2-methyl-1-propanol, triethanolamine or N,N-dimethyl ethanolamine to form a setting lotion and with a cetylstearyl alcohol/ethylene oxide condensate and an aerosol propellant, e.g. a fluorinated hydrocarbon, to form an aerosol foam.

    57.
    发明专利
    未知

    公开(公告)号：FR1344212A

    公开(公告)日：1963-11-29

    申请号：FR888177

    申请日：1962-02-15

    Applicant: OREAL

    Inventor： KALOPISSIS GREGOIRE ,  VIOUT ANDRE

    IPC: C07C233/46 ,  C07C237/00 ,  C07D295/13 ,  C09K23/00 ,  C11D1/88

    Abstract: 1,125,919. Dyeing hair. L'OREAL. 27 Jan., 1966 [22 June, 1965], No. 26106/67. Divided out of 1,094,205. Addition to 1,003,345. Heading D1B. Compositions for dyeing: human hair comprise a hair dye and a compound of formula:- or an acid addition or Na, K, or NH 4 salt thereof wherein R 1 and R 2 are C 1-4 alkyl or together with the N atom form a heterocyclic ring and R 3 is a C 10-18 aliphatic hydrocarbon radical and n is 2, 3, 4 or 5. Specified dyes are oxidation dyes in which case an oxidising agent e.g. H 2 O 2 will normally be added shortly before the composition is used.

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