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公开(公告)号：US20150315343A1
公开(公告)日：2015-11-05
申请号：US14427012
申请日：2013-09-19
Applicant: BASF SE
Inventor： Norbert Eugen Voll , Oskar Stephan , Karl J. Possemiers , Matthias Weismantel , Rüdiger Funk , Monte Peterson , Leo Van Miert , Rene Callot
CPC classification number: C08J5/00 , C08F220/06 , C08F222/1006 , C08J2333/02 , F26B25/00
Abstract: The invention relates to a process for producing water-absorbing polymer particles, comprising polymerization and drying the resulting polymer gel on a through-circulation belt dryer having at the end of the belt in transport direction a means for guiding the dried polymer gel down towards a means for crushing the dried polymer gel.
Abstract translation: 本发明涉及一种生产吸水性聚合物颗粒的方法，其包括将聚合物凝胶聚合并干燥在循环带式干燥器上，该循环带式干燥器在输送方向上在带端部具有将干燥聚合物凝胶向下引导的装置 破碎干燥聚合物凝胶的方法。
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公开(公告)号：US08883961B2
公开(公告)日：2014-11-11
申请号：US13975681
申请日：2013-08-26
Applicant: BASF SE
Inventor： Monte Peterson , Filip Mees , John Perry Guentzel , Justin Martin , Dominicus van Esbroeck , Karl J. Possemiers , Leo Van Miert , Oskar Stephan , Rüdiger Funk , Matthias Weismantel
CPC classification number: B01J20/3078 , B01J19/0053 , B01J19/1862 , C08J3/245 , C08J3/247 , C08J2333/02
Abstract: The invention relates to a process for producing water-absorbing polymer particles, comprising thermal postcrosslinking in a contact dryer having external heated outer surfaces.
Abstract translation: 本发明涉及一种生产吸水性聚合物颗粒的方法，包括在具有外部加热外表面的接触式干燥器中进行热后交联。
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公开(公告)号：US20130296509A1
公开(公告)日：2013-11-07
申请号：US13887972
申请日：2013-05-06
Applicant: BASF SE
Inventor： Oskar Stephan , Monte Peterson , Karl J. Possemiers , Steven Lippens
IPC: C08F2/01
CPC classification number: C08F2/01 , B01F7/041 , B01F15/065 , B01F15/068 , B01F2015/062 , B01F2215/0472 , G05D15/00 , G05D23/026 , Y10S526/918 , Y10S526/93
Abstract: The invention relates to a process for operating a mixing kneader, comprising one or more shafts on whose surfaces are disposed kneading bars and which are surrounded by a casing, comprising the following steps:(a) supplying reactants at an addition site in the mixing kneader,(b) converting the reactants in an exothermic reaction, the reaction at first forming a coherent kneadable intermediate,(c) tearing and dividing the coherent kneadable intermediate to form a product, the exothermic reaction optionally continuing during the tearing and division,(d) withdrawing the product at a withdrawal site in the mixing kneader, wherein at least one of the shafts and/or the casing is heated to a temperature above 20° C. during the operation of the mixing kneader.
Abstract translation: 本发明涉及一种操作混合捏合机的方法，该混合捏合机包括一个或多个轴，其表面设置有捏合杆并被壳体包围，包括以下步骤：（a）在混合捏合机中的加料部位供应反应物 （b）在放热反应中转化反应物，反应首先形成相干的可捏合中间体，（c）撕裂和分割粘结的可捏合中间体以形成产物，放热反应任选地在撕裂和分裂期间持续，（d ）在混合捏合机中的取出部位取出产品，其中在混合捏合机的操作期间将轴和/或壳体中的至少一个加热到高于20℃的温度。
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公开(公告)号：US20170246607A1
公开(公告)日：2017-08-31
申请号：US15320773
申请日：2015-06-10
Applicant: BASF SE
Inventor： Andreas Daiss , Robert Bayer , Rudolf Schliwa , Jürgen Freiberg , Karl J. Possemiers , Marco Krüger
IPC: B01J8/18 , C08F120/14 , B01J8/24
CPC classification number: B01J8/1872 , B01J4/001 , B01J8/24 , B01J2208/00893 , B01J2219/00247 , C08F2/01 , C08F120/14
Abstract: An apparatus for production of pulverulent poly(meth)acrylate, comprising a reactor or droplet polymerization, having an apparatus for dropletization of a monomer solution for the production of the poly(meth)acrylate, having holes through which the solution is dropletized, an addition point for a gas above the apparatus for dropletization, at least one gas withdrawal point on the periphery of the reactor and a fluidized bed. The outermost holes through which the solution is dropletized are positioned such that a droplet falling vertically downward falls into the fluidized bed and the hydraulic diameter at the level of the midpoint between the apparatus for dropletization and the gas withdrawal point is at least 10% greater than the hydraulic diameter of the fluidized bed.
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Patent Agency Ranking
公开(公告)号：US20170232418A1
公开(公告)日：2017-08-17
申请号：US15320771
申请日：2015-06-23
Applicant: BASF SE
Inventor： Andreas Daiss , Robert Bayer , Rudolf Schliwa , Jürgen Freiberg , Karl J. Possemiers , Marco Krüger
CPC classification number: B01J19/06 , B01J4/004 , B01J8/1818 , B01J19/24 , B01J2208/00371 , B01J2208/0092 , B01J2208/00938 , B01J2219/24 , C08F20/18
Abstract: An apparatus for introducing droplets of a monomer solution for production of poly(meth)acrylate into a reactor for droplet polymerization, comprising at least one channel or a dropletizer head, the channel or the dropletizer head being sealed at its base by a dropletizer plate, the dropletizer plate having holes through which the monomer solution is introduced into the reactor, and the dropletizer plate being configured such that holes that, in an axially symmetric dropletizer plate or in an annular dropletizer plate or in one configured as a ring segment, are not on a center line of the dropletizer plate or, in the case of a circular dropletizer plate, are not at the center of the dropletizer plate are aligned such that monomer solution is introduced through the holes into the reactor at an angle to the vertical, and the holes in the case of a radial alignment of axially symmetric dropletizer plates being aligned such that the angle at which the monomer solution is introduced into the reactor decreases in the direction of the axis of the reactor and, in the case of dropletizer plates arranged parallel to one another or of concentrically arranged dropletizer plates, each being aligned on a line parallel to the center line or line running concentrically about the center, such that the angle at which the monomer solution is introduced into the reactor is constant.
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公开(公告)号：US20170225138A1
公开(公告)日：2017-08-10
申请号：US15320776
申请日：2015-06-16
Applicant: BASF SE
Inventor： Andreas Daiss , Robert Bayer , Rudolf Schliwa , Jürgen Freiberg , Karl J. Possemiers , Marco Krüger
IPC: B01J4/00 , C08F120/14
CPC classification number: B01J4/001 , B01J2204/002 , B01J2208/00893 , B01J2219/00247 , C08F2/01 , C08F120/14
Abstract: An apparatus for addition of droplets of a monomer solution for production of poly(meth)acrylate to a reactor for droplet polymerization, comprising at least one channel or a dropletizer head having, at its base, holes through which the solution is dropletized into the reactor, at least one of the following features being fulfilled: (a) the ratio of the area covered by the channels or the dropletizer head in the reactor relative to the area which is defined by the circumference of a line along the outermost holes is less than 50%, (b) the number of holes relative to the area which is defined by the circumference of a line along the outermost holes is within a range from 100 to 1000 holes/m2.
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17.发明授权Process for producing water-absorbing polymer particles in a polymerization reactor with at least two axially parallel rotating shafts 有权在具有至少两个轴向平行的旋转轴的聚合反应器中生产吸水性聚合物颗粒的方法公开(公告)号：US09248429B2
公开(公告)日：2016-02-02
申请号：US13915927
申请日：2013-06-12
Applicant: BASF SE
Inventor： Monte Peterson , Karl J. Possemiers , Ronny De Kaey , Dominicus van Esbroeck , Rüdiger Funk
CPC classification number: B01J20/30 , B01J20/267 , B01J2220/68 , C08F2/01 , C08F220/06 , C08F2222/1013
Abstract: A process for producing water-absorbing polymer particles by polymerizing an aqueous monomer solution in a polymerization reactor with at least two axially parallel rotating shafts, wherein the polymerization is performed in the presence of an inert gas and under positive pressure.
Abstract translation: 通过在聚合反应器中聚合具有至少两个轴向平行的旋转轴的聚合反应器中的单体水溶液来生产吸水聚合物颗粒的方法，其中聚合在惰性气体存在下并在正压下进行。
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公开(公告)号：US08853333B2
公开(公告)日：2014-10-07
申请号：US13887972
申请日：2013-05-06
Applicant: BASF SE
Inventor： Oskar Stephan , Monte Peterson , Karl J. Possemiers , Steven Lippens
CPC classification number: C08F2/01 , B01F7/041 , B01F15/065 , B01F15/068 , B01F2015/062 , B01F2215/0472 , G05D15/00 , G05D23/026 , Y10S526/918 , Y10S526/93
Abstract: The invention relates to a process for operating a mixing kneader, comprising one or more shafts on whose surfaces are disposed kneading bars and which are surrounded by a casing, comprising the following steps: (a) supplying reactants at an addition site in the mixing kneader, (b) converting the reactants in an exothermic reaction, the reaction at first forming a coherent kneadable intermediate, (c) tearing and dividing the coherent kneadable intermediate to form a product, the exothermic reaction optionally continuing during the tearing and division, (d) withdrawing the product at a withdrawal site in the mixing kneader, wherein at least one of the shafts and/or the casing is heated to a temperature above 20° C. during the operation of the mixing kneader.
Abstract translation: 本发明涉及一种操作混合捏合机的方法，该混合捏合机包括一个或多个轴，其表面设置有捏合杆并被壳体包围，包括以下步骤：（a）在混合捏合机中的加料部位供应反应物 （b）在放热反应中转化反应物，反应首先形成相干的可捏合中间体，（c）撕裂和分割粘结的可捏合中间体以形成产物，放热反应任选地在撕裂和分裂期间持续，（d ）在混合捏合机中的取出部位取出产品，其中在混合捏合机的操作期间将轴和/或壳体中的至少一个加热到高于20℃的温度。
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19.发明申请Process for Producing Water-Absorbing Polymer Particles in a Polymerization Reactor with At Least Two Axially Parallel Rotating Shafts 有权在具有至少两个轴向平行旋转轴的聚合反应器中制造吸水聚合物颗粒的方法公开(公告)号：US20130338325A1
公开(公告)日：2013-12-19
申请号：US13915927
申请日：2013-06-12
Applicant: BASF SE
Inventor： Monte Peterson , Karl J. Possemiers , Ronny De Kaey , Dominicus van Esbroeck , Rüdiger Funk
IPC: B01J20/30
CPC classification number: B01J20/30 , B01J20/267 , B01J2220/68 , C08F2/01 , C08F220/06 , C08F2222/1013
Abstract: A process for producing water-absorbing polymer particles by polymerizing an aqueous monomer solution in a polymerization reactor with at least two axially parallel rotating shafts, wherein the polymerization is performed in the presence of an inert gas and under positive pressure.
Abstract translation: 通过在聚合反应器中聚合具有至少两个轴向平行的旋转轴的聚合反应器中的单体水溶液来生产吸水聚合物颗粒的方法，其中聚合在惰性气体存在下并在正压下进行。
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