公开(公告)号：US06241890B1

公开(公告)日：2001-06-05

申请号：US09332710

申请日：1999-06-14

Applicant: Dale Lee Clay ,  Robert W. Allington ,  Philip Bernard Liescheski, III ,  Robin Randall Winter ,  Daniel Gene Jameson

Inventor： Dale Lee Clay ,  Robert W. Allington ,  Philip Bernard Liescheski, III ,  Robin Randall Winter ,  Daniel Gene Jameson

IPC: B01D1100

CPC classification number: B01D11/0203 ,  B01D11/0407 ,  F04B9/042 ,  F04B15/08 ,  F04B49/065 ,  F04B2205/03 ,  F04B2205/05 ,  F04B2205/09 ,  F05B2230/41 ,  F05C2201/0493 ,  F05C2253/12 ,  F16K15/183 ,  G01F1/34 ,  G01N1/34 ,  G01N1/40 ,  G01N30/02 ,  G01N30/28 ,  G01N2001/4033 ,  G01N2001/4061 ,  G01N2030/6013 ,  G01N2035/0441 ,  G21F5/015 ,  B01D15/40

Abstract: To collect analyte from a supercritical fluid extractor, the collector lifts vials into place by a biasing means that guides the file up to the restrictor where it is sealed. The vial can be moved back down from the collecting mechanism even if frost forms on the vial while the restrictor means remains stationary. This vial is held in place by a guide that contains the seal for sealing the vial when it is raised in place.

Abstract translation: 为了从超临界流体提取器收集分析物，收集器通过偏压装置将小瓶提升到适当位置，该偏压装置将文件引导到限制器的密封位置。 即使在限制器装置保持静止的情况下，小瓶也可以从收集机构向后移回。 该小瓶通过包含用于密封小瓶的密封件的引导件保持在适当位置，当它被升高到适当位置时。

公开(公告)号：US6129996A

公开(公告)日：2000-10-10

申请号：US375251

申请日：1999-08-16

Applicant: Carl Edward Cordy

Inventor： Carl Edward Cordy

IPC: F04B39/00 ,  B32B15/01 ,  C22C13/00 ,  C22C13/02 ,  C23C22/00 ,  C23C22/66 ,  F04B27/08 ,  F04B27/10

CPC classification number: C22C13/02 ,  B32B15/017 ,  C22C13/00 ,  C23C22/66 ,  F04B27/1054 ,  F05C2201/0463 ,  F05C2201/0469 ,  F05C2201/0493 ,  F05C2253/12 ,  Y10S428/926 ,  Y10S428/936 ,  Y10T428/12583 ,  Y10T428/1259 ,  Y10T428/12708 ,  Y10T428/12736 ,  Y10T428/1275

Abstract: An aluminum or aluminum alloy surface which during use is exposed to sliding friction has a chemical conversion coating of mostly tin with 0.2-10.0 wt. % cobalt and 0.1 to 12 wt. % bismuth. For example, a swashplate of a swashplate type compressor may be conversion coated on at least part thereof, that is the part that during use contact the shoes. Preferably, the coating is between 0.8 to 2.5 microns thick. The coating on the swash plate permits the use of low silicon alloy aluminum without the need of metal plating or high finish polishing.

Abstract translation: 在使用中暴露于滑动摩擦的铝或铝合金表面具有主要为锡的化学转化涂层，其为0.2-10.0重量％ ％钴和0.1至12wt。 ％铋。 例如，斜盘式压缩机的旋转斜盘可以在其至少部分转化涂层，即在使用过程中与鞋接触的部分。 优选地，涂层在0.8至2.5微米厚之间。 旋转斜盘上的涂层允许使用低硅合金铝，而不需要金属电镀或高精抛光。

公开(公告)号：US6071408A

公开(公告)日：2000-06-06

申请号：US80826

申请日：1998-05-18

Applicant: Robert William Allington ,  Daniel Gene Jameson ,  Dale A. Davison ,  Dale Clay ,  Robin R. Winter ,  Yoossef Tehrani

Inventor： Robert William Allington ,  Daniel Gene Jameson ,  Dale A. Davison ,  Dale Clay ,  Robin R. Winter ,  Yoossef Tehrani

IPC: B01D11/00 ,  B01D11/02 ,  B01D11/04 ,  F04B9/04 ,  F04B15/08 ,  F04B49/06 ,  F04B53/08 ,  F04B53/14 ,  F16K15/18 ,  G01F1/34 ,  G01N1/34 ,  G01N1/40 ,  G01N30/02 ,  G01N30/28 ,  G01N30/60 ,  G01N35/04 ,  G21F5/015 ,  B01D17/12

CPC classification number: G01N1/34 ,  B01D11/0203 ,  B01D11/0407 ,  F04B15/08 ,  F04B49/065 ,  F04B53/08 ,  F04B53/143 ,  F04B9/042 ,  F16K15/183 ,  G01F1/34 ,  G01N1/40 ,  G01N30/28 ,  G21F5/015 ,  F04B2201/0209 ,  F04B2205/03 ,  F04B2205/05 ,  F04B2205/09 ,  F05B2230/41 ,  F05C2201/0493 ,  F05C2253/12 ,  G01N2001/4033 ,  G01N2001/4061 ,  G01N2030/6013 ,  G01N2035/0441 ,  G01N30/02

Abstract: To provide performance particularly in handling supercritical extraction systems, a specially designed pump includes a cam-driven, single-plunger with a cam having a profile that enables the pumping system to avoid destructive reverse torque on the cam, gear train and drive motor after the cam passes top dead center. The fluid volume leaving the pump is determined by measuring only pressure or other parameters related to flow and movement of the plunger. Measurement of the fluid volume leaving the pump is useful for recording or indicating the flow rate while the pump is operating.

Abstract translation: 为了提供特别在处理超临界萃取系统中的性能，专门设计的泵包括凸轮驱动的单柱塞，其具有凸轮，该凸轮具有轮廓，使得泵系统能够避免在凸轮，齿轮系和驱动马达之后的破坏性反向扭矩 凸轮通过上死点。 通过仅测量与柱塞的流动和运动相关的压力或其它参数来确定离开泵的流体体积。 离开泵的流体体积的测量对于在泵运行时记录或指示流量是有用的。

公开(公告)号：US5738498A

公开(公告)日：1998-04-14

申请号：US673202

申请日：1996-06-27

Applicant: Robert William Allington ,  Daniel Gene Jameson ,  Dale A. Davison ,  Dale Clay ,  Robin R. Winter ,  Yoossef Tehrani

Inventor： Robert William Allington ,  Daniel Gene Jameson ,  Dale A. Davison ,  Dale Clay ,  Robin R. Winter ,  Yoossef Tehrani

IPC: B01D11/00 ,  B01D11/02 ,  B01D11/04 ,  F04B9/04 ,  F04B15/08 ,  F04B49/06 ,  F04B53/08 ,  F04B53/14 ,  F16K15/18 ,  G01F1/34 ,  G01N1/34 ,  G01N1/40 ,  G01N30/02 ,  G01N30/28 ,  G01N30/60 ,  G01N35/04 ,  G21F5/015 ,  F04B39/06 ,  F25B21/02

CPC classification number: G01N1/34 ,  B01D11/0203 ,  B01D11/0407 ,  F04B15/08 ,  F04B49/065 ,  F04B53/08 ,  F04B53/143 ,  F04B9/042 ,  F16K15/183 ,  G01F1/34 ,  G01N1/40 ,  G01N30/28 ,  G21F5/015 ,  F04B2201/0209 ,  F04B2205/03 ,  F04B2205/05 ,  F04B2205/09 ,  F05B2230/41 ,  F05C2201/0493 ,  F05C2253/12 ,  G01N2001/4033 ,  G01N2001/4061 ,  G01N2030/6013 ,  G01N2035/0441 ,  G01N30/02

Abstract: In a piston pump for pumping liquid carbon dioxide at a temperature below 30 degrees Fahrenheit and pressures at least as high as 7500 psi at an outlet flow rate in excess of 10 milliliters per minute, the inlet to the pump and the pumphead are each cooled by thermoelectric heat exchangers that are air cooled. The pump is a cam-driven, single-plunger pump with a cam profile that enables the pumping system to avoid distructive reverse torque on the cam, gear train and drive motor after the cam passes top dead center. The volume leaving the pump is determined by measuring only pressure or other parameter related to flow and movement of the plunger. The piston of the pump is supported on both sides of the seal and the support for the piston within the pumphead are machined consentrically and colinearly to the seal gland.

Abstract translation: 在用于在低于30华氏度的温度下泵送液体二氧化碳的活塞泵和在超过10毫升/分钟的出口流速下至少高达7500psi的压力下，泵和泵头的入口各自被 空气冷却的热电换热器。 泵是具有凸轮轮廓的凸轮驱动的单柱塞泵，其能够使泵送系统在凸轮通过上止点之后避免凸轮，齿轮系和驱动马达上的破坏性反向扭矩。 通过仅测量与柱塞的流动和运动相关的压力或其他参数来确定离开泵的体积。 泵的活塞支撑在密封件的两侧，并且泵头内的活塞支撑件同步地并且与密封压盖共同加工。

公开(公告)号：US5635070A

公开(公告)日：1997-06-03

申请号：US208121

申请日：1994-03-08

Applicant: Robert W. Allington ,  Daniel G. Jameson ,  Dale A. Davison ,  Dale Clay ,  Robin R. Winter ,  Yoossef Tehrani

Inventor： Robert W. Allington ,  Daniel G. Jameson ,  Dale A. Davison ,  Dale Clay ,  Robin R. Winter ,  Yoossef Tehrani

IPC: B01D11/00 ,  B01D11/02 ,  B01D11/04 ,  F04B9/04 ,  F04B15/08 ,  F04B49/06 ,  F04B53/08 ,  F04B53/14 ,  F16K15/18 ,  G01F1/34 ,  G01N1/34 ,  G01N1/40 ,  G01N30/02 ,  G01N30/28 ,  G01N30/60 ,  G01N35/04 ,  G21F5/015

CPC classification number: G01N1/34 ,  B01D11/0203 ,  B01D11/0407 ,  F04B15/08 ,  F04B49/065 ,  F04B53/08 ,  F04B53/143 ,  F04B9/042 ,  F16K15/183 ,  G01F1/34 ,  G01N1/40 ,  G01N30/28 ,  G21F5/015 ,  F04B2201/0209 ,  F04B2205/03 ,  F04B2205/05 ,  F04B2205/09 ,  F05B2230/41 ,  F05C2201/0493 ,  F05C2253/12 ,  G01N2001/4033 ,  G01N2001/4061 ,  G01N2030/6013 ,  G01N2035/0441 ,  G01N30/02

Abstract: To pump supercritical carbon dioxide into a supercritical extractor without overpressure in the reservoir and to record the volume being delivered, the pumping speed is controlled and the volume pumped is determined from a pressure-related signal used in a feedback circuit. The feedback controls the velocity of pumping in conjunction with programmed values to avoid destructive reverse torque. A cam in the pump controls piston stroke, has a depressurization portion with an initial slope equal to but in the opposite direction of the final slope, rounded transition slopes, increasing linear velocity to the refill portion and constant velocity in the refill portion.

公开(公告)号：US5614089A

公开(公告)日：1997-03-25

申请号：US542683

申请日：1995-10-13

Applicant: Robert W. Allington ,  Henry L. Walters ,  Daniel G. Jameson ,  Yoossef Tehrani

Inventor： Robert W. Allington ,  Henry L. Walters ,  Daniel G. Jameson ,  Yoossef Tehrani

IPC: B01D11/02 ,  B01D11/04 ,  F04B9/04 ,  F04B15/08 ,  F04B49/06 ,  F16K15/18 ,  G01F1/34 ,  G01N1/34 ,  G01N1/40 ,  G01N30/02 ,  G01N30/28 ,  G01N30/32 ,  G01N30/60 ,  G01N30/82 ,  G01N35/04 ,  G21F5/015 ,  B01D15/08

CPC classification number: B01D11/0407 ,  B01D11/0203 ,  F04B15/08 ,  F04B49/065 ,  F04B9/042 ,  F16K15/183 ,  G01F1/34 ,  G01N1/34 ,  G01N1/40 ,  G01N30/28 ,  G01N30/82 ,  G21F5/015 ,  F04B2205/03 ,  F04B2205/05 ,  F04B2205/09 ,  F05B2230/41 ,  F05C2201/0493 ,  F05C2253/12 ,  G01N2001/4033 ,  G01N2001/4061 ,  G01N2030/6008 ,  G01N2030/6013 ,  G01N2035/0441 ,  G01N30/02 ,  G01N30/32 ,  G01N30/60

Abstract: A variable-orifice fluid restrictor for use with a supercritical extractor or chromatograph includes an inlet line for fluid at a pressure above its critical pressure, an extended tubular probe having an inner and an outer surface and a proximal and a distal end. The proximal end of the probe is disposed toward the inlet line. The distal end of the probe includes an adjustable orifice means adapted for metering the fluid and having first and second orifice members and an adjusting stem having first and second ends. The adjustable orifice means is adjacent to the outer surface of the probe and the orifice means is adjustable with the adjusting stem. The end of the adjusting stem is located at the distal end of the probe and is adapted for moving the first orifice member with respect to the second orifice member to control the adjustable orifice for varying the restriction of fluid passing through the adjustable orifice.

Abstract translation: 用于超临界萃取器或色谱仪的可变孔口流体限制器包括用于高于其临界压力的压力的流体的入口管线，具有内外表面和近端和远端的延伸管状探针。 探针的近端朝向入口线设置。 探针的远端包括适于计量流体并具有第一和第二孔口构件的调节孔口装置和具有第一和第二端部的调节杆。 可调整的孔口装置与探针的外表面相邻，孔口装置可用调节杆调节。 调节杆的端部位于探针的远端，并且适于相对于第二孔构件移动第一孔构件以控制可调节孔，以改变通过可调节孔的流体的限制。

公开(公告)号：US5198197A

公开(公告)日：1993-03-30

申请号：US908458

申请日：1992-07-06

Applicant: Dale L. Clay ,  Robert W. Allington

Inventor： Dale L. Clay ,  Robert W. Allington

IPC: B01D11/02 ,  B01D11/04 ,  F04B9/04 ,  F04B15/08 ,  F04B49/06 ,  F16K15/18 ,  G01F1/34 ,  G01N1/34 ,  G01N1/40 ,  G01N30/02 ,  G01N30/28 ,  G01N30/60 ,  G01N35/04 ,  G21F5/015

CPC classification number: G01N30/28 ,  B01D11/0203 ,  B01D11/0407 ,  F04B15/08 ,  F04B49/065 ,  F04B9/042 ,  F16K15/183 ,  G01F1/34 ,  G01N1/34 ,  G01N1/40 ,  G21F5/015 ,  F04B2205/03 ,  F04B2205/05 ,  F04B2205/09 ,  F05B2230/41 ,  F05C2201/0493 ,  F05C2253/12 ,  G01N2001/4033 ,  G01N2001/4061 ,  G01N2030/6013 ,  G01N2035/0441 ,  G01N30/02

Abstract: An apparatus for supercritical fluid extraction incorporates a removable extraction cartridge which in operation has insignificant pressure difference between its inside and outside walls. Because of the low pressure difference, the extraction cartridge need not have the strength to withstand significant pressure and can be made out of molded plastic for disposable use as well as stainless steel and/or machined plastic for reusability. The extraction cartridge can be removed and opened for sample access without the use of tools. The outside of the cartridge can be purged after it is installed in a heated high pressure vessel to remove contamination from its exterior. In one embodiment, the extractor includes a fraction collector for extractments, an automatic sample changer and an automatic carteidge transfer mechanism which provide completely automated extractions.

Abstract translation: 用于超临界流体萃取的装置包括可移除的提取筒，其在操作中在其内壁和外壁之间具有不显着的压力差。 由于低压差，提取筒不需要具有承受显着压力的强度，并且可以由用于一次性使用的模制塑料以及用于可重复使用的不锈钢和/或加工塑料制成。 提取盒可以拆卸和打开，无需使用工具进行样品通道。 在将其安装在加热的高压容器中以清除其外部的污染物之后，可将其清除。 在一个实施例中，提取器包括用于提取的馏分收集器，自动取样器和自动提升机输送机构，其提供完全自动提取。

公开(公告)号：US5056417A

公开(公告)日：1991-10-15

申请号：US434240

申请日：1989-11-13

Applicant: Masafumi Kato ,  Takenori Sawa ,  Futoshi Sakata ,  Yoshifumi Kato

Inventor： Masafumi Kato ,  Takenori Sawa ,  Futoshi Sakata ,  Yoshifumi Kato

IPC: F04B27/08 ,  F04B27/10

CPC classification number: F04B27/1054 ,  F05C2201/0466 ,  F05C2201/0475 ,  F05C2201/0493 ,  F05C2203/06 ,  F05C2203/083 ,  F05C2203/086 ,  F05C2253/12

Abstract: A swash plate type compressor is provided with a surface coating layer on the surface of a swash plate. The surface coating layer acts to prevent the frictional resistance which leads to seizure conventionally occurring by the direct contact of the shoes and the swash plate body. The swash plate body is produced from aluminum or aluminum alloy and the surface coating layer is made of tin and at least one metal selected from the group consisting of copper, nickel, zinc, lead and indium.

Abstract translation: 旋转斜盘式压缩机在旋转斜盘表面设有表面涂层。 表面涂层的作用是防止摩擦阻力通过鞋和旋转斜盘体的直接接触而常常发生。 旋转斜盘体由铝或铝合金制成，表面涂层由锡和至少一种选自铜，镍，锌，铅和铟的金属制成。

公开(公告)号：US4662267A

公开(公告)日：1987-05-05

申请号：US699109

申请日：1985-02-07

Applicant: Yoshihiro Kaku ,  Keiichiro Otsu

Inventor： Yoshihiro Kaku ,  Keiichiro Otsu

IPC: B21K1/76 ,  B21K3/00 ,  F04B27/08 ,  F01B3/00 ,  F04B1/12

CPC classification number: B21K1/76 ,  B21K3/00 ,  F04B27/0882 ,  F04B27/0886 ,  F05C2201/025 ,  F05C2201/0457 ,  F05C2201/0466 ,  F05C2201/0493 ,  F05C2203/04 ,  F05C2203/086 ,  F05C2253/12 ,  Y10T74/18336

Abstract: There are disclosed a shoe which is interposed between a swash plate and a piston of a swash plate type compressor and which converts rotary movement of the swash plate into reciprocal movement of the piston, and a method for manufacturing the same. The shoe has a hemispherical part which is in slidable contact with the surface of a piston defining a hemispherical recess, and a flat end face which is in slidable contact with a bottom end face of the swash plate. According to the method of the invention, a columnar element is compressed in the axial direction for plastic deformation in such a manner that one end of the columnar element is deformed along the inner surface of a hemispherical recess of a die while the other end is urged against the flat end surface of another die. A shoe can be easily manufactured with this method, which has a flank between the hemispherical part which is in slidable contact with the surface of the piston defining the hemispherical recess and the bottom end face of the swash plate which is in slidable contact with the swash plate. According to this method, a hole of a predetermined size may alternatively be formed at the end face of a columnar part of the element, and the end face of the columnar part is cut into a conical shape while reducing the diameter of the hole toward the opening side thereof. Still alternatively, the periphery of the end face of the columnar part may be cut into a conical shape and then pressed to form a hemispherical part. A great flow of the material and local exertion of a high load on the element are prevented.

公开(公告)号：US4512175A

公开(公告)日：1985-04-23

申请号：US328547

申请日：1981-11-27

Applicant: Yoshihiro Kaku ,  Keiichiro Otsu

Inventor： Yoshihiro Kaku ,  Keiichiro Otsu

IPC: B21K1/76 ,  B21K3/00 ,  F04B27/08 ,  B21J13/02

CPC classification number: B21K1/76 ,  B21K3/00 ,  F04B27/0882 ,  F04B27/0886 ,  F05C2201/025 ,  F05C2201/0457 ,  F05C2201/0466 ,  F05C2201/0493 ,  F05C2203/04 ,  F05C2203/086 ,  F05C2253/12 ,  Y10T74/18336

Abstract: There are disclosed a shoe which is interposed between a swash plate and a piston of a swash plate type compressor and which converts rotary movement of the swash plate into reciprocal movement of the piston, and a method for manufacturing the same. According to the method of the invention, a columnar element is compressed in the axial direction for plastic deformation in such a manner that one end of the columnar element is deformed along the inner surface of a hemispherical recess of a die while the other end is urged against the flat end surface of another die. A shoe can be easily manufactured with this method, which has a flank between the hemispherical part which is in slidable contact with the surface of the piston defining the hemispherical recess and the bottom end face of the swash plate which is in slidable contact with the swash plate. According to this method, a hole of a predetermined size may alternatively be formed at the end face of a columnar part of the element, and the end face of the columnar part is cut into a conical shape while reducing the diameter of the hole toward the opening side thereof. Still alternatively, the periphery of the end face of the columnar part may be cut into a conical shape and then pressed to form a hemispherical part. A great flow of the material and local exertion of a high load on the element are prevented.

Abstract translation: PCT No.PCT / JP81 / 00067 Sec。 371日期：1981年11月27日 102（e）1981年11月27日PCT PCT Fils 3月28日PCT公布。 公开号WO81 / 02767 日本公报1981年10月1日。公开了一种插入斜盘式压缩机的旋转斜盘和活塞之间的鞋，其将旋转斜盘的旋转运动转换为活塞的往复运动，以及用于制造 相同。 根据本发明的方法，柱状元件在轴向被压缩以进行塑性变形，使得柱状元件的一端沿着模具的半球形凹部的内表面变形，同时另一端被推动 抵靠另一个模具的平坦端面。 可以容易地制造鞋子，该方法在半球形部分之间具有侧面，该半球形部分与限定半球形凹部的活塞的表面可滑动接触，以及与斜盘可滑动接触的斜盘的底端面 盘子。 根据该方法，也可以在元件的柱状部的端面形成预定尺寸的孔，并且将柱状部的端面切割成圆锥形状，同时将孔的直径减小到 其开口侧。 或者，柱状部分的端面的周边可以被切割成圆锥形，然后被压制以形成半球形部分。 材料的大量流动和元件上的高负载的局部耗尽被阻止。