Process for the selective deposition of particulate material
    21.
    发明授权
    Process for the selective deposition of particulate material 失效
    颗粒材料的选择性沉积工艺

    公开(公告)号:US07220456B2

    公开(公告)日:2007-05-22

    申请号:US10815010

    申请日:2004-03-31

    CPC classification number: B05D1/025 B05D1/12 B05D2401/90

    Abstract: A process for the patterning of a desired substance on a surface includes: (i) charging a particle formation vessel with a compressed fluid; (ii) introducing into the particle formation vessel a first feed stream comprising a solvent and the desired substance dissolved therein and a second feed stream comprising the compressed fluid, wherein the desired substance is less soluble in the compressed fluid relative to its solubility in the solvent and the solvent is soluble in the compressed fluid, and wherein the first feed stream is dispersed in the compressed fluid, allowing extraction of the solvent into the compressed fluid and precipitation of particles of the desired substance; (iii) exhausting compressed fluid, solvent and the desired substance from the particle formation vessel at a rate substantially equal to a rate of addition of such components to the vessel in step (ii) through a restrictive passage to a lower pressure whereby the compressed fluid is transformed to a gaseous state, and wherein the restrictive passage includes a discharge device that produces a shaped beam of particles of the desired substance at a point beyond an outlet of the discharge device, where the fluid is in a gaseous state at a location before or beyond the outlet of the discharge device; and (iv) exposing a receiver surface to the shaped beam of particles of the desired substance and selectively depositing a pattern of particles on the receiver surface.

    Abstract translation: 用于在表面上图案化所需物质的方法包括:(i)用压缩流体填充颗粒形成容器; (ii)向颗粒形成容器中引入包含溶剂和所需物质溶解在其中的第一进料流和包含压缩流体的第二进料流,其中所需物质相对于其在溶剂中的溶解度较不溶于压缩流体 并且溶剂可溶于压缩流体中,并且其中第一进料流分散在压缩流体中,允许将溶剂萃取到压缩流体中并沉淀所需物质的颗粒; (iii)通过限制性通道将压缩流体,溶剂和所需物质从所述颗粒形成容器排出,其速率基本上等于在步骤(ii)中通过限制通道将这些组分添加到容器中的速率,由此压缩流体 转化为气态,并且其中限制通道包括排出装置,其在超出排放装置的出口的点处产生所需物质的成形颗粒束,其中流体在气体状态处于位于之前的位置处 或超出排出装置的出口; 和(iv)将接收器表面暴露于所需物质的成形的颗粒束并选择性地在接收器表面上沉积颗粒图案。

    Process for the preparation of high bromide cubic grain emulsions
    24.
    发明授权
    Process for the preparation of high bromide cubic grain emulsions 失效
    制备高溴化物立方颗粒乳剂的方法

    公开(公告)号:US06753134B2

    公开(公告)日:2004-06-22

    申请号:US10202314

    申请日:2002-07-24

    Abstract: A process for the preparation of a radiation-sensitive silver halide emulsion comprised of high bromide cubical silver halide grains is described, the process comprising: (a) providing in a stirred reaction vessel a dispersing medium and high bromide silver halide seed grains, the seed grains comprising at least 5 mole % of the final emulsion silver, and (b) precipitating a silver halide shell which comprises at least 5 mole % of the final emulsion silver onto the seed grains by introducing at least a silver salt solution into the dispersing medium at a rate such that the normalized shell molar addition rate, Rs, is above 1.0×10−3 min−2, Rs satisfying the formula: R s = M s M t ⁢ t s 2 where Ms is the number of moles of silver halides added to the reaction vessel during the formation of the shell, ts is the run time, in minutes, of the silver salt solution for the formation of the shell, and Mt is total moles of silver halide in the reaction vessel at the end of the precipitation of the shell; wherein the concentration of silver halide grains in the reaction vessel at the end of the precipitation of the shell is at least 0.5 mole/L. The invention provides an improved manufacturing process for the preparation of high bromide silver halide cubical grain emulsion enabling concentrated emulsion batches to be prepared with desired photographic properties. In certain embodiments of the invention, further advantages are enabled in accordance with the discovery that when the exterior portion of high bromide silver halide cubic grains are grown under specific conditions of high molar addition rates, emulsions of enhanced sensitivity, improved contrast and radiographic curve shape may be produced while controlling the minimum fog level.

    Abstract translation: 描述了制备由高溴化物立方卤化银颗粒组成的辐射敏感卤化银乳剂的方法,该方法包括:(a)在搅拌的反应容器中提供分散介质和高溴化物卤化银种子颗粒,种子 包含至少5摩尔%的最终乳液银的颗粒,和(b)通过将至少一种银盐溶液引入到分散介质中,将包含至少5摩尔%的最终乳液银的卤化银壳沉淀到种子晶粒上 使得归一化的壳摩尔加成速率Rs大于1.0×10 -3 min 2,Rs满足下式:其中Ms是在反应容器中加入的卤化银的摩尔数 壳的形成,ts是用于形成壳的银盐溶液的运行时间(分钟),Mt是壳体沉淀结束时反应容器中卤化银的总摩尔数; 其中壳体沉淀结束时反应容器中卤化银颗粒的浓度为至少0.5mol / L。 本发明提供了一种用于制备高溴化银卤化银立方颗粒乳液的改进的制备方法,使得能够制备具有所需照相性能的浓缩乳液批料。 在本发明的某些实施方案中,根据以下发现可以实现进一步的优点:当高溴化银卤化银立方晶粒的外部部分在高摩尔添加速率的特定条件下生长时,增强灵敏度,改善的对比度和放射线形状曲线形状的乳剂 可以在控制最小雾水平的同时产生。

    High chloride emulsions doped with iridium complexes
    25.
    发明授权
    High chloride emulsions doped with iridium complexes 失效
    掺有铱络合物的高氯化物乳液

    公开(公告)号:US06242172B1

    公开(公告)日:2001-06-05

    申请号:US09475841

    申请日:1999-12-30

    Abstract: A radiation-sensitive emulsion is disclosed comprised of cubical silver halide grains containing from 0.05 to 3 mole percent iodide, based on total silver, and an iridium coordination complex dopant, wherein (i) the iodide is incorporated in the grains in a controlled, non-uniform distribution forming a core containing at least 50 percent of total silver, an iodide free surface shell having a thickness of greater than 50 Å, and a sub-surface shell that contains a maximum iodide concentration, and (ii) the iridium coordination complex dopant is incorporated into the sub-surface shell or into a region of the core extending up to 60% of the total silver into the grain from the sub-surface shell. Speed and reciprocity of iodochloride emulsions can be improved by localized addition of known in the art reciprocity-controlling iridium dopants in relation to high iodide region of the grain. By carefully incorporating reciprocity-controlling dopant within a well defined band within a grain the difficulties of the prior art can be overcome.

    Abstract translation: 公开了一种辐射敏感性乳剂,其包含基于总银含有0.05至3摩尔%碘化物的立方体卤化银颗粒和铱配位络合物掺杂剂,其中(i)碘化物以受控的非 - - 均匀分布,形成含有至少50%的总银,不含碘离子的表面壳,厚度大于的核心,以及含有最大碘化物浓度的亚表面壳,和(ⅱ)铱配位络合物 掺杂剂结合到子表面壳体中或引入芯部的区域中,该区域从底表面壳体延伸到总银的60%到晶粒内。 通过本领域已知的互易控制铱掺杂剂相对于颗粒的高碘化物区域的局部添加可以提高碘氯化物乳剂的速度和互惠。 通过将互易控制掺杂剂小心地结合在晶粒内的良好限定的带内,可以克服现有技术的困难。

    Robust process for the preparation of high chloride emulsions
    26.
    发明授权
    Robust process for the preparation of high chloride emulsions 失效
    用于制备高氯化物乳液的坚固的工艺

    公开(公告)号:US06048683A

    公开(公告)日:2000-04-11

    申请号:US218683

    申请日:1998-12-22

    CPC classification number: G03C1/015 G03C1/035 G03C1/07

    Abstract: A method is disclosed of manufacturing radiation-sensitive emulsions by a pulsed flow double-jet process in which high chloride silver halide grains are grown in the presence of a thioether ripening agent in the dispersing medium in the reaction vessel the silver halide grains exhibiting an average grain roundness coefficient n in the range of from 2 to less than 15.

    Abstract translation: 公开了一种通过脉冲流双喷射法制造辐射敏感乳剂的方法,其中高氯化物卤化银颗粒在硫醚熟化剂存在下在反应容器中的分散介质中生长,卤化银颗粒呈平均值 颗粒圆度系数n在2到小于15的范围内。

    Printhead including particulate tolerant filter
    27.
    发明授权
    Printhead including particulate tolerant filter 有权
    打印头包括颗粒容纳过滤器

    公开(公告)号:US08534818B2

    公开(公告)日:2013-09-17

    申请号:US12767822

    申请日:2010-04-27

    Abstract: A printhead includes a nozzle plate, a filter, and a plurality of walls. Portions of the nozzle plate define a plurality of nozzles. The filter, for example, a filter membrane, includes a plurality of pores grouped in a plurality of pore clusters. Each of the plurality of walls extends from the nozzle plate to the filter membrane to define a plurality of liquid chambers positioned between the nozzle plate and the filter membrane. Each liquid chamber of the plurality of liquid chambers is in fluid communication with a respective one of the plurality of nozzles. Each liquid chamber of the plurality of liquid chambers is in fluid communication with the plurality of pores of a respective one of the plurality of pore clusters. The respective one of the plurality of pore clusters includes two pore sub-clusters spaced apart from each other by a non-porous portion of the filter membrane.

    Abstract translation: 打印头包括喷嘴板,过滤器和多个壁。 喷嘴板的一部分限定多个喷嘴。 过滤器,例如过滤膜,包括分组在多个孔群中的多个孔。 多个壁中的每一个从喷嘴板延伸到过滤膜以限定位于喷嘴板和过滤膜之间的多个液体室。 多个液体室中的每个液体室与多个喷嘴中的相应一个流体连通。 多个液体室中的每个液体室与多个孔群中的相应一个的多个孔流体连通。 多个孔群中的相应一个包括通过过滤膜的无孔部分彼此间隔开的两个孔子群。

    PRINTHEAD INCLUDING PARTICULATE TOLERANT FILTER
    28.
    发明申请
    PRINTHEAD INCLUDING PARTICULATE TOLERANT FILTER 有权
    包括颗粒容器过滤器

    公开(公告)号:US20110261123A1

    公开(公告)日:2011-10-27

    申请号:US12767822

    申请日:2010-04-27

    Abstract: A printhead includes a nozzle plate, a filter, and a plurality of walls. Portions of the nozzle plate define a plurality of nozzles. The filter, for example, a filter membrane, includes a plurality of pores grouped in a plurality of pore clusters. Each of the plurality of walls extends from the nozzle plate to the filter membrane to define a plurality of liquid chambers positioned between the nozzle plate and the filter membrane. Each liquid chamber of the plurality of liquid chambers is in fluid communication with a respective one of the plurality of nozzles. Each liquid chamber of the plurality of liquid chambers is in fluid communication with the plurality of pores of a respective one of the plurality of pore clusters. The respective one of the plurality of pore clusters includes two pore sub-clusters spaced apart from each other by a non-porous portion of the filter membrane.

    Abstract translation: 打印头包括喷嘴板,过滤器和多个壁。 喷嘴板的一部分限定多个喷嘴。 过滤器,例如过滤膜,包括分组在多个孔群中的多个孔。 多个壁中的每一个从喷嘴板延伸到过滤膜以限定位于喷嘴板和过滤膜之间的多个液体室。 多个液体室中的每个液体室与多个喷嘴中的相应一个流体连通。 多个液体室中的每个液体室与多个孔群中的相应一个的多个孔流体连通。 多个孔群中的相应一个包括通过过滤膜的无孔部分彼此间隔开的两个孔子群。

    MICROVALVE FOR CONTROL OF COMPRESSED FLUIDS
    29.
    发明申请
    MICROVALVE FOR CONTROL OF COMPRESSED FLUIDS 审中-公开
    用于控制压缩流体的微量元件

    公开(公告)号:US20110073788A1

    公开(公告)日:2011-03-31

    申请号:US12570312

    申请日:2009-09-30

    Abstract: A micro-electromechanical device for controlling compressed fluid flow is provided. A chamber includes a fluid flow inlet port, a high pressure region exceeding 30 bar, and a fluid flow outlet port. A moveable micro-electromechanical valve is positioned to contact the fluid flow outlet port when the moveable micro-electromechanical valve is in a first position. An electrical connection to the moveable micro-electromechanical valve provides an electrical pulse train to the moveable micro-electromechanical valve to actuate the valve at a rate of 10 KHz or more to move the valve in order to control fluid communication between the high pressure region and a low pressure region downstream from the fluid flow outlet port.

    Abstract translation: 提供了一种用于控制压缩流体流动的微机电装置。 腔室包括流体流入口,高压区域超过30巴,以及流体流出口。 当可移动的微机电阀处于第一位置时,可移动的微机电阀定位成接触流体流出口。 与可移动的微机电阀的电连接提供到可移动微机电阀的电脉冲串,以10KHz或更高的速率驱动阀,以便移动阀,以便控制高压区和 在流体出口端口下游的低压区域。

    Process for the deposition of uniform layer of particulate material
    30.
    发明授权
    Process for the deposition of uniform layer of particulate material 失效
    沉积均匀颗粒材料层的工艺

    公开(公告)号:US07223445B2

    公开(公告)日:2007-05-29

    申请号:US10815026

    申请日:2004-03-31

    Abstract: A process for the deposition of particulate material of a desired substance on a surface includes: (i) charging a particle formation vessel with a compressed fluid; (ii) introducing into the particle formation vessel a first feed stream comprising a solvent and the desired substance dissolved therein and a second feed stream comprising the compressed fluid, wherein the desired substance is less soluble in the compressed fluid relative to its solubility in the solvent and the solvent is soluble in the compressed fluid, and wherein the first feed stream is dispersed in the compressed fluid, allowing extraction of the solvent into the compressed fluid and precipitation of particles of the desired substance; (iii) exhausting compressed fluid, solvent and the desired substance from the particle formation vessel at a rate substantially equal to the rate of addition of such components to the vessel in step (ii) through a restrictive passage to a lower pressure whereby the compressed fluid is transformed to a gaseous state and a flow of particles of the desired substance is formed; and (iv) exposing a receiver surface to the exhausted flow of particles of the desired substance and depositing a uniform layer of particles on the receiver surface.

    Abstract translation: 将所需物质的颗粒材料沉积在表面上的方法包括:(i)用压缩流体填充颗粒形成容器; (ii)向颗粒形成容器中引入包含溶剂和所需物质溶解在其中的第一进料流和包含压缩流体的第二进料流,其中所需物质相对于其在溶剂中的溶解度较不溶于压缩流体 并且溶剂可溶于压缩流体中,并且其中第一进料流分散在压缩流体中,允许将溶剂萃取到压缩流体中并沉淀所需物质的颗粒; (iii)通过限制性通道将压缩流体,溶剂和所需物质从所述颗粒形成容器排出,其速率基本上等于步骤(ii)中通过限制性通道将这些组分加入到容器中的速率,由此压缩流体 转化为气态,形成所需物质的颗粒流; 和(iv)将接收器表面暴露于所需物质的排出的颗粒流中,并在接收器表面上沉积均匀的颗粒层。

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