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公开(公告)号:US4054641A
公开(公告)日:1977-10-18
申请号:US684108
申请日:1976-05-07
Applicant: Justice N. Carman
Inventor: Justice N. Carman
CPC classification number: C01B33/182 , B01J19/02 , C01B33/12 , C03B17/04 , C03C3/06 , B01J2219/0209 , C01P2006/80 , C03C2201/32 , C03C2201/3435 , C03C2201/42 , C03C2203/00 , Y02P20/142
Abstract: Method and apparatus for making vitreous silica of high purity including producing a melt of liquid silicon in a first chamber, mixing the liquid silicon with carbon dioxide in an upper zone of a second chamber to produce silicon monoxide, mixing the silicon monoxide with oxygen in a lower zone of the second chamber producing silicon dioxide in gaseous form, condensing the silicon dioxide on the wall of the second chamber, and withdrawing the resultant tube of vitreous silica from the lower end of the second chamber. The apparatus is lined with silica to prevent introduction of impurities. The liquid silicon is produced by mixing hydrogen and trichlorosilane.
Abstract translation: 用于制造高纯度的二氧化硅玻璃的方法和设备,包括在第一室中产生液态硅熔体,在第二室的上部区域中混合液体硅与二氧化碳以产生一氧化硅,将一氧化硅与氧气混合在一起 第二室的下部区域产生气态二氧化硅,将二氧化硅冷凝在第二室的壁上,并从第二室的下端抽出所得到的二氧化硅管。 该装置衬有二氧化硅以防止引入杂质。 液态硅是通过混合氢气和三氯硅烷来生产的。