GRANULES OR POWDERS AND METHODS FOR THEIR MANUFACTURE

    公开(公告)号:US20210179978A1

    公开(公告)日:2021-06-17

    申请号:US17052364

    申请日:2019-04-25

    Applicant: BASF SE

    Abstract: Process for manufacturing granules or powders comprising the steps of (a) providing an aqueous solution or slurry of (A) at least one chelating agent according to general formula (I a) [CH3—CH(COO)—N(CH2—COO)2]M3-XHX (I a) wherein M is selected from alkali metal cations and ammonium, same or different, and x is in the range of from 0.01 to 1.0 or (I b) [OOC—CH2CH2—CH(COO)—N(CH2—COO)2]M4-XHX (I b) wherein M is as defined above, and x in formula (I b) is in the range of from 0.01 to 2.0, and (B) at least one polymer selected from (B1) polyaspartates with an average molecular weight Mw in the range of from 1,000 to 20,000 g/mole, and (B2) copolymers comprising, in copolymerized form, (α) at least one ester of an ethylenically unsaturated mono- or dicarboxylic acid, and (β) at least one ethylenically unsaturated N-containing monomer, and (b) spray drying or granulating said solution or slurry.

    PROCESS FOR MAKING MIXTURES OF CHELATING AGENTS

    公开(公告)号:US20180105486A1

    公开(公告)日:2018-04-19

    申请号:US15573155

    申请日:2016-05-03

    Applicant: BASF SE

    Abstract: Process for making a chelating agent according to the general formula (I), R1—CH(COOX1)—N(CH2COOX1)2 wherein R1 is selected from hydrogen, C1-C4-alkyl, phenyl, benzyl, CH2OH, and CH2CH2COOX1, X1 is (MχH1-χ), M being selected from alkali metal, x is in the range of from 0.6 to 1, said process comprising the following steps: (a) providing a solid, a slurry or a solution of a compound according to general formula (II a) R1—CH(COOX2)—N(CH2CN)2 wherein X2 is (MyH1-y), M being selected from alkali metal, y is in the range of from zero to 1, (b) contacting said solid or slurry or solution with an aqueous solution of alkali metal hydroxide, wherein the molar ratio of alkali metal ions to nitrile groups is in the range of from 0.6:1 to 0.95:1, (c) reacting said compound according to general formula (II a) with said alkali metal hydroxide.

    N,N-BIS(2-AMINOALKYL)-1,2-ALKYL DIAMINE DERIVATIVES
    14.
    发明申请
    N,N-BIS(2-AMINOALKYL)-1,2-ALKYL DIAMINE DERIVATIVES 审中-公开
    N,N-BIS(2-氨基甲酰基)-1,2-AlKYL DIAMINE衍生物

    公开(公告)号:US20160304445A1

    公开(公告)日:2016-10-20

    申请号:US15101964

    申请日:2014-11-21

    Applicant: BASF SE

    CPC classification number: C07C265/04 C07C209/48 C07C211/14 C07C263/10

    Abstract: The present invention relates to 2-N,N-(bis-2-aminoalkyl)-1,2-alkyldiamine derivatives of formula (I) as such, to a process for preparing the 2-N,N-(bis-2-aminoalkyl)-1,2-alkyldiamine derivatives, to the use of the 2-N,N-(bis-2-aminoalkyl)-1,2-alkyldiamine derivatives as hardeners for epoxy resins, as an intermediate in the preparation of triisocyanates, as initiators for polyetherols and/or as monomers for the preparation of polyamides, to triisocyanates derived from the 2-N,N-(bis-2-aminoalkyl)-1,2-alkyldiamine derivatives of formula (I) and also to a process for preparing these triisocyanates.

    Abstract translation: 本发明涉及式(I)的2-N,N-(二-2-氨基烷基)-1,2-烷基二胺衍生物本身涉及制备2-N,N-(双-2- 使用2-N,N-(二-2-氨基烷基)-1,2-烷基二胺衍生物作为环氧树脂的硬化剂,作为制备三异氰酸酯的中间体, 作为用于制备聚酰胺的聚醚和/或单体的引发剂,衍生自式(I)的2-N,N-(二-2-氨基烷基)-1,2-烷基二胺衍生物的三异氰酸酯,还涉及一种方法 用于制备这些三异氰酸酯。

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