Abstract:
본 발명은 이성질체 혼합물의 스펙트럼을 기록하고 스펙트럼을 계량화학적 보정 모델로 보내는, 이소시아네이트 이성질체 혼합물 내 이성질체 조성을 측정하는 방법에 관한 것이다. 이소시아네이트 이성질체 혼합물, 계량화학적 보정 모델, 이성질체 조성의 측정 방법
Abstract:
A method and apparatus for measuring the concentration of a very small amount of impurities in an object gas by an infrared spectroscopic analysis using a semiconductor laser. In order to carry out the analysis with a high sensitivity and a high accuracy, an object gas is introduced into a sample cell (5) and the cell is evacuated by a vacuum pump (16). An infrared beam of a wavelength in a region in which a high absorption peak due to impurities appears is emitted from a semiconductor laser (1) and passed through the sample cell (5) and a reference sample cell (8) in which impurities alone are sealed to measure a differential value absorption spectrum. The impurities are identified by comparing the spectrum of the object gas with that of impurities alone and determining a plurality of absorption peaks concerning the impurities, and the quantity of the impurities is determined on the basis of the absorption intensity at the highest peak. When impurity gas molecules form clusters in the object gas, the light of not less than 0.5 eV is applied to the clusters to dissociate the same, and the analysis of the gas is then carried out. This invention is suitably utilized, especially, for analyzing a very small amount of impurities in a semiconductor material gas.
Abstract:
A polarization imaging device is provided to improve a space resolution of a microscope by extracting a non-linear vibration polarization signal using a short-wavelength probe beam. A pump source(10) and a probe source(20) generate pump and probe beams, respectively. Polarizers(11,21) linearly polarize the pump and probe beams. A beam combiner(30) temporally synchronizes the pump and probe beams and guides the beams on the same axis. A scanner(40) scans the beams on a plane. An optical focusing system(50) focuses the beams on a test material. A collecting optical system(60) collects beams, which are phase-shifted due to a birefringence, to generate a parallel beam. A beam splitter(70) removes an IR(InfraRed) pump beam from the parallel beam and separates an anisotropy phase-shifted probe beam. A polarizing beam splitter(80) converts the separated probe beam to a linear polarizing beam having normal axial components. Light detectors(91,92) detect a magnitude of the linear polarizing beam. A polarization difference detector(100) detects a polarization difference due to a magnitude of the detected linear polarizing beam. A data analyzer(110) collects the polarization difference and generates and extracts a polarizing signal according to a molecular vibration resonance intensity.
Abstract:
PURPOSE: A measuring method of composition of isomer in manufacturing isocyanate and a device thereof are provided to increase the yield rate by measuring the spectrum of isomer compound and detecting the density of the isomer compound. CONSTITUTION: An isomer compound is manufactured(100), and an isomer mixture(G1) is separated from the raw isomer compound by distilling or crystallizing(102). The index is initialized(104), and the spectrum of the isomer mixture is measured at the outlet of the isomer manufacturing system. The NIR spectrum is analyzed by using the compensation model(108). The difference between the predetermined isomer compound and the actual isomer compound is measured(112), and the isomer manufacturing system is adjusted based on the difference value(114). The index is increased(116), and the next spectrum is measured.
Abstract in simplified Chinese:一种系统,包括传输器被配置用以将电磁信号经由样本胞元(包括样本媒介)传输至接收器,该接收器被配置用以接收该电磁信号以及用以与其混合的另一个电磁信号。该信号传至该传输器以及接收器的传播路径包括该电磁信号至该传输器的第一传播路径,以及该另一个电磁信号至该接收器的第二传播路径。沿着信号至该传输器以及接收器之传播路径的其中一个或每一个而被设置的该排列被配置用以改变分别传播路径的长度。以及该处理器被配置用以恢复所传输之电磁信号的振幅以及相位,以及以所传输之电磁信号的振幅以及相位为函数而计算该样本媒介的复折射指数。