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    Method of applying high pressures to a high pressure assembly
    91.
    发明授权
    Method of applying high pressures to a high pressure assembly 失效
    向高压组件施加高压的方法

    公开(公告)号：US07540075B2

    公开(公告)日：2009-06-02

    申请号：US11211140

    申请日：2005-08-24

    Applicant: Chien-Min Sung

    Inventor： Chien-Min Sung

    IPC: B23P11/00 ,  B28B3/00

    CPC classification number: B01J3/065 ,  B01J3/067 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B30B11/004 ,  B30B11/007 ,  Y10T29/49826 ,  Y10T29/49863 ,  Y10T29/49998 ,  Y10T29/51

    Abstract: An improved high pressure apparatus can include a plurality of complementary die segments. The die segments can have inner surfaces which are shaped to form a die chamber upon assembly of the die segments. A pair of anvils can be oriented such that an anvil is at each end of the die chamber. To prevent the die segments from being forced apart during movement of the anvils, force members can be connected to the die segments. The force members can apply discrete forces to the die segments sufficient to retain the die segments in substantially fixed positions relative to each other during application of force by the pair of anvils. Using such a high pressure apparatus can achieve pressures as high as 10 GPa with improved useful die life and larger reaction volumes.

    Abstract translation: 改进的高压装置可以包括多个互补的模片段。 模具段可以具有内表面，其在模具段的组装时成形为形成模腔。 一对砧座可以被定向成使得砧座在模腔的每个端部。 为了防止模具段在砧座移动期间被迫分开，可以将力构件连接到模具段。 力构件可以向模具段施加离散的力，足以在由一对砧施加力期间将模具段保持在相对于彼此的基本上固定的位置。 使用这种高压装置可以实现高达10GPa的压力，并且具有改善的有用的模具寿命和较大的反应体积。

    Polycrystalline diamond materials formed from coarse-sized diamond grains
    93.
    发明授权
    Polycrystalline diamond materials formed from coarse-sized diamond grains 有权
    由粗大的金刚石颗粒形​​成的多晶金刚石材料

    公开(公告)号：US06951578B1

    公开(公告)日：2005-10-04

    申请号：US09637092

    申请日：2000-08-10

    Applicant: Daniel J. Belnap ,  Nathan R. Anderson ,  Zhigang Fang ,  Anthony Griffo ,  Brian A. White

    Inventor： Daniel J. Belnap ,  Nathan R. Anderson ,  Zhigang Fang ,  Anthony Griffo ,  Brian A. White

    IPC: B01J3/06 ,  C22C26/00 ,  E21B10/52 ,  B32B9/00

    CPC classification number: E21B10/52 ,  B01J3/065 ,  B01J2203/062 ,  C22C26/00

    Abstract: PCD materials of this invention comprise diamond crystals that are bonded together with a catalyst/binder material. The PCD material is prepared by combining diamond grains with a catalyst/binder material either as a premixture or by infiltration during sintering. The PCD material comprises 15 percent by volume or less diamond grains sized 20 micrometers or less. The diamond grains are pressurized under elevated temperature conditions to form the desired PCD material. PCD materials of this invention can constitute the exclusive material phase of a PCD construction, or can form one or more material phase in a multi-phase material microstructure, wherein the multiple material phase can be arranged in an ordered/oriented or random fashion. PCD materials of this invention display improved properties of impact and fatigue resistance, and functional toughness, when used in complex wear environments, when compared to conventional PCs materials comprising intentionally added fine-sized diamond grains.

    Abstract translation: 本发明的PCD材料包括与催化剂/粘合剂材料结合在一起的金刚石晶体。 通过将金刚石晶粒与催化剂/粘合剂材料组合作为预混合物或通过在烧结期间的渗透来制备PCD材料。 PCD材料包括15微摩尔或更小的15体积％或更少的金刚石颗粒。 金刚石晶粒在高温条件下被加压以形成所需的PCD材料。 本发明的PCD材料可以构成PCD结构的独特材料相，或者可以在多相材料微结构中形成一个或多个材料相，其中多个材料相可以以有序/定向或随机的方式布置。 当与常规的包含有意添加的精细尺寸的金刚石颗粒的材料相比时，本发明的PCD材料在复杂的磨损环境中使用时显示改善的冲击和抗疲劳性能以及功能性韧性。

    High pressure apparatus having transition slope binding ring that mitigates tensile stresses and corresponding method
    95.
    发明授权
    High pressure apparatus having transition slope binding ring that mitigates tensile stresses and corresponding method 有权
    具有缓和拉伸应力的过渡边缘结合环的高压装置和相应的方法

    公开(公告)号：US06375446B1

    公开(公告)日：2002-04-23

    申请号：US09740777

    申请日：2000-12-19

    Applicant: Robert V. Leonelli, Jr.

    Inventor： Robert V. Leonelli, Jr.

    IPC: B30B1102

    CPC classification number: B30B11/004 ,  B01J3/065 ,  B01J3/067

    Abstract: A belt/die, pre-tensioned loaded windings, or other high-pressure apparatus has a series of annular rings for confining material being subjected to high-pressure treatment. The series of annular rings has an inner annular ring having an inner upper edge, an outer upper edge, an inner lower edge, and an outer lower edge. The inner lower edge is chamfered at an angle of greater than about 60° from the vertical in order to create a transition slope that mitigates tensile stresses.

    Abstract translation: 带/模，预张紧的绕组或其它高压装置具有一系列用于限制材料经受高压处理的环形圈。 一系列环形环具有内环形环，其具有内上边缘，外上边缘，内下边缘和外下边缘。 内部下边缘以与垂直方向大于约60°的角度进行倒角，以产生减轻拉伸应力的过渡斜率。

    Supported polycrystalline compacts having improved physical properties and method for making same
    96.
    发明授权
    Supported polycrystalline compacts having improved physical properties and method for making same 失效
    具有改善的物理性能的支撑多晶压块及其制造方法

    公开(公告)号：US5512235A

    公开(公告)日：1996-04-30

    申请号：US239156

    申请日：1994-05-06

    Applicant: David B. Cerutti ,  Henry S. Marek

    Inventor： David B. Cerutti ,  Henry S. Marek

    IPC: C04B41/87 ,  B01J3/06 ,  B22F3/14 ,  B22F7/02

    CPC classification number: B01J3/062 ,  B01J3/065 ,  B01J2203/062 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0685 ,  Y10T428/12056 ,  Y10T428/26 ,  Y10T428/30 ,  Y10T428/31678

    Abstract: Supported polycrystalline compacts having improved shear strength, impact, and fracture toughness properties, and methods for making the same under high temperature/high pressure (HT/HP) processing conditions. The method involves a HT/HP apparatus formed of a generally cylindrical reaction cell assembly having an inner chamber of predefined axial and radial extents and containing pressure transmitting medium, and a charge assembly having axial and radial surfaces and formed of at least one sub-assembly comprising a mass of crystalline particles adjacent a metal carbide support layer. The charge assembly is disposed within the chamber of the reaction cell assembly, with the pressure transmitting medium being interposed between the axial and radial surfaces of the charge assembly and the extents of the reaction cell chamber to define an axial pressure transmitting medium thickness, L.sub.h, and a radial pressure transmitting medium thickness, L.sub.r, the ratio of which, L.sub.h /L.sub.r being selected as less than 1. The reaction cell assembly containing the charge assembly then is subjected to HT/HP conditions selected as effective to sinter the crystalline particles into a polycrystalline compact layer and to bond the polycrystalline compact layer at an interface to the metal carbide support layer for forming a metal carbide supported polycrystalline compact. The supported compact is characterized as having an essentially constant or increasing residual compressive stress on the surface of its compact layer as portions of a predefined thickness, W, of its support layer, as measured from the interfaced, are incrementally removed.

    Abstract translation: 具有改进的剪切强度，冲击和断裂韧性性能的支撑多晶压块及其在高温/高压（HT / HP）加工条件下制备该多晶压块的方法。 该方法包括由具有预定的轴向和径向范围的内室并包含压力传递介质的大致圆柱形的反应池组件形成的HT / HP设备，以及具有轴向和径向表面并由至少一个子组件形成的电荷组件 包括邻近金属碳化物支撑层的大量结晶颗粒。 电荷组件设置在反应池组件的腔室内，压力传递介质介于电荷组件的轴向和径向表面之间以及反应室室的范围，以限定轴向压力传递介质厚度Lh， 和径向压力传递介质厚度Lr，其比例Lh / Lr被选择为小于1.然后将含有电荷组件的反应池组件经受选择为有效地将结晶颗粒烧结的HT / HP条件 多晶致密层并且在与金属碳化物支撑层的界面处结合多晶致密层以形成金属碳化物负载的多晶结构体。 支撑的压实体的特征在于在其紧密层的表面上具有基本恒定或增加的残余压应力，因为从界面测量的其支撑层的预定厚度W的部分被递增地移除。

    High pressure reaction vessel
    98.
    发明授权
    High pressure reaction vessel 失效
    高压反应釜

    公开(公告)号：US5236674A

    公开(公告)日：1993-08-17

    申请号：US826809

    申请日：1992-01-28

    Applicant: Robert H. Frushour

    Inventor： Robert H. Frushour

    IPC: B01J3/06

    CPC classification number: B01J3/065 ,  B01J3/06

    Abstract: A high pressure reaction vessel includes an inner bushing surrounding a reaction charge. The inner bushing is formed of at least one material having a low shear strength that undergoes a polymorphic phase change to a more dense phase within the operating pressure range of the reaction vessel. The bushing may be formed of at least two low shear strength materials with one of the materials undergoing polymorphic phase change to a more dense phase. The one of the two materials which undergoes a polymorphic phase change forms between 10% and 90% of the total volume of the inner bushing. In another embodiment, a pressure transmitting media and an electrical resistance heater tube are concentrically arranged within the inner bushing. The pressure transmitting media is formed of a low shear strength material that undergoes a polymorphic phase change to a more dense phase. In both embodiments, the low shear strength material undergoing polymorphic phase change is potassium bromide.

    Abstract translation: 高压反应容器包括围绕反应装料的内衬套。 内衬套由至少一种具有低剪切强度的材料形成，该材料在反应容器的操作压力范围内经历多晶相转变为更致密相。 衬套可以由至少两种低剪切强度材料形成，其中材料之一经历多晶相转变为更致密的相。 经历多晶相变的两种材料之一形成内衬套总体积的10％至90％。 在另一个实施例中，压力传递介质和电阻加热器管同心地布置在内衬套内。 压力传递介质由经受多相态变为更致密相的低剪切强度材料形成。 在两个实施方案中，经历多晶型相变的低剪切强度材料是溴化钾。

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