SAFETY PROCESS FOR PRESSURE EQUIPMENT IN CONTACT WITH CORROSIVE FLUIDS
    81.
    发明授权
    SAFETY PROCESS FOR PRESSURE EQUIPMENT IN CONTACT WITH CORROSIVE FLUIDS 失效
    用于打印设备的安全程序,接触腐蚀性液体IS

    公开(公告)号:EP0888176B2

    公开(公告)日:2003-12-03

    申请号:EP97914213.0

    申请日:1997-03-21

    Inventor: MIOLA, Cesare

    Abstract: Method for the safety and extension of the operating life of pressure equipment comprising an internal chamber suitable for containing a process fluid, surrounded by a pressure-resistant body (1) equipped with weep-holes (2), consisting of a material subject to corrosion by contact with said process fluid during operation, coated inside with an anticorrosive lining (4) made up of several elements welded to each other, wherein said lining weldings (3) are completely isolated from contact with the process fluid of the normal operating run, by a coating with adjoining strips (or plates) (10, 10', 10', 10'''), of the same material as said lining (4) or other corrosion-resistant material weldable thereto, which are subsequently seal-welded on the edges to said lining (4) and to each other, characterized in that the arrangement and welding of the edges of these strips (10, 10', 10', 10''') are such as to create a network of underlying interstices (or meati) (9, 11), communicating with each other and with at least one weep-hole (2).

    ISOSTAT FOR THE TREATMENT OF MATERIALS IN LIQUID
    83.
    发明公开
    ISOSTAT FOR THE TREATMENT OF MATERIALS IN LIQUID 审中-公开
    ISOSTATFÜRDIE BEHANDLUNG VON MATERIALIEN IN EINERFLÜSSIGKEIT

    公开(公告)号:EP1252953A1

    公开(公告)日:2002-10-30

    申请号:EP00923035.0

    申请日:2000-04-25

    CPC classification number: B01J3/048 B22F2998/00 B30B11/002 B22F3/15

    Abstract: The invention relates to the equipment for high-pressure, high-temperature treatment of materials in liquid and enables to broaden the technological capabilities of an isostatic press. The isostatic press for treatment of materials in liquid comprises a multi-cylinder pressure vessel forming a hermetically sealed working chamber connected to a gas source. The open-top container for liquid is placed in the working chamber in such a way that a gap is created between the inner wall of the pressure vessel and the outer wall of the container. The container with the liquid and the treated material is placed on an electrically insulated heater which, in its turn, is mounted on a protective magnetic block.

    Abstract translation: 本发明涉及用于液体材料的高压,高温处理的设备,并且能够扩大等静压机的技术能力。 用于处理液体中的材料的等静压机包括形成连接到气源的气密密封工作室的多气缸压力容器。 用于液体的敞开顶部容器以这样的方式放置在工作室中,使得在压力容器的内壁和容器的外壁之间产生间隙。 具有液体和经处理的材料的容器放置在电绝缘加热器上,该加热器依次安装在保护性磁性块上。

    Pressure vessel with composite sleeve
    84.
    发明公开
    Pressure vessel with composite sleeve 有权
    DruckbehältermitHülleaus zusammengesetztem材料

    公开(公告)号:EP1228801A1

    公开(公告)日:2002-08-07

    申请号:EP01204407.9

    申请日:2000-02-25

    Abstract: A self sealing vessel assembly for high pressure microwave assisted chemistry is disclosed. The vessel assembly includes a polymeric cylinder (12) and a circular polymeric cap (13) for the cylinder, the cylinder being closed at one end and open at the other end to receive the cap. The open end of the cylinder has a lip that is bevelled inwardly from the open end, and the circular polymeric cap (13) has a bevelled lower edge that engages the bevelled lip when the cap (13) is placed upon the polymeric cylinder (12). For high pressure applications, a choke cylinder depends from the bevelled lower edge of the cap, and has an outer diameter substantially the same as the inner diameter of the polymeric cylinder (12) so that the choke provides a self sealing mechanism for the cylinder as pressure from a chemical reaction increases within the cylinder. A supporting frame (14) extends along the cylinder (12) and across the lid (13) and across the closed end of the cylinder, and prevents the lid from being displaced from the cylinder when pressure is generated inside of the vessel.

    Abstract translation: 公开了一种用于高压微波辅助化学的自密封容器组件。 容器组件包括用于气缸的聚合物圆筒(12)和圆形聚合物盖(13),所述圆筒在一端封闭并在另一端开口以接收盖子。 圆筒的开口端具有从开口端向内倾斜的唇缘,并且圆形聚合物盖(13)具有倾斜的下边缘,当盖(13)放置在聚合物圆柱体(12)上时,该下边缘与斜边缘接合 )。 对于高压应用,阻塞气缸从盖的倾斜的下边缘延伸,并且具有与聚合物气缸(12)的内径基本相同的外径,使得扼流圈为气缸提供自密封机构 来自化学反应的压力在气缸内增加。 支撑框架(14)沿着圆柱体(12)延伸并跨过盖子(13)并且横过气缸的封闭端延伸,并且当在容器内产生压力时防止盖子从气缸移位。

    Pressurized reaction block
    85.
    发明公开
    Pressurized reaction block 有权
    Druckreaktionsblock

    公开(公告)号:EP1055452A3

    公开(公告)日:2001-09-19

    申请号:EP00110336.5

    申请日:2000-05-13

    Abstract: A reaction block assembly (11) of reaction vessels (13) for conducting chemical reactions under pressure. The assembly (11) includes a heat conductive reactive block (31,131) having reaction vessel (13) receiving openings (41,133) formed in the block (31,131). A heat exchanger (49) is mounted in heat transfer engagement with some of the exterior walls (39) of the reaction block (31,131). The heat exchangers (49) can operate in different modes, to provide a heat differential across the reaction block (31,131). A reaction vessel (13) is positioned in each reaction vessel receiving opening (41,133) in the block (31,131). A cap (81) is attached to each reaction vessel (13) and a cannula opening is formed in each cap (81). A cannula passage (111) is connected at one end to a cannula opening in each cap (81) and it has a septum (203) at the other end. A valve (193) controls each cannula passage (111). An operating mechanism is provided for opening and closing each cannula passage controlling valve (193). The reaction block assembly (11) may be used to determine when the reaction of a solution in a reaction vessel (13) is completed. This is accomplished by using a calibration curve comparing the frequency of rotation of the stirring bar (73) with the viscosity of the reaction solution in which the frequency is inversely proportional to the viscosity. The time interval at which the stir bar (73) decouples from rotation with the driving magnet is determined. This time interval of decoupling is compared with the calibration table to determine the viscosity of the solution at the time the reaction was completed which takes place at the time the stir bar (73) was decoupled.

    Abstract translation: 用于在压力下进行化学反应的反应容器的反应块组件。 该组件包括具有形成在块中的反应容器接收开口的导热反应性块。 热交换器安装成与反应块的一些外壁传热接合。 热交换器可以以不同的模式操作,以在反应块上提供热差。 反应容器位于块体中的每个反应容器接收开口中。 在每个反应容器上连接一个盖子,并且在每个盖子中形成套管开口。 套管通道在一端连接到每个帽中的套管开口,并且在另一端具有隔膜。 一个阀门控制每个插管通道。 提供了用于打开和关闭每个插管通道控制阀的操作机构。 反应块组件可用于确定反应容器中溶液的反应何时完成。 这通过使用将搅拌棒的旋转频率与其中频率与粘度成反比的反应溶液的粘度进行比较的校准曲线来实现。 确定搅拌棒与驱动磁体与旋转分离的时间间隔。 将该去耦的时间间隔与校准表进行比较,以确定在搅拌棒解耦时发生的反应完成时溶液的粘度。

    SAFETY PROCESS FOR PRESSURE EQUIPMENT IN CONTACT WITH CORROSIVE FLUIDS
    86.
    发明公开
    SAFETY PROCESS FOR PRESSURE EQUIPMENT IN CONTACT WITH CORROSIVE FLUIDS 失效
    与腐蚀性液体接触的压力设备的安全过程

    公开(公告)号:EP0888176A1

    公开(公告)日:1999-01-07

    申请号:EP97914213.0

    申请日:1997-03-21

    Inventor: MIOLA, Cesare

    Abstract: Method for the safety and extension of the operating life of pressure equipment comprising an internal chamber suitable for containing a process fluid, surrounded by a pressure-resistant body (1) equipped with weep-holes (2), consisting of a material subject to corrosion by contact with said process fluid during operation, coated inside with an anticorrosive lining (4) made up of several elements welded to each other, wherein said lining weldings (3) are completely isolated from contact with the process fluid of the normal operating run, by a coating with adjoining strips (or plates) (10, 10', 10', 10'''), of the same material as said lining (4) or other corrosion-resistant material weldable thereto, which are subsequently seal-welded on the edges to said lining (4) and to each other, characterized in that the arrangement and welding of the edges of these strips (10, 10', 10', 10''') are such as to create a network of underlying interstices (or meati) (9, 11), communicating with each other and with at least one weep-hole (2).

    Abstract translation: 一种用于压力设备的使用寿命的安全和延长的方法,所述压力设备包括适于容纳过程流体的内部腔室,所述内部腔室由配备有排泄孔(2)的耐压体(1)围绕,所述排泄孔(2)由受腐蚀的材料 通过在操作过程中与所述过程流体接触,在内部涂覆由彼此焊接的多个元件组成的防腐衬里(4),其中所述衬里焊接(3)完全与正常运行的过程流体接触隔离, 通过具有与所述衬里(4)相同的材料或可焊接到其上的其他耐腐蚀材料的相邻带(或板)(10,10',10',10''')的涂层,随后密封焊接 在所述衬里(4)的边缘和彼此之间,其特征在于,这些条带(10,10',10',10“')的边缘的布置和焊接是为了形成下伏的网络 间隙(或meati)(9,11),与每个o进行通信 并且至少有一个泄水孔(2)。

    HIGH PRESSURE PRESS AND METHOD FOR HIGH PRESSURE TREATMENT OF SUBSTANCES
    87.
    发明公开
    HIGH PRESSURE PRESS AND METHOD FOR HIGH PRESSURE TREATMENT OF SUBSTANCES 失效
    高压压制和方法物质的高压处理

    公开(公告)号:EP0744993A1

    公开(公告)日:1996-12-04

    申请号:EP95910052.0

    申请日:1995-02-14

    CPC classification number: B30B11/004 B01J3/048 B01J3/06

    Abstract: A high-pressure and a method for high-pressure treatment of substances. The high-pressure press comprises a high-pressure cylinder consisting of a number of concentrically arranged cylinder elements (1, 2, 3). The cylinder elements (1, 2, 3) are radially prestressed to a predetermined prestress and surround a high-pressure chamber (6) for accommodating a pressurized medium. A thin safety liner (3), which is intended to be placed in the high-pressure cylinder until a fracture arises on the safety liner (3), is arranged in the interior of the high-pressure cylinder. Further, means (14, 15) are provided to conduct at least part of the pressurized medium from the high-pressure chamber (6) when a fracture arises on the safety liner (3). The means (14, 15) comprise at least one channel (14) running essentially along the outer envelope surface of the safety liner (3). The method comprises using the high-pressure press without liner replacement until a fracture has occurred on the thin safety liner.

    Höchstdruckbehältnis
    88.
    发明公开
    Höchstdruckbehältnis 失效
    Höchstdruckbehältnis。

    公开(公告)号:EP0288453A1

    公开(公告)日:1988-10-26

    申请号:EP88890079.2

    申请日:1988-03-28

    CPC classification number: B01J3/048 B01J3/00 F16J12/00

    Abstract: Einem mehrwandigen Höchst­druckbehältnis ist aus mit Boden (3, 6, 9) und Deckel (4, 7, 10) versehenen Hohl­zylindern (2, 5, 8) gebildet, mit zwischen den Behältern herrschen­den Drücken, das im Druckbereich von 1,2 GPa anwendbar ist. Hierbei soll eine Verbesserung der Materialausnut­zung und Spannungsverteilung erzielt werden, wobei eine Minimierung der Belastungsspanne und des Materialvolumens angestrebt wird. Dies wird dadurch erreicht, daß jeder Hohlzylinder-Boden-Deckel-Teil (A, B, C) ein für sich abgeschlos­senes System darstellt, das jeweils schwimmend im nächst­folgend äußeren System angeordnet ist, und die Zwischen­räume gestuft druckbeaufschlagt sind.

    Abstract translation: 多壁高压容器由设置有基部(3,6,9)和盖(4,7,10)的中空圆柱体(2,5,8)形成,其具有在容器之间的压力,该容器可以 在1.2 GPa的压力范围内使用。 在这种情况下,旨在实现材料利用和应力分布的改进,其目的是使负载范围和材料体积最小化。 这是通过每个中空圆筒底盖部分(A,B,C)实现的,这些空心圆筒底盖部分(A,B,C)表示本体密封系统,每个中空圆柱体底盖部分布置在随后的外部系统中,并且中间空间以阶梯式方式受到压力。

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