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    Enzymatically and hydrolytically stable resins, resin monomers, and resin composites for use in dental preventive and restorative applications
    11.
    发明授权
    Enzymatically and hydrolytically stable resins, resin monomers, and resin composites for use in dental preventive and restorative applications 有权
    酶和水解稳定性树脂，树脂单体和树脂复合材料，用于牙科预防和修复应用

    公开(公告)号：US09572753B2

    公开(公告)日：2017-02-21

    申请号：US14660466

    申请日：2015-03-17

    Applicant: ADA Foundation

    Inventor： Jirun Sun ,  Rafael Lee Bowen

    IPC: C08L33/08 ,  A61K6/083

    CPC classification number: A61K6/083 ,  A61K6/0835 ,  C08L33/08

    Abstract: A composition of matter includes one or more functionalized vinylbenzyl components of the formula covalently connected to one or more R functional components; the one or more R functional groups selected from a group including one or more hydroxyl methyl (—CHOH—) moieties and/or derivatives thereof, one or more ethoxy (—CH2—CH2—O—) moieties and/or derivatives thereof, and one or more benzene (C6H6) and/or derivatives thereof; and ether links that connect the functionalized vinylbenzyl components and the R functional components.

    Abstract translation: 其中n是等于或大于1的整数，其共价连接到一个或多个R官能组分; 一个或多个选自包括一个或多个羟基甲基（-CHOH-）部分和/或其衍生物，一个或多个乙氧基（-CH 2 -CH 2 -O-）部分和/或其衍生物的基团的R官能团，以及 一种或多种苯衍生物; 和连接官能化乙烯基苄基组分和R官能组分的醚连接。

    ELECTRON PARMAGNETIC RESONANCE DOSIMETER, METHODS OF MANUFACTURE, AND METHODS OF USE
    13.
    发明申请
    ELECTRON PARMAGNETIC RESONANCE DOSIMETER, METHODS OF MANUFACTURE, AND METHODS OF USE 审中-公开

    公开(公告)号：US20190285714A1

    公开(公告)日：2019-09-19

    申请号：US16431872

    申请日：2019-06-05

    Applicant: ADA Foundation

    Inventor： Laurence C. Chow ,  Shozo Takagi ,  Marc Frederic Desrosiers

    IPC: G01R33/60 ,  G01T1/04 ,  G01N24/10 ,  A61B6/10

    Abstract: An electron paramagnetic resonance device includes a crystalline, emission-sensitive mass and a housing containing the device. The mass includes structurally incorporated carbonate content in a range of about 3% by weight to about 10% by weight of the mass, one or more structurally incorporated non-calcium metallic cations, and one or more structurally incorporated phosphate anions. When irradiated with a known source, the EPR device may function as a reference. When unirradiated, the EPR may function as a dosimeter. As a dosimeter, the EPR device may be used as a personal dosimeter or as a monitor for inanimate objects being subjected to radiation sources. The EPR dosimeter may be used for both gamma radiation and neutron radiation measurements.

    Enzymatically and hydrolytically stable dental preventive and restorative systems
    14.
    发明授权
    Enzymatically and hydrolytically stable dental preventive and restorative systems 有权

    公开(公告)号：US10231906B2

    公开(公告)日：2019-03-19

    申请号：US15345733

    申请日：2016-11-08

    Applicant: ADA Foundation

    Inventor： Jirun Sun ,  Rafael Bowen

    IPC: C08L33/08 ,  A61K6/083

    Abstract: A composition of matter includes one or more functionalized vinylbenzyl components of the formula wherein n is an integer equal to or greater than 1 covalently connected to one or more R functional components; the one or more R functional groups selected from a group including one or more hydroxyl methyl (—CHOH—) moieties and/or derivatives thereof, one or more ethoxy (—CH2—CH2—O—) moieties and/or derivatives thereof, and one or more benzene derivatives; and ether links that connect the functionalized vinylbenzyl components and the R functional components.

    Multi-functional self-healing dental composites, methods of synthesis and methods of use
    15.
    发明授权
    Multi-functional self-healing dental composites, methods of synthesis and methods of use 有权

    公开(公告)号：US09931281B2

    公开(公告)日：2018-04-03

    申请号：US14952492

    申请日：2015-11-25

    Applicant: ADA Foundation

    Inventor： Jirun Sun

    IPC: A61K6/083 ,  A61K6/00

    CPC classification number: A61K6/083 ,  A61K6/0052 ,  A61K6/0091 ,  A61K6/0038 ,  C08L33/08 ,  A61K6/0835

    Abstract: A multi-functional self-healing dental composite may intrinsically repair the micro-crack and prevent the crack from propagating to catastrophic failure, thus significantly extending the service life of the restorative material. The self-healing dental composite includes a dental resin matrix, fillers, healing powder, and healing liquid containing micro-capsules distributed throughout the matrix. Each of the micro-capsules have a silica she formed by the hydrolysis condensation of TEOS in the presence of an aqueous solution of a healing liquid. The healing liquid includes a homo-polymers(s) and/or copolymer(s) of carboxylic acid(s). The healing powder particles distributed throughout the resin matrix, and include alumina, silica and other elements. The self-healing may be triggered automatically as a result of micro-cracking, induced by thereto/mechanical fatigue. During the self-healing process, antibacterial agents may be released to provide protection of the composites against cariogenic bacteria. The self-healing dental composites also may improve tooth remineralization, and caries prevention though fluoride release.

    Dental and endodontic filling materials and methods
    17.
    发明授权
    Dental and endodontic filling materials and methods 有权

    公开(公告)号：US09668825B2

    公开(公告)日：2017-06-06

    申请号：US14805137

    申请日：2015-07-21

    Applicant: ADA Foundation

    Inventor： Laurence C. Chow ,  Shozo Takagi

    IPC: A61K6/08 ,  A61C5/04 ,  A61K6/00

    CPC classification number: A61C5/50 ,  A61K6/0038

    Abstract: Disclosed are endodontic filling materials and methods. A method for filling a dental root canal may include providing a hydrosetting filling material and inserting the hydrosetting filling material into the dental root canal, the material setting in the root canal to form a biocompatible filling. The hydrosetting filling material comprises a hydrogel former and a filler. The hydrogel former is at least one of a reactive organic hydrogel formers, an inorganic hydrogel formers, and a non-reactive organic hydrogel formers, and the filler is at least one of a self-hardening and a non-hardening filler. Plural filling material precursor compositions that collectively contain hydrogel formers and fillers may be provided.

    ELECTRON PARAMAGNETIC RESONANCE DOSIMETER, METHODS OF MANUFACTURE, AND METHODS OF USE
    19.
    发明申请
    ELECTRON PARAMAGNETIC RESONANCE DOSIMETER, METHODS OF MANUFACTURE, AND METHODS OF USE 审中-公开
    电子参比共振剂量计，制造方法和使用方法

    公开(公告)号：US20160266226A1

    公开(公告)日：2016-09-15

    申请号：US15068943

    申请日：2016-03-14

    Applicant: ADA Foundation

    Inventor： Laurence C. Chow ,  Shozo Takagi ,  Marc Frederic Desrosiers

    IPC: G01R33/60 ,  A61B5/00

    Abstract: A dosimeter for EPR dosimetry systems includes a carbonated hydroxyapatite cement formed by mixing a cement powder and a cement liquid in a ratio of a range of about 0.5 to 5.0 powder-to-liquid ratio. The cement powder includes one or more calcium phosphate compounds and one or more carbonate compounds. The cement liquid includes a sodium phosphate solution. The cement, when irradiated by a radiation source, is capable of producing a measurable signal as a spectrally clean EPR spectrum. Furthermore, the measurable signal is proportional to the received radiation dose

    Abstract translation: 用于EPR剂量测定系统的剂量计包括通过以约0.5至5.0的粉末与液体比的比例混合水泥粉末和水泥液体而形成的碳酸羟基磷灰石水泥。 水泥粉末包括一种或多种磷酸钙化合物和一种或多种碳酸酯化合物。 水泥液体包括磷酸钠溶液。 水泥当被辐射源照射时，能够产生可测量的信号作为光谱干净的EPR光谱。 此外，可测量的信号与接收的辐射剂量成比例

    MULTI-FUNCTIONAL SELF-HEALING DENTAL COMPOSITES, METHODS OF SYNTHESIS AND METHODS OF USE
    20.
    发明申请
    MULTI-FUNCTIONAL SELF-HEALING DENTAL COMPOSITES, METHODS OF SYNTHESIS AND METHODS OF USE 审中-公开
    多功能自愈牙齿复合材料，合成方法及使用方法

    公开(公告)号：US20160193119A1

    公开(公告)日：2016-07-07

    申请号：US14952492

    申请日：2015-11-25

    Applicant: ADA Foundation

    Inventor： Jirun Sun

    IPC: A61K6/083 ,  A61K6/00

    CPC classification number: A61K6/083 ,  A61K6/0052 ,  A61K6/0091 ,  A61K6/0038 ,  C08L33/08 ,  A61K6/0835

    Abstract: A multi-functional self-healing dental composite may intrinsically repair the micro-crack and prevent the crack from propagating to catastrophic failure, thus significantly extending the service life of the restorative material. The self-healing dental composite includes a dental resin matrix, fillers, healing powder, and healing liquid containing micro-capsules distributed throughout the matrix. Each of the micro-capsules have a silica she formed by the hydrolysis condensation of TEOS in the presence of an aqueous solution of a healing liquid. The healing liquid includes a homo-polymers(s) and/or copolymer(s) of carboxylic acid(s). The healing powder particles distributed throughout the resin matrix, and include alumina, silica and other elements. The self-healing may be triggered automatically as a result of micro-cracking, induced by thereto/mechanical fatigue. During the self-healing process, antibacterial agents may be released to provide protection of the composites against cariogenic bacteria. The self-healing dental composites also may improve tooth remineralization, and caries prevention though fluoride release.

    Abstract translation: 多功能自愈牙科复合材料可以固有地修复微裂纹，防止裂纹传播到灾难性故障，从而显着延长修复材料的使用寿命。 自愈牙科复合材料包括牙科树脂基质，填充剂，愈合粉末和包含分布在整个基质中的微胶囊的愈合液。 每个微胶囊都具有通过TEOS在愈合液体的水溶液存在下水解缩合形成的二氧化硅。 愈合液体包括一种或多种羧酸的均聚物和/或共聚物。 愈合粉末颗粒分布在整个树脂基体上，包括氧化铝，二氧化硅等元素。 由于由其引起的微裂纹或机械疲劳，自愈可自动触发。 在自愈过程中，可以释放抗菌剂以提供复合材料对致龋细菌的保护。 自愈牙科复合材料还可以改善牙齿再矿化，并且通过氟化物释放来预防龋齿。

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