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    グリシドール官能化陰イオン交換固定相
    83.
    发明专利
    グリシドール官能化陰イオン交換固定相 审中-公开

    公开(公告)号：JP2015527596A

    公开(公告)日：2015-09-17

    申请号：JP2015531333

    申请日：2013-09-11

    Applicant: ダイオネックス コーポレイション ,  ダイオネックス コーポレイション

    Inventor： クリストファー エイ ポール ,  クリストファー エイ ポール

    IPC: G01N30/88 ,  G01N30/26

    CPC classification number: B01J41/20 ,  B01D15/363 ,  B01J20/288 ,  B01J20/3251 ,  B01J20/3289 ,  B01J41/09

    Abstract: ヒドロキシド型の第4級中心に対してベータ位にあるヒドロキシル含有部分を含有する陰イオン交換材料をグリシドールによって処理することで、陰イオン交換材料の選択性を実質的に変更する。さらに、交互の順序で、最初に、陰イオン交換材料をヒドロキシド型にするためのヒドロキシド含有溶液の連続処理、続いて、グリシドールによる処理によって、選択性の容易な操作を可能にする予想できる様式で次第に選択性が変化する。硫酸イオンおよび炭酸イオンの溶離の順番を逆転させる能力は、この化学で達成可能な選択性に独特である。他の全ての既知のシステムでは、炭酸イオンは硫酸イオンより前に溶離して、硫酸イオンを定量する能力が損なわれることがある。グリシドール処理によって、炭酸イオンは硫酸イオンの後に移動することができ、このことは、硫酸イオンより有意に多くの炭酸イオンを含有する試料の干渉の問題を排除する。この変性は、ヒドロキシド溶離剤システムで動作されるカラム、ならびに炭酸イオン溶離剤システムで動作されるカラムのために有用である。【選択図】図4

    GLYCIDOL FUNCTIONALIZED ANION EXCHANGE STATONARY PHASES
    85.
    发明授权
    GLYCIDOL FUNCTIONALIZED ANION EXCHANGE STATONARY PHASES 有权

    公开(公告)号：EP2895266B1

    公开(公告)日：2018-06-06

    申请号：EP13766187.2

    申请日：2013-09-11

    Applicant: Dionex Corporation

    Inventor： POHL, Christopher, A.

    IPC: B01J41/08 ,  B01J41/09 ,  B01J41/20 ,  B01D15/02 ,  B01D15/36 ,  B01J20/288 ,  B01J20/32

    CPC classification number: B01J41/20 ,  B01D15/363 ,  B01J20/288 ,  B01J20/3251 ,  B01J20/3289 ,  B01J41/09

    Abstract: Treatment of anion exchange materials containing hydroxyl containing moieties in the beta position relative to the quaternary center in the hydroxide form with glycidol substantially alters the selectivity of the anion exchange material. Furthermore, sequential treatments of first a hydroxide containing solution to put the anion exchange material in the hydroxide form followed by treatment with glycidol in an alternating sequence progressively changes selectivity in a predictable manner allowing facile manipulation of selectivity. Unique to the selectivities achievable with this chemistry is the ability to reverse the elution order of sulfate and carbonate. With all other known systems, carbonate elutes ahead of sulfate and sometimes compromises the ability to quantitate sulfate. With glycidol treatment, carbonate can be moved after sulfate which eliminates interference issues for samples containing significantly more carbonate than sulfate. This modification is useful for columns operated with a hydroxide or carbonate eluent system.

    METHOD FOR REGENERATING WEAKLY BASIC ION-EXCHANGE RESIN
    86.
    发明公开
    METHOD FOR REGENERATING WEAKLY BASIC ION-EXCHANGE RESIN 审中-公开
    再生弱碱性离子交换树脂的方法

    公开(公告)号：EP3296261A1

    公开(公告)日：2018-03-21

    申请号：EP17196935.5

    申请日：2014-01-15

    Applicant: Shin-Etsu Chemical Co., Ltd.

    Inventor： ISHIDA, Masahiko ,  SAITO, Hiroshi ,  YOSHIDA, Atsushi

    IPC: C01B33/107 ,  B01J20/26 ,  B01J20/34 ,  C01B33/04 ,  B01J49/00 ,  B01J41/08 ,  B01J41/04 ,  B01J49/57 ,  B01J41/09 ,  B01J41/07 ,  C01B35/02

    CPC classification number: B01J49/57 ,  B01J41/07 ,  B01J41/09 ,  C01B33/046 ,  C01B33/1071 ,  C01B33/10778 ,  C01B33/10784

    Abstract: The present invention provides a technique which allows stable use of an ion-exchange resin for removing boron impurities over a long period of time in the purification step of a silane compound or a chlorosilane compound. In the present invention, a weakly basic ion-exchange resin used for the purification of a silane compound and a chlorosilane compound is cleaned with a gas containing hydrogen chloride. When this cleaning treatment is used for the initial activation of the weakly basic ion-exchange resin, a higher impurity-adsorbing capacity can be obtained. Further, use of the cleaning treatment for the regeneration of the weakly basic ion-exchange resin allows stable use of the ion-exchange resin for a long time. This allows reduction in the amount of the resin used in a long-term operation and reduction in the cost of used resin disposal.

    Abstract translation: 本发明提供一种技术，其能够在硅烷化合物或氯硅烷化合物的纯化步骤中长期稳定地使用用于除去硼杂质的离子交换树脂。 在本发明中，用含氯化氢的气体清洗用于硅烷化合物和氯硅烷化合物的纯化的弱碱性离子交换树脂。 当该清洁处理用于弱碱性离子交换树脂的初始活化时，可以获得更高的杂质吸附能力。 此外，使用弱碱性离子交换树脂再生的清洁处理可以长时间稳定地使用离子交换树脂。 这允许减少长期操作中使用的树脂的量并降低使用的树脂处理的成本。

    METHOD FOR PURIFYING SILANE COMPOUND OR CHLOROSILANE COMPOUND, METHOD FOR PRODUCING POLYCRYSTALLINE SILICON, AND METHOD FOR REGENERATING WEAKLY BASIC ION-EXCHANGE RESIN
    87.
    发明公开
    METHOD FOR PURIFYING SILANE COMPOUND OR CHLOROSILANE COMPOUND, METHOD FOR PRODUCING POLYCRYSTALLINE SILICON, AND METHOD FOR REGENERATING WEAKLY BASIC ION-EXCHANGE RESIN 审中-公开
    方法用于清洁或硅烷化合物的氯硅烷PROCESS FOR PRODUCING多晶硅AND METHOD FOR的弱碱性离子交换树脂的再生

    公开(公告)号：EP2985262A4

    公开(公告)日：2017-03-29

    申请号：EP14782400

    申请日：2014-01-15

    Applicant: SHIN-ETSU CHEMICAL CO LTD

    Inventor： ISHIDA MASAHIKO ,  SAITO HIROSHI ,  YOSHIDA ATSUSHI

    IPC: C01B33/107 ,  B01J20/26 ,  B01J20/34 ,  B01J41/04 ,  B01J41/07 ,  B01J41/08 ,  B01J41/09 ,  B01J49/00 ,  B01J49/57 ,  C01B33/04

    CPC classification number: B01J49/57 ,  B01J41/07 ,  B01J41/09 ,  C01B33/046 ,  C01B33/1071 ,  C01B33/10778 ,  C01B33/10784

    Abstract: The present invention provides a technique which allows stable use of an ion-exchange resin for removing boron impurities over a long period of time in the purification step of a silane compound or a chlorosilane compound. In the present invention, a weakly basic ion-exchange resin used for the purification of a silane compound and a chlorosilane compound is cleaned with a gas containing hydrogen chloride. When this cleaning treatment is used for the initial activation of the weakly basic ion-exchange resin, a higher impurity-adsorbing capacity can be obtained. Further, use of the cleaning treatment for the regeneration of the weakly basic ion-exchange resin allows stable use of the ion-exchange resin for a long time. This allows reduction in the amount of the resin used in a long-term operation and reduction in the cost of used resin disposal.

    Abstract translation: 本发明提供了一种技术，它允许稳定地使用离子交换树脂的超过的时间在硅烷化合物或氯硅烷化合物的纯化步骤长时间除去硼的杂质。 在本发明中，用于硅烷化合物的纯化和一氯硅烷化合物的弱碱性离子交换树脂进行清洗含气体的氯化氢。 当该清洗处理用于弱碱性离子交换树脂的初始活化，较高杂质吸附能力可以得到。 此外，使用清洗处理的弱碱性离子交换树脂的再生的允许长时间稳定使用的离子交换树脂构成。 这允许树脂在在所使用的树脂处理的成本长期运行和减少使用量的减少。

    A METHOD FOR ANION-EXCHANGE ADSORPTION AND ANION-EXCHANGERS
    89.
    发明公开
    A METHOD FOR ANION-EXCHANGE ADSORPTION AND ANION-EXCHANGERS 有权
    ANIONAUSTAUSCHADSORPTIONSVERFAHREN和阴离子交换

    公开(公告)号：EP1235748A2

    公开(公告)日：2002-09-04

    申请号：EP00979615.2

    申请日：2000-11-22

    Applicant: Amersham Biosciences AB

    Inventor： JOHANSSON, Bo-Lennart ,  ANDERSSON, Mikael ,  GUSTAVSSON, Jan ,  BELEW, Makonnen ,  MALOISEL, Jean-Luc

    IPC: C02F1/28 ,  B01J41/00

    CPC classification number: B01J41/20 ,  B01D15/327 ,  B01J41/09 ,  C02F1/42

    Abstract: A method for the removal of a substance carrying a negative charge and being present in an aqueous liquid (I). The method comprises the steps of: (i) contacting the liquid with a matrix carrying a plurality of ligands comprising a positively charged structure and a hydrophobic structure, and (ii) desorbing the substance. The characterizing feature is that (I) each of said ligands together with a spacer has the formula: -- SP---[Ar-R1-N+(R2R3R4)] where (A) [Ar-R1-N+(R2R3R4)] represents a ligand a) Ar is an aromatic ring, b) R1 is [(L)nR'1]m where n and m are integers selected amongst zero or 1; L is amino nitrogen, ether oxygen or thioether sulphur; R'1 is a linker selected among 1) hydrocarbon groups; 2) -C(=NH)-; c) R2-4 are selected among hydrogen and alkyls; (B) SP is a spacer providing a carbon or a heteroatom directly attached to Ar-R1-N+(R2R3R4); (C) --- represents that SP replaces a hydrogen in (Ar-R1-N+(R2R3R4); (D) -- represents binding to the matrix; and (II) desorption. There is also described (a) anion-exchangers having high breakthrough capacities, (b) a screening method and (c) a desalting protocol.

    Cation exchange process, certain cation exchange resins and materials useful therein and processes for their preparation
    90.
    发明公开
    Cation exchange process, certain cation exchange resins and materials useful therein and processes for their preparation 失效
    阳离子交换过程，在这种情况下使用的一些阳离子交换树脂和材料，它们的制备方法。

    公开(公告)号：EP0009395A1

    公开(公告)日：1980-04-02

    申请号：EP79301937.3

    申请日：1979-09-19

    Applicant: ROHM AND HAAS COMPANY

    Inventor： Chong, Berni Patricia

    IPC: B01J39/04 ,  B01J39/20 ,  C08J5/20 ,  C08F220/18 ,  C08F2/18

    CPC classification number: B01J47/018 ,  B01J39/09 ,  B01J41/09 ,  Y10S977/773 ,  Y10S977/775 ,  Y10S977/788 ,  Y10S977/896

    Abstract: Cation exchange processes can be carried out by treating liquids containing ionic impurities with particles, optionally in emulsion in aqueous media, of cation exchange resin which comprise approximately spherical beads of crosslinked copolymer having diameters of 0.01 to 1.5 micrometers and bearing 0.7 to 1.5 cation exchange functional groups per monomer unit (see fig. 1). The particles may be removed from the treated liquid by flocculation. The particles or emulsions thereof may be made by emulsion polymerization followed by functionalization, in some cases after, in some cases at the same time as, and in some cases without, coagulation of the emulsion polymer to form coagulum particles of the copolymer beads which may, if necessary, be subsequently redispersed in liquids. Emulsions of the strong acid resins and particles of the weak acid resins in the free base form. both as such and in emulsions are also claimed.

    Abstract translation: 阳离子交换处理可以由处理含有带颗粒的离子性杂质，可任选在在wässrige媒体乳液，阳离子交换树脂的包含具有的0点01分至1.5微米适当直径和轴承0.7〜1.5的阳离子交换官能交联共聚物的近似球形的珠的液体来开展 每单体单元的基团。 所述颗粒可从通过絮凝处理的液体被除去。 颗粒或其乳液可以通过乳液聚合随后官能化之后，在相同的时间制成，在一些情况下，在一些情况下，在某些情况下没有，所述乳液聚合物的凝固，形成的共聚物珠粒凝结物颗粒可 如果需要，随后在液体中再分散。 强酸树脂和以游离碱形式的弱酸树脂颗粒的乳液，这两种作为搜索和在乳液因此已声明。

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