公开(公告)号：US09238875B2

公开(公告)日：2016-01-19

申请号：US12929567

申请日：2011-02-01

Applicant: Hexiang Zhu ,  Karl Pearson ,  Joo Ro Kim

Inventor： Hexiang Zhu ,  Karl Pearson ,  Joo Ro Kim

IPC: C30B29/04 ,  B01J3/06

CPC classification number: C30B29/04 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068 ,  Y10T117/10

Abstract: A multi-layer structure in a reaction cell for a diamond growth is provided. The multi-layer structure includes: a diamond seed; a first metal catalyst layer provided on the diamond seed, the first metal catalyst layer containing a first concentration of carbon; a second metal catalyst layer provided on the first metal layer, the second metal catalyst layer containing a second concentration of carbon that is higher than the first concentration; and a carbon source layer provided on the second metal layer.

Abstract translation: 提供了用于金刚石生长的反应池中的多层结构。 多层结构包括：金刚石种子; 设置在所述金刚石晶种上的第一金属催化剂层，所述第一金属催化剂层含有第一浓度的碳; 设置在所述第一金属层上的第二金属催化剂层，所述第二金属催化剂层含有高于所述第一浓度的第二浓度的碳; 以及设置在第二金属层上的碳源层。

公开(公告)号：US09227166B2

公开(公告)日：2016-01-05

申请号：US11988891

申请日：2006-07-21

Applicant: Hitoshi Sumiya

Inventor： Hitoshi Sumiya

IPC: B01J3/06 ,  B82Y30/00 ,  C04B35/52 ,  C04B35/626 ,  C04B35/645

CPC classification number: B01J3/062 ,  B01J2203/0625 ,  B01J2203/0655 ,  B01J2203/068 ,  B01J2203/0685 ,  B82Y30/00 ,  C04B35/52 ,  C04B35/6261 ,  C04B35/645 ,  C04B2235/422 ,  C04B2235/425 ,  C04B2235/427 ,  C04B2235/528 ,  C04B2235/5288 ,  C04B2235/5436 ,  C04B2235/5445 ,  C04B2235/5454 ,  C04B2235/656 ,  C04B2235/78 ,  C04B2235/781 ,  C04B2235/785 ,  C04B2235/96 ,  Y10T428/2982

Abstract: There are provided sufficiently strong, hard, and heat resistant, dense and homogenous polycrystalline diamond applicable to cutting tools, dressers, dies and other working tools and excavation bits and the like, and a cutting tool having a cutting edge of the polycrystalline diamond. The polycrystalline diamond is formed substantially only of diamond formed using a composition of material containing a non diamond type carbon material, the composition of material being converted directly into diamond and sintered at ultra high pressure and ultra high temperature without aid of a sintering aid or a catalyst, and has a mixed microstructure having a fine crystal grain of diamond having a maximal grain size of at most 100 nm and an average grain size of at most 50 nm and a coarse crystal grain of diamond in the form of one of a platelet and a granule having a grain size of at least 50 nm and at most 10,000 nm.

公开(公告)号：US09199357B2

公开(公告)日：2015-12-01

申请号：US13644790

申请日：2012-10-04

Applicant: Chien-Min Sung

Inventor： Chien-Min Sung

IPC: B24B53/02 ,  B24D18/00 ,  B24B53/017 ,  B01J3/06

CPC classification number: B24D18/0054 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B24B53/017

Abstract: Superabrasive tools and methods for the making thereof are disclosed and described. In one aspect, superabrasive particles are chemically bonded to a matrix support material according to a predetermined pattern by a braze alloy. The brazing alloy may be provided as a powder, thin sheet, or sheet of amorphous alloy. A template having a plurality of apertures arranged in a predetermined pattern may be used to place the superabrasive particles on a given substrate or matrix support material.

公开(公告)号：US09192899B2

公开(公告)日：2015-11-24

申请号：US13528511

申请日：2012-06-20

Applicant: Hitoshi Sumiya

Inventor： Hitoshi Sumiya

IPC: B01J3/06 ,  C01B31/06 ,  C04B35/52 ,  C04B35/626 ,  C04B35/645 ,  B82Y30/00

CPC classification number: B01J3/062 ,  B01J2203/0655 ,  B82Y30/00 ,  C01B32/25 ,  C04B35/52 ,  C04B35/6261 ,  C04B35/645 ,  C04B2235/421 ,  C04B2235/422 ,  C04B2235/425 ,  C04B2235/427 ,  C04B2235/5436 ,  C04B2235/5445 ,  C04B2235/5454 ,  C04B2235/656 ,  C04B2235/72 ,  C04B2235/781 ,  C04B2235/785 ,  C04B2235/786 ,  C04B2235/96

Abstract: A diamond sintered body conventionally used in a cutting tool or the like includes an iron group metal element as a sintering aid, and therefore has a problem in heat resistance. A diamond sintered body not including the iron group metal, on the other hand, does not have sufficient mechanical strength to be used as a tool material, and also does not have conductivity, which makes electrical discharge machining impossible, and thus processing thereof is difficult. A diamond polycrystalline body having high heat resistance and mechanical strength and having conductivity enabling electrical discharge machining is obtained by using only an amorphous or fine graphite-type carbon material as a starting material, adding boron thereto and concurrently performing conversion into diamond and sintering in an ultra-high pressure and temperature condition.

Abstract translation: 通常用于切削工具等的金刚石烧结体包括作为烧结助剂的铁族金属元素，因此具有耐热性问题。 另一方面，不包含铁族金属的金刚石烧结体不具有足够的机械强度用作工具材料，也不具有导电性，这使得不能进行放电加工，因此其处理困难 。 通过仅使用无定形或细石墨型碳材料作为起始材料，可以获得具有高耐热性和机械强度并且具有导电性的金刚石多晶体，其中加入硼并同时进行金刚石的转化和烧结 超高压和温度条件。

公开(公告)号：US09150419B2

公开(公告)日：2015-10-06

申请号：US12463413

申请日：2009-05-10

Applicant: Matthew R. Linford ,  Michael A. Vail

Inventor： Matthew R. Linford ,  Michael A. Vail

IPC: C09K3/00 ,  C01B31/06 ,  B01L3/00 ,  A61J3/07 ,  B29C39/10 ,  B01J3/06 ,  B01J3/08 ,  B32B3/26 ,  G01N35/10

CPC classification number: C01B31/06 ,  B01L3/52 ,  B01L2200/12 ,  B01L2300/12 ,  C01B32/25 ,  G01N35/1002 ,  Y10T428/249953

Abstract: A reagent delivering article comprising porous sintered polycrystalline diamond where the delivering article is capable of retaining at least one chemical reagent and releasing the chemical reagent in a fluid or has reactive sites on diamond surfaces of the article.

Abstract translation: 一种包含多孔烧结多晶金刚石的试剂递送制品，其中所述递送制品能够保留至少一种化学试剂并将所述化学试剂释放在流体中或者在所述制品的金刚石表面上具有反应性位点。

公开(公告)号：US09120204B2

公开(公告)日：2015-09-01

申请号：US13641390

申请日：2011-04-20

Applicant: Robert Fries

Inventor： Robert Fries

IPC: B24D3/00 ,  B24D3/34 ,  B01J3/06 ,  C22C1/05 ,  C22C26/00 ,  E21B10/567

CPC classification number: B24D3/348 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0685 ,  B22F2998/10 ,  C22C1/051 ,  C22C26/00 ,  E21B10/567 ,  C22C1/05 ,  C25D15/00 ,  B22F3/14

Abstract: A polycrystalline superhard material comprises a sintered mass of superhard grains having a mean superhard grain contiguity of at least 62 percent and at most 92 percent. There is also disclosed a method of making such a polycrystalline superhard material. The method comprises providing a precursor body comprising superhard grains and interstices between the superhard grains, and introducing additive particles into the interstices to form a pre-sinter body. The pre-sinter body is submitted to a temperature and pressure at which superhard material is thermodynamically stable, sintering it and forming polycrystalline superhard material.

Abstract translation: 多晶超硬材料包括具有至少62％且至多92％的平均超硬颗粒接近度的超硬颗粒的烧结块。 还公开了制造这种多晶超硬材料的方法。 该方法包括提供包含超硬颗粒和超硬颗粒之间的间隙的前体体，并将添加剂颗粒引入到间隙中以形成预烧结体。 预烧结体承受超硬材料在热力学上稳定的温度和压力，烧结并形成多晶超硬材料。

公开(公告)号：US09061336B2

公开(公告)日：2015-06-23

申请号：US12523545

申请日：2008-01-18

Applicant: Hitoshi Sumiya ,  Makoto Yukawa

Inventor： Hitoshi Sumiya ,  Makoto Yukawa

IPC: B21C3/02 ,  B21C3/18 ,  C30B29/60 ,  B01J3/06 ,  B82Y30/00 ,  C04B35/52 ,  C04B35/645

CPC classification number: B21C3/025 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/0625 ,  B01J2203/0655 ,  B01J2203/068 ,  B01J2203/0685 ,  B21C3/18 ,  B82Y30/00 ,  C04B35/52 ,  C04B35/645 ,  C04B2235/422 ,  C04B2235/425 ,  C04B2235/427 ,  C04B2235/656 ,  C04B2235/781 ,  C04B2235/783 ,  C04B2235/785 ,  C30B29/605

Abstract: One object of the present invention is to provide a wire drawing die excellent in strength and wear resistance. The wire drawing die has a core formed using highly hard diamond polycrystalline body made substantially only of diamond and produced by directly converting a raw material composition including a non-diamond type carbon material into diamond and sintering the diamond at an ultra high pressure and an ultra high temperature without adding a sintering aid or a catalyst, the polycrystalline body having a mixed construction including fine-grained diamond crystals with a maximum grain size of less than or equal to 100 nm and an average grain size of less than or equal to 50 nm and plate-like or particulate coarse-grained diamond crystals with a minimum grain size of greater than or equal to 50 nm and a maximum grain size of less than or equal to 10000 nm.

Abstract translation: 本发明的一个目的是提供一种强度和耐磨性优异的拉丝模具。 拉丝模具具有使用基本上仅由金刚石制成的高硬度金刚石多晶体形成的芯，其通过将包含非金刚石型碳材料的原料组合物直接转化为金刚石并以超高压和超高压烧结金刚石 高温而不添加烧结助剂或催化剂，所述多晶体具有混合结构，其包括最大粒径小于或等于100nm的细晶粒金刚石晶体和小于或等于50nm的平均粒度 以及最小晶粒尺寸大于或等于50nm并且最大晶粒尺寸小于或等于10000nm的板状或颗粒状粗粒金刚石晶体。

公开(公告)号：US09061264B2

公开(公告)日：2015-06-23

申请号：US13210681

申请日：2011-08-16

Applicant: Robert H. Frushour

Inventor： Robert H. Frushour

IPC: B24D11/00 ,  B01J3/06

CPC classification number: B01J3/062 ,  B01J2203/0605 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685

Abstract: A polycrystalline diamond cutting element for use in rock drilling or other operations that requires very high abrasion resistance with high transverse rupture strength at temperatures above 700 degrees centigrade. The cutting element includes a diamond layer that contains pre-sintered polycrystalline diamond agglomerate (PPDA) bonded to a supporting substrate. The PPDA can be made thermally stable and can be selected to produce a cutting element with any desired abrasion resistance characteristic without affecting internal stress.

Abstract translation: 用于岩石钻探或其他操作的多晶金刚石切割元件，其在高于700摄氏度的温度下需要非常高的耐磨性和高的横向断裂强度。 切割元件包括金刚石层，其包含结合到支撑基底的预烧结多晶金刚石附聚物（PPDA）。 PPDA可以制成热稳定的并且可以选择以产生具有任何期望的耐磨特性的切割元件而不影响内部应力。

公开(公告)号：US09039832B2

公开(公告)日：2015-05-26

申请号：US13144512

申请日：2010-01-15

Applicant: Raymond Anthony Spits ,  Carlton Nigel Dodge

Inventor： Raymond Anthony Spits ,  Carlton Nigel Dodge

IPC: C30B29/04 ,  B01J3/06 ,  B01J23/745 ,  B01J23/75 ,  B01J23/755

CPC classification number: C30B29/04 ,  B01J3/062 ,  B01J23/745 ,  B01J23/75 ,  B01J23/755 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068

Abstract: A high pressure high temperature (HPHT) method for synthesizing single crystal diamond, wherein a single crystal diamond seed having an aspect ratio of at least (1) and a growth surface substantially parallel to a {110} crystallographic plane is utilized is described. The growth is effected at a temperature in the range from 1280° C. to 1390° C.

Abstract translation: 描述了用于合成单晶金刚石的高压高温（HPHT）方法，其中使用具有至少（1）的纵横比和基本上平行于{110}晶面的生长表面的单晶金刚石晶种。 生长在1280℃至1390℃的温度下进行。

公开(公告)号：US09034296B2

公开(公告)日：2015-05-19

申请号：US14019663

申请日：2013-09-06

Applicant: Carlton Nigel Dodge ,  Raymond Anthony Spits

Inventor： Carlton Nigel Dodge ,  Raymond Anthony Spits

IPC: B01J3/06 ,  C01B31/06 ,  B01J3/08 ,  C30B25/18

CPC classification number: C30B25/18 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068 ,  Y10T428/24942 ,  Y10T428/30

Abstract: The present invention relates to an HPHT method for synthesizing single crystal diamond, wherein a single crystal diamond seed having an aspect ratio of at least 1.5 is utilized. Single crystal diamond seeds having an aspect ratio of at least 1.5 and synthetic single crystal diamond which may be obtained by the method recited are also described. The growth surface is substantially aligned along a or direction in the plane of the growth surface.

Abstract translation: 本发明涉及一种用于合成单晶金刚石的HPHT方法，其中使用纵横比为至少1.5的单晶金刚石晶种。 还描述了可以通过所述方法获得的具有至少1.5的纵横比的单晶金刚石种子和合成单晶金刚石。 生长表面在生长表面的平面中沿着<100>或<110>方向基本排列。