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    Telechelic polystyrene/polyethylene copolymers and processes for making same
    11.
    发明授权
    Telechelic polystyrene/polyethylene copolymers and processes for making same 失效
    聚酯/聚乙烯共聚物及其制备方法

    公开(公告)号：US5849847A

    公开(公告)日：1998-12-15

    申请号：US681805

    申请日：1996-07-29

    Applicant: Roderic P. Quirk

    Inventor： Roderic P. Quirk

    IPC: C08F4/46 ,  C08F4/72 ,  C08F110/02 ,  C08F212/06 ,  C08F297/02

    CPC classification number: C08F297/02 ,  C08F110/02 ,  C08F212/06 ,  C08F4/461

    Abstract: Polyalkenylaromatic-polyethylene copolymers are prepared using protected functional organolithium initiators. Polymerization of an alkenylsubstituted aromatic monomer followed by ethylene, results in a protected functional block polystyrene-co-polyethylenyllithium. Termination with a functionalizing agent followed by deprotection produces polymeric products with high functionalization at the initiating chain-end and at least partial functionalization at the terminal chain-end.

    Abstract translation: 使用保护的官能的有机锂引发剂制备聚烯基芳族聚乙烯共聚物。 烯基取代的芳族单体随后是乙烯的聚合得到保护的官能嵌段聚苯乙烯 - 共 - 聚乙烯基锂。 用官能化剂终止脱保护后，在起始链末端产生具有高官能度的聚合产物，并在末端链末端产生至少部分功能化。

    Compatibilization of polymer blends
    12.
    发明授权
    Compatibilization of polymer blends 失效
    聚合物共混物的增容

    公开(公告)号：US5264491A

    公开(公告)日：1993-11-23

    申请号：US935650

    申请日：1992-08-26

    Applicant: Roderic P. Quirk

    Inventor： Roderic P. Quirk

    IPC: C08G63/00 ,  C08G63/181 ,  C08G63/20

    CPC classification number: C08G63/00

    Abstract: Compatibilizing agents suitable for blending otherwise immiscible polymers comprise a block or graft copolymer in which at least one of the block segments is formed by a living anionic polymerization and thereafter chemically converted to provide a polymer having at least one functional end group. The functional groups of the polymer blocks thus formed are reacted with a functionalized monomer, or an oligomer to provide a second block polymer segment. Compatibilizing agents containing more than two blocks may be formed in similar fashion. The compatibilizing agents are used to provide uniform blends of polar and non-polar polymers having superior uniformity and other physical properties.

    Abstract translation: 适用于混合其它不混溶性聚合物的相容剂包括嵌段或接枝共聚物，其中至少一个嵌段链段通过活性阴离子聚合形成，然后化学转化成提供具有至少一个官能端基的聚合物。 由此形成的聚合物嵌段的官能团与官能化单体或低聚物反应以提供第二嵌段聚合物链段。 含有多于两个嵌段的相容剂可以以类似的方式形成。 相容剂用于提供具有优异均匀性和其它物理性质的极性和非极性聚合物的均匀共混物。

    Triblock polymers of a monovinyl aromatic compound and myrcene
    14.
    发明授权
    Triblock polymers of a monovinyl aromatic compound and myrcene 失效
    单乙烯基芳族化合物和月桂烯的三嵌段聚合物

    公开(公告)号：US4374957A

    公开(公告)日：1983-02-22

    申请号：US316299

    申请日：1981-10-29

    Applicant: Roderic P. Quirk

    Inventor： Roderic P. Quirk

    IPC: C08F297/04

    CPC classification number: C08F297/04

    Abstract: A tacky thermoplastic elastomeric linear triblock polymer corresponding to the formula A-B-A is made from a monovinyl aromatic hydrocarbon and myrcene. A is a polymer block of a monovinyl aromatic hydrocarbon, e.g. styrene, having an average molecular weight between 2,000 and 100,000 and a glass transition temperature above 25.degree. C. B is a polymeric block of myrcene (7-methyl-3-methylene-1,6-octadiene, C.sub.10 H.sub.16) having an average molecular weight between 10,000 and 1,000,000 and a glass transition temperature below -40.degree. C. B constitutes from 40 to 80 percent of the total. The products are made by sequential polymerization with an organolithium initiator.

    Abstract translation: 对应于式A-B-A的粘性热塑性弹性线性三嵌段聚合物由单乙烯基芳族烃和月桂烯制成。 A是单乙烯基芳族烃的聚合物嵌段，例如 苯乙烯，平均分子量在2,000和100,000之间，玻璃化转变温度高于25℃。B是具有平均分子量的月桂烯（7-甲基-3-亚甲基-1,6-辛二烯，C10H16）的聚合物嵌段 10,000至1,000,000之间，玻璃化转变温度低于-40℃.B占总量的40％至80％。 产物通过与有机锂引发剂的顺序聚合制备。

    Synthetic polymers with highly-functionalized liquid-rubber chain-end moieties
    15.
    发明授权
    Synthetic polymers with highly-functionalized liquid-rubber chain-end moieties 有权
    具有高官能化液体 - 橡胶链端部分的合成聚合物

    公开(公告)号：US07235615B2

    公开(公告)日：2007-06-26

    申请号：US10782432

    申请日：2004-02-18

    Applicant: Roderic P. Quirk ,  Jin-Ping Zhou

    Inventor： Roderic P. Quirk ,  Jin-Ping Zhou

    IPC: C08F4/48 ,  C08F36/06

    CPC classification number: C08F297/04 ,  C08C19/30 ,  C08C19/44 ,  C08F8/00 ,  C08F297/02 ,  C08F12/08

    Abstract: A method is provided for synthesizing a polymer that has highly-functionalized chain-end moieties. The method functionalizes liquid rubber to terminate a metallic or organometallic initiated living polymer. After the living polymer has been terminated with the functionalized liquid rubber, the functionalities on the residue of the liquid rubber are preferably modified to yield more advantageous functionalities.

    Abstract translation: 提供了一种合成具有高度官能化的链端部分的聚合物的方法。 该方法使液体橡胶功能化以终止金属或有机金属引发的活性聚合物。 活性聚合物用功能化液体橡胶终止后，液态橡胶残余物的功能性被优选地改性以产生更有利的功能。

    Star polymers from mixed initiators
    16.
    发明授权
    Star polymers from mixed initiators 失效
    混合引发剂的星形聚合物

    公开(公告)号：US5798418A

    公开(公告)日：1998-08-25

    申请号：US683487

    申请日：1996-07-18

    Applicant: Roderic P. Quirk

    Inventor： Roderic P. Quirk

    IPC: C08C19/44 ,  C08F4/46 ,  C08F4/72 ,  C08F12/06 ,  C08F36/04 ,  C08F297/04 ,  C08G81/02 ,  C08G83/00 ,  C08F6/00

    CPC classification number: C08G83/00 ,  C08C19/44 ,  C08F12/06 ,  C08F297/044 ,  C08F36/04 ,  C08F4/461 ,  C08F4/72 ,  C08G81/022

    Abstract: The present invention provides novel, multi-arm or star-shaped polymers having mixed protected functional and non-functional ends, their optionally hydrogenated analogues, and the polymers produced by removal of the protecting groups. The invention also provides a process for the preparation of novel multi-arm or star-shaped polymers having branched-end functionality on some, but not all, of the branches. The multi-arm or star polymers of this invention are produced from more than one type of initiator, i.e., from both functional and non-functional initiators which, by design, incorporates both desired physical properties associated with multi-arm or star polymers with non-functional branch-ends and the versatility of functional branch end multi-arm or star polymers.

    Abstract translation: 本发明提供具有混合保护的官能和非官能末端的新型多臂或星形聚合物，它们任选氢化的类似物，以及通过除去保护基产生的聚合物。 本发明还提供了一种制备新颖的多臂或星形聚合物的方法，其在一些但不是全部的分支上具有支链官能团。 本发明的多臂或星形聚合物由多于一种类型的引发剂生产，即从功能性和非功能性引发剂两者产生，其通过设计将包含与多臂或星形聚合物相关的所需物理性能与非 - 功能分支端和功能性分支端多臂或星形聚合物的多功能性。

    Hetero-telechelic polymers and processes for making same
    18.
    发明授权
    Hetero-telechelic polymers and processes for making same 失效
    杂环聚合物和制备相同的方法

    公开(公告)号：US06703446B2

    公开(公告)日：2004-03-09

    申请号：US10176816

    申请日：2002-06-21

    Applicant: James A. Schwindeman ,  Robert J. Letchford ,  Conrad W. Kamienski ,  Roderic P. Quirk

    Inventor： James A. Schwindeman ,  Robert J. Letchford ,  Conrad W. Kamienski ,  Roderic P. Quirk

    IPC: C08F29704

    CPC classification number: C08F36/04 ,  C08C19/44 ,  C08F4/46 ,  C08F4/48 ,  C08F4/72 ,  C08F8/34 ,  C08F12/04 ,  C08F2810/40 ,  C08F112/08

    Abstract: Hetero-telechelic polymers having the formula: FG—(Q)d—Z—J—[A(R1R2R3)]x  (I) wherein FG is a protected or non-protected functional group; Q is a saturated or unsaturated hydrocarbyl group derived by incorporation of a compound selected from the group consisting of conjugated diene hydrocarbons, alkenylsubstituted aromatic hydrocarbons, and mixtures thereof; d is an integer from 10 to 200; Z is a branched or straight chain hydrocarbon group which contains 3-25 carbon atoms, optionally containing aryl or substituted aryl groups; J is oxygen, sulfur, or nitrogen; [A(R1R2R3)]x is a protecting group, wherein A is an element selected from Group IVa of the Periodic Table of Elements; R1, R2, and R3 are each independently selected from the group consisting of hydrogen, alkyl, substituted alkyl groups containing lower alkyl, lower alkylthio, and lower dialkylamino groups, aryl or substituted aryl groups containing lower alkyl, lower alkylthio, and lower dialkylamino groups, and cycloalkyl and substituted cycloalkyl containing 5 to 12 carbon atoms; and x is dependent on the valence of J and varies from one when J is oxygen or sulfur to two when J is nitrogen, with the proviso J and FG are not the same, and processes for making the same.

    Abstract translation: 具有下式的异烟酰基聚合物：其中FG是被保护或未被保护的官能团; Q是通过引入选自共轭二烯烃，烯基取代的芳族烃及其混合物的化合物衍生的饱和或不饱和烃基; d为10〜200的整数; Z是含有3-25个碳原子的支链或直链烃基，任选含有芳基或取代的芳基; J是氧，硫或氮; [A（R 1 R 2 R 3）] x是保护基，其中A是选自元素周期表Ⅳa族的元素; R 1，R 2和R 3各自独立地选自氢，烷基，含有低级烷基，低级烷硫基和低级二烷基氨基的取代烷基，含低级烷基的低级烷基 烷基，低级烷硫基和低级二烷基氨基，环烷基和取代环烷基，含有5至12个碳原子; 并且x取决于J的化合价，并且当J是氮时，当J是氧或硫时，J的值是不同的，条件是J和FG不相同，并且其制备方法。

    Hetero-telechelic polymers and processes for making same
    20.
    发明授权
    Hetero-telechelic polymers and processes for making same 失效

    公开(公告)号：US06699939B2

    公开(公告)日：2004-03-02

    申请号：US10176723

    申请日：2002-06-21

    Applicant: James A. Schwindeman ,  Robert J. Letchford ,  Conrad W. Kamienski ,  Roderic P. Quirk

    Inventor： James A. Schwindeman ,  Robert J. Letchford ,  Conrad W. Kamienski ,  Roderic P. Quirk

    IPC: C08F29704

    CPC classification number: C08F36/04 ,  C08C19/44 ,  C08F4/46 ,  C08F4/48 ,  C08F4/72 ,  C08F8/34 ,  C08F12/04 ,  C08F2810/40 ,  C08F112/08

    Abstract: Hetero-telechelic polymers having the formula: FG—(Q)d—Z—J—[A(R1R2R3)]x  (I) wherein FG is a protected or non-protected functional group; Q is a saturated or unsaturated hydrocarbyl group derived by incorporation of a compound selected from the group consisting of conjugated diene hydrocarbons, alkenylsubstituted aromatic hydrocarbons, and mixtures thereof; d is an integer from 10 to 200; Z is a branched or straight chain hydrocarbon group which contains 3-25 carbon atoms, optionally containing aryl or substituted aryl groups; J is oxygen, sulfur, or nitrogen; [A(R1R2R3)]x is a protecting group, wherein A is an element selected from Group IVa of the Periodic Table of Elements; R1, R2, and R3 are each independently selected from the group consisting of hydrogen, alkyl, substituted alkyl groups containing lower alkyl, lower alkylthio, and lower dialkylamino groups, aryl or substituted aryl groups containing lower alkyl, lower alkylthio, and lower dialkylamino groups, and cycloalkyl and substituted cycloalkyl containing 5 to 12 carbon atoms; and x is dependent on the valence of J and varies from one when J is oxygen or sulfur to two when J is nitrogen, with the proviso J and FG are not the same, and processes for making the same.

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