公开(公告)号：US3691205A

公开(公告)日：1972-09-12

申请号：US3691205D

申请日：1971-02-09

Applicant: HERWIG HOFFMANN ,  GERHARD JESCHEK ,  ALFRED KUERZINGER ,  ERWIN SCHMIDT ,  WILLIBALD SCHOENLEBEN ,  DIETER VOGES ,  SIEGFRIED WINDERL

Inventor： HOFFMANN HERWIG ,  JESCHEK GERHARD ,  KUERZINGER ALFRED ,  SCHMIDT ERWIN ,  SCHOENLEBEN WILLIBALD ,  VOGES DIETER ,  WINDERL SIEGFRIED

IPC: C07D309/30 ,  C07D7/10

CPC classification number: C07D309/30

Abstract: A process for the production of 6-alkoxy-5,6-dihydro-4H-pyrans by reaction of Alpha , Beta -unsaturated aldehydes with vinyl ethers. The products are valuable intermediates, for example for the production of glutaraldehyde or substituted glutaraldehydes which may be used for example as tanning agents for leather.

公开(公告)号：US4567303A

公开(公告)日：1986-01-28

申请号：US638522

申请日：1984-08-06

Applicant: Guenter Boettger ,  Hans Hammer ,  Otto Hertel ,  Gerhard Jeschek ,  Herbert Mueller ,  Emil Scharf ,  Willibald Schoenleben

Inventor： Guenter Boettger ,  Hans Hammer ,  Otto Hertel ,  Gerhard Jeschek ,  Herbert Mueller ,  Emil Scharf ,  Willibald Schoenleben

IPC: C07C211/10 ,  C07C67/00 ,  C07C209/00 ,  C07C209/16 ,  C07C211/09 ,  C07C211/65 ,  C07C213/00 ,  C07C213/04 ,  C07C215/08 ,  C07C215/14 ,  C07D295/088 ,  C07C65/01

CPC classification number: C07D295/088

Abstract: In preparing or reacting alkanolamines, especially at high temperatures, the use of substantially nickel-free alloy steels prevents corrosion and discoloration.

Abstract translation: 在制备或反应链烷醇胺时，特别是在高温下，使用基本上不含镍的合金钢可防止腐蚀和变色。

公开(公告)号：US5416240A

公开(公告)日：1995-05-16

申请号：US24903

申请日：1993-03-02

Applicant: Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Franz Merger ,  Herbert Mueller

Inventor： Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Franz Merger ,  Herbert Mueller

IPC: C08G65/02 ,  C08G65/08 ,  C08G65/16 ,  C08G65/20 ,  C07C41/01 ,  C07C41/02

CPC classification number: C08G65/20

Abstract: Polyoxyalkylene glycols are prepared by a process in which tetrahydrofuran is polymerized with a total of not more than 95 mol %, based on the amount of tetrahydrofuran used, of one or more comonomers from the group consisting of the cyclic ethers and acetals in the absence of water and in the presence of a monohydric alcohol or of a monocarboxylic acid with the aid of an anhydrous heteropoly acid catalyst, and the polyoxyalkylene glycol is liberated from the resulting polyoxyalkylene glycol monoethers or polyoxyalkylene glycol monoesters by cleavage of the monoether or monoester bond.

Abstract translation: 聚氧亚烷基二醇通过以下方法制备，其中四氢呋喃基于所用四氢呋喃的总量不超过95摩尔％，在不存在共聚单体的情况下聚合来自由环醚和缩醛组成的组中的一种或多种共聚单体 水和一元醇或单羧酸存在下，借助于无水杂多酸催化剂，通过裂解单醚或单酯键，从所得聚氧亚烷基二醇单醚或聚氧亚烷基二醇单酯中释放出聚氧亚烷基二醇。

公开(公告)号：US4775540A

公开(公告)日：1988-10-04

申请号：US33849

申请日：1987-04-03

Applicant: Otto Hertel ,  Gerhard Jeschek ,  Walter Klink ,  Wolfgang Koernig ,  Theodor Weber ,  Fritz Rateike

Inventor： Otto Hertel ,  Gerhard Jeschek ,  Walter Klink ,  Wolfgang Koernig ,  Theodor Weber ,  Fritz Rateike

IPC: A23K1/00 ,  A23K1/16 ,  A61K9/14 ,  A23K1/175

CPC classification number: A61K9/143 ,  A23K20/174 ,  A23K40/10 ,  A61K9/145 ,  Y10S426/807

Abstract: A process for the preparation of pourable choline chloride/silica powders by mixing silica with choline chloride and, where appropriate, drying this mixture, wherein spray-dried or fluidized bed-dried silica which has a particle size of from 30 to 250 .mu.m is mixed with an aqueous choline chloride solution which contains from 70 to 80% by weight, based on the solution, of choline chloride and is at from 40.degree. to 80.degree. C., thereafter from 0.05 to 0.4% by weight, based on the mixture, of magnesium stearate or calcium stearate is added and, if appropriate, the resulting mixture is dried.

Abstract translation: 通过将二氧化硅与氯化胆碱混合并适当地干燥该混合物来制备可倾倒的氯化胆碱/二氧化硅粉末的方法，其中具有30至250μm的粒度的喷雾干燥或流化床干燥的二氧化硅是 与氯化胆碱氯化物溶液混合，该溶液含有70至80重量％的氯化胆碱溶液，为40-80℃，其后为0.05至0.4重量％，基于混合物 ，硬脂酸镁或硬脂酸钙，如果合适，将所得混合物干燥。

公开(公告)号：US5659068A

公开(公告)日：1997-08-19

申请号：US255549

申请日：1994-05-31

Applicant: Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Mueller

Inventor： Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Mueller

IPC: C08G65/08 ,  C08G2/32 ,  C08G65/02 ,  C08G65/16 ,  C08G65/20 ,  C07C41/01 ,  C07C41/02

CPC classification number: C08G65/20

Abstract: Polyoxyalkylene glycol monoesters of carboxylic acids are prepared by a process in which tetrahydrofuran or a mixture of tetrahydrofuran with a total of not more than 95 mol %, based on the amount of tetrahydrofuran used, of one or more comonomers from the group consisting of the cyclic ethers and acetals is polymerized in the absence of water and in the presence of a carboxylic acid and of an anhydrous heteropolyacid catalyst.

Abstract translation: 羧酸的聚氧化亚烷基二醇单酯通过以下方法制备：其中四氢呋喃或四氢呋喃的混合物，总共不超过95摩尔％，基于所用四氢呋喃的一种或多种共聚单体来自由环状 醚和缩醛在不存在水和羧酸和无水杂多酸催化剂的存在下聚合。

公开(公告)号：US5414143A

公开(公告)日：1995-05-09

申请号：US24904

申请日：1993-03-02

Applicant: Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Mueller

Inventor： Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Mueller

IPC: C08G65/08 ,  C08G2/32 ,  C08G65/02 ,  C08G65/16 ,  C08G65/20 ,  C07C41/01 ,  C07C41/02

CPC classification number: C08G65/20

Abstract: Polyoxyalkylene glycol monoethers of monohydric alcohols are prepared by a process in which tetrahydrofuran or a mixture of tetrahydrofuran with a total of not more than 95 mol %, based on the amount of tetrahydrofuran used, of one or more comonomers from the group consisting of the cyclic ethers and acetals is polymerised in the absence of water and in the presence of a monohydric alcohol and of an anhydrous heteropoly acid catalyst.

Abstract translation: 一元醇的聚氧亚烷基二醇单醚通过以下方法制备，其中四氢呋喃或四氢呋喃的混合物，总共不超过95摩尔％，基于所用四氢呋喃的一种或多种共聚单体来自由环状 醚和缩醛在不存在水和在一元醇和无水杂多酸催化剂的存在下聚合。

公开(公告)号：US5951829A

公开(公告)日：1999-09-14

申请号：US809688

申请日：1997-03-27

Applicant: Hans-Jurgen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Muller

Inventor： Hans-Jurgen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Muller

IPC: C08G18/28 ,  C08G63/90 ,  C08G65/30 ,  B01D3/34 ,  C07C41/34 ,  C08G65/10 ,  C08G65/20

CPC classification number: C08G18/28 ,  C08G63/90 ,  C08G65/30

Abstract: A method of separating heteropoly compounds from mixtures of polyethers, polyesters and/or polyether esters, a protic component and heteropoly compounds, wherein the protic component is removed from the mixture and subsequently separating off the heteropoly compound as a separate phase. The polymer phase which remains is preferably brought into further contact with a solid adsorbent that is capable of adsorbing heteropoly compounds.

Abstract translation: PCT No.PCT / EP95 / 03955 371日期1997年3月27日 102（e）1997年3月27日PCT PCT 1995年10月6日PCT公布。 出版物WO96 / 11221 日期1996年04月18日从聚醚，聚酯和/或聚醚酯的混合物中分离杂多化合物的方法，质子成分和杂多化合物，其中将质子成分从混合物中除去，随后将杂多化合物分离出来， 。 保留的聚合物相优选与能够吸附杂多化合物的固体吸附剂进一步接触。

公开(公告)号：US5714638A

公开(公告)日：1998-02-03

申请号：US381733

申请日：1995-02-01

Applicant: Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Mueller

Inventor： Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Mueller

IPC: C08G65/08 ,  C08G2/32 ,  C08G65/02 ,  C08G65/16 ,  C08G65/20 ,  C07C41/01 ,  C07C41/02

CPC classification number: C08G65/20

Abstract: Polyoxyalkylene glycol monoethers of monohydric alcohols are prepared by a process in which tetrahydrofuran or a mixture of tetrahydrofuran with a total of not more than 95 mol %, based on the amount of tetrahydrofuran used, of one or more comonomers from the group consisting of the cyclic ethers and acetals is polymerized in the absence of water and in the presence of a monohydric alcohol and of an anhydrous heteropoly acid catalyst.

Abstract translation: 一元醇的聚氧亚烷基二醇单醚通过以下方法制备，其中四氢呋喃或四氢呋喃的混合物，总共不超过95摩尔％，基于所用四氢呋喃的一种或多种共聚单体来自由环状 醚和缩醛在不存在水和在一元醇和无水杂多酸催化剂的存在下聚合。

公开(公告)号：US5395959A

公开(公告)日：1995-03-07

申请号：US110297

申请日：1993-08-20

Applicant: Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Mueller

Inventor： Hans-Juergen Weyer ,  Rolf Fischer ,  Gerhard Jeschek ,  Herbert Mueller

IPC: C08G65/04 ,  C08G65/00 ,  C08G65/02 ,  C08G65/08 ,  C08G65/20 ,  C07C69/02

CPC classification number: C08G65/00 ,  C08G65/20

Abstract: The average molecular weight of polyoxyalkylene glycols and polyoxyalkylene glycol derivatives is adjusted in the heteropolyacid-catalyzed polymerization of cyclic ethers and/or acetals with ring cleavage in the presence of proton donors by a process in which the amount of the relevant proton donor present in the reaction system is regulated in the course of the reaction by the measurement of the electrical conductivity.

Abstract translation: 聚合氧亚烷基二醇和聚氧化亚烷基二醇衍生物的平均分子量在质子供体存在下，通过环状醚和/或缩醛环进行杂多酸催化聚合来调节，其中存在于 通过测量电导率，在反应过程中调节反应体系。

公开(公告)号：US5099074A

公开(公告)日：1992-03-24

申请号：US603519

申请日：1990-10-26

Applicant: Herbert Mueller ,  Gerhard Jeschek ,  Rolf Fischer ,  Hans-Juergen Weyer

Inventor： Herbert Mueller ,  Gerhard Jeschek ,  Rolf Fischer ,  Hans-Juergen Weyer

IPC: C08G65/16 ,  C08G65/20

CPC classification number: C08G65/20

Abstract: A process for the preparation of polyether glycols by polymerization of tetrahydrofuran or copolymerization of tetrahydrofuran with oxiranes in the presence of from 20 to 500% w/w of a hydrocarbon, based on the weight of tetrahydrofuran used.

Abstract translation: 基于所用四氢呋喃的重量，通过四氢呋喃聚合制备聚醚二醇的方法或四氢呋喃与环氧乙烷在20-500％w / w烃存在下共聚合的方法。