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    Micro-scale chemical process simulation methods and apparatus useful for design of full scale processes, emergency relief systems and associated equipment
    11.
    发明授权
    Micro-scale chemical process simulation methods and apparatus useful for design of full scale processes, emergency relief systems and associated equipment 失效
    微型化学过程模拟方法和设备，适用于全尺寸过程，应急救援系统及相关设备的设计

    公开(公告)号：US4670404A

    公开(公告)日：1987-06-02

    申请号：US801734

    申请日：1985-11-26

    Applicant: Ian Swift ,  Hans K. Fauske

    Inventor： Ian Swift ,  Hans K. Fauske

    IPC: B01J3/00 ,  B01J3/04 ,  B01J19/00 ,  G01N25/20 ,  G05B9/00

    CPC classification number: B01J3/002 ,  B01J19/0006 ,  B01J19/0093 ,  B01J3/046 ,  B01J2219/00015 ,  B01J2219/00058 ,  B01J2219/00162

    Abstract: Micro-scale chemical process simulation apparatus is disclosed which is useful for design of full-scale processes and associated equipment as well as emergency relief systems. A thin-walled vessel for receiving a quantity of the material to be evaluated is supportd within and thermally insulated from the walls of a surrounding containment unit. A guard heater is provided around the vessel and temperature thermocouples and pressure transducers are strategically located to monitor the temperature conditions existing in the material in the vessel as well as the pressure within the vessel and the containment unit respectively. Fluid may be selectively introduced into or exhausted from the containment unit to maintain a required pressure balance between the interior of the vessel and that of the containment unit. The wall thickness of the pilot vessel is such that the phi factor defined by the thermal mass of the material plus the thermal mass of the vessel divided by the thermal mass of the material is not significantly greater than the same ratio of thermal masses which obtain during a full-scale chemical operation in a pressure vessel.

    Abstract translation: 公开了一种微型化学过程模拟装置，其用于设计全尺寸过程及相关设备以及紧急救援系统。 用于接收一定量待评估材料的薄壁容器被支撑在周围的容纳单元的壁内并与其隔热。 在容器周围提供防护加热器，温度热电偶和压力传感器位于战略位置，以分别监测容器中材料中存在的温度条件以及容器和容纳单元内的压力。 流体可以选择性地引入到容纳单元中或从容纳单元中排出，以在容器的内部和容纳单元的内部之间保持所需的压力平衡。 先导容器的壁厚使得由材料的热质量加上容器的热质量除以材料的热质量所限定的phi因子不显着大于在材料中获得的热质量的相同比例 在压力容器中进行全面的化学操作。

    High-pressure fluidized bed reactor for preparing granular polycrystalline silicon
    14.
    发明授权
    High-pressure fluidized bed reactor for preparing granular polycrystalline silicon 有权
    用于制备颗粒状多晶硅的高压流化床反应器

    公开(公告)号：US07972562B2

    公开(公告)日：2011-07-05

    申请号：US12093513

    申请日：2007-02-07

    Applicant: Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    Inventor： Hee Young Kim ,  Kyung Koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC: G05D16/00 ,  B01J19/00 ,  B01J8/18 ,  F27B15/08 ,  F27B15/14 ,  F27B15/16 ,  C01B33/02

    CPC classification number: C01B33/027 ,  B01J3/046 ,  B01J8/1827 ,  B01J8/1836 ,  B01J2208/00398 ,  B01J2208/00407 ,  C01B33/029 ,  C01B33/03

    Abstract: The present invention relates to a high-pressure fluidized bed reactor for preparing granular polycrystalline silicon, comprising (a) a reactor tube, (b) a reactor shell encompassing the reactor tube, (c) an inner zone formed within the reactor tube, where a silicon particle bed is formed and silicon deposition occurs, and an outer zone formed in between the reactor shell and the reactor tube, which is maintained under the inert gas atmosphere, and (d) a controlling means to keep the difference between pressures in the inner zone and the outer zone being maintained within the range of 0 to 1 bar, thereby enabling to maintain physical stability of the reactor tube and efficiently prepare granular polycrystalline silicon even at relatively high reaction pressure.

    Abstract translation: 本发明涉及一种用于制备颗粒状多晶硅的高压流化床反应器，包括（a）反应器管，（b）包围反应器管的反应器壳，（c）在反应器管内形成的内部区，其中 形成硅颗粒床并发生硅沉积，并且在反应器壳体和反应器管之间形成的外部区域保持在惰性气体气氛下，以及（d）控制装置，以保持在 内部区域和外部区域保持在0至1巴的范围内，从而能够保持反应管的物理稳定性，并且即使在相对高的反应压力下也能有效地制备颗粒状多晶硅。

    High-Pressure Fluidized Bed Reactor for Preparing Granular Polycrystalline Silicon
    16.
    发明申请
    High-Pressure Fluidized Bed Reactor for Preparing Granular Polycrystalline Silicon 有权
    用于制备颗粒状多晶硅的高压流化床反应器

    公开(公告)号：US20080267834A1

    公开(公告)日：2008-10-30

    申请号：US12093513

    申请日：2007-02-07

    Applicant: Hee Young Kim ,  Kyung koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    Inventor： Hee Young Kim ,  Kyung koo Yoon ,  Yong Ki Park ,  Won Choon Choi

    IPC: F27B15/10

    CPC classification number: C01B33/027 ,  B01J3/046 ,  B01J8/1827 ,  B01J8/1836 ,  B01J2208/00398 ,  B01J2208/00407 ,  C01B33/029 ,  C01B33/03

    Abstract: The present invention relates to a high-pressure fluidized bed reactor for preparing granular polycrystalline silicon, comprising (a) a reactor tube, (b) a reactor shell encompassing the reactor tube, (c) an inner zone formed within the reactor tube, where a silicon particle bed is formed and silicon deposition occurs, and an outer zone formed in between the reactor shell and the reactor tube, which is maintained under the inert gas atmosphere, and (d) a controlling means to keep the difference between pressures in the inner zone and the outer zone being maintained within the range of 0 to 1 bar, thereby enabling to maintain physical stability of the reactor tube and efficiently prepare granular polycrystalline silicon even at relatively high reaction pressure.

    Abstract translation: 本发明涉及一种用于制备颗粒状多晶硅的高压流化床反应器，包括（a）反应器管，（b）包围反应器管的反应器壳，（c）在反应器管内形成的内部区，其中 形成硅颗粒床并发生硅沉积，并且在反应器壳体和反应器管之间形成的外部区域保持在惰性气体气氛下，以及（d）控制装置，以保持在 内部区域和外部区域保持在0至1巴的范围内，从而能够保持反应管的物理稳定性，并且即使在相对高的反应压力下也能有效地制备颗粒状多晶硅。

    Downflow hydrothermal treatment
    17.
    发明授权
    Downflow hydrothermal treatment 失效
    下流水热处理

    公开(公告)号：US6054057A

    公开(公告)日：2000-04-25

    申请号：US938899

    申请日：1997-09-26

    Applicant: David A. Hazlebeck ,  Kevin W. Downey ,  Michael H. Spritzer

    Inventor： David A. Hazlebeck ,  Kevin W. Downey ,  Michael H. Spritzer

    IPC: B09B3/00 ,  B01J3/00 ,  B01J3/04 ,  B01J8/00 ,  B01J19/02 ,  B01J19/24 ,  B01J19/26 ,  C02F1/02 ,  C02F1/72 ,  C02F1/74 ,  C02F11/08 ,  C02F1/68 ,  A61B1/30

    CPC classification number: B01J3/046 ,  B01J19/02 ,  B01J19/26 ,  B01J3/008 ,  C02F11/086 ,  B01J2219/00103 ,  B01J2219/00155 ,  B01J2219/00159 ,  B01J2219/00162

    Abstract: A system and method for treatment of a feed material includes a reactor chamber in a reactor vessel. The reactor vessel has a longitudinal axis which is vertically oriented so that gravitational forces act generally in a direction along the axis between a top and a bottom of the vessel. A feed material is introduced by a nozzle into the reactor chamber as a jet stream through the top end of the vessel. This jet stream causes back-mixing in the reactor chamber, contributing to rapid initiation of reaction and general down flow of material through the reactor chamber. The material in the reactor chamber can be quenched to dissolve sticky solids in the effluent before the effluent is discharged from the lower end of the vessel. Further, the reactor vessel can include a plug flow section to carry out additional reaction of the feed material.

    Abstract translation: 用于处理进料的系统和方法包括在反应器容器中的反应室。 反应器容器具有垂直取向的纵向轴线，使得重力通常沿着容器顶部和底部之间的轴线的方向起作用。 通过喷嘴将进料材料作为喷射流通过容器的顶端引入反应器室。 该喷射流在反应器室中引起反混合，有助于反应室的快速启动和材料通过反应器室的一般向下流动。 在流出物从容器的下端排出之前，可以将反应器室中的材料淬火以溶解流出物中的粘性固体。 此外，反应器容器可以包括用于进行进料的附加反应的活塞流动部分。

    Method and apparatus for multiphase coal hydrogenation reactors with exothermal heat of reaction having gas cooling in sump-phase reactors
    19.
    发明授权
    Method and apparatus for multiphase coal hydrogenation reactors with exothermal heat of reaction having gas cooling in sump-phase reactors 失效
    多相煤加氢反应器的方法和装置，其具有在储池相反应器中具有气体冷却的反应放热

    公开(公告)号：US4696735A

    公开(公告)日：1987-09-29

    申请号：US789799

    申请日：1985-10-21

    Applicant: Eckard Wolowski ,  Frank Mirtsch ,  Herbert Dybus

    Inventor： Eckard Wolowski ,  Frank Mirtsch ,  Herbert Dybus

    IPC: B01J8/00 ,  B01J19/00 ,  C10G1/06 ,  C10G1/00 ,  B01J10/00

    CPC classification number: B01J3/046 ,  C10G1/065

    Abstract: A practically isothermal temperature distribution of the reactor contents is obtained, especially for high temperature and pressurized hydrogenation reactors operating in the sump-phase by a hydrogenation gas passing over the outer region of the reaction chamber, so that the hydrogenation gas cools the reaction in the chamber. Additionally, the reaction heat which is extracted by the hydrogenation gas is used to heat the reaction components at a stage in the hydrogenation process. The major portion of the reaction heat is used to heat charges, preferably for the reactors, which charges contain no appreciable amounts of solid material. These charges, preferably comprising hydrogenation gas, preferably pass through a jacket space between the reaction chambers and the external portion of the reactors, which external portions preferably make contact with the atmosphere. Only comparatively small quantities of a cold gas, mixed into the reactors for the cooling thereof, are required to establish the desired isothermal temperature distribution.

    Abstract translation: 获得反应器内容物的几乎等温的温度分布，特别是对于通过在反应室的外部区域上通过的氢化气体在油槽相中操作的高温和加压氢化反应器，使得氢化气体在 房间。 此外，由氢化气体提取的反应热用于在氢化过程的一个阶段加热反应组分。 反应热的主要部分用于加热电荷，优选用于反应器，该电荷不含可观量的固体材料。 这些电荷优选包括氢化气体，优选地通过反应室和反应器外部之间的护套空间，这些外部部分优选地与大气接触。 需要混合到反应器中用于冷却的相对少量的冷气体来建立所需的等温温度分布。

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