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    Modified mineral filler for thermosets
    21.
    发明授权
    Modified mineral filler for thermosets 失效
    改性矿物填料用于热固性材料

    公开(公告)号：US6011087A

    公开(公告)日：2000-01-04

    申请号：US995729

    申请日：1997-12-22

    Applicant: Carl J. Marshall ,  Thomas J. Lynch ,  Gary M. Freeman

    Inventor： Carl J. Marshall ,  Thomas J. Lynch ,  Gary M. Freeman

    IPC: C08K9/04 ,  C08K9/06 ,  C09C1/42 ,  C09C3/12 ,  C08K3/00

    CPC classification number: C09C1/42 ,  C08K9/04 ,  C08K9/06 ,  C09C3/12 ,  C01P2004/54 ,  C01P2004/61 ,  C01P2006/12 ,  C01P2006/22 ,  C01P2006/80

    Abstract: Modified mineral fillers, derived from either a coarse particle kaolin clay or a coarse particle ATH, having excellent utility in thermoset polymers as low paste viscosity fillers are disclosed. The method of treatment involves the use of specific weight ratio combinations of a silane and a long chain aliphatic alcohol. The treatment of clay can also involve the auxiliary use of a surfactant in small amounts, which is utilized to emulsify the silane and aliphatic alcohol treatment components in water either individually or as a co-emulsion blend prior to their addition to the clay. The surfactant, which is preferably a nonionic surfactant having a HLB value of 12-18, aides in uniformly treating all the clay particle surfaces with the silane/alcohol treatment combination. Coarse particle clays having general utility in the invention are those having an average Stokes equivalent particle diameter of at least 3.0 microns, while the coarse particle ATH fillers having general utility in the invention are those having a BET surface area value less than 5.0 m.sup.2 /g. Clays or ATH so treated with the inventive silane/alcohol treatment provide unique viscosity reduction benefits in thermoset polymers unattainable by using either treatment additive alone in any amount. This low viscosity characteristic allows the treated mineral products to be used at high loadings in various thermoset compounds, as fillers or extenders, which is advantageous in terms of reducing cost and/or gaining certain performance properties, such as physical reinforcement, composite surface smoothness or flame retardancy.

    Abstract translation: 公开了一种衍生自粗颗粒高岭土或粗颗粒ATH的改性矿物填料，在热固性聚合物中作为低粘度粘度填料具有极好的用途。 处理方法包括使用硅烷和长链脂族醇的特定重量比组合。 粘土的处理还可以涉及少量辅助使用表面活性剂，其用于在水中单独地或作为共乳液共混物将硅烷和脂族醇处理组分在添加到粘土之前乳化。 表面活性剂，其优选HLB值为12-18的非离子表面活性剂，用硅烷/醇处理组合均匀处理所有粘土颗粒表面的助剂。 在本发明中具有通用效用的粗颗粒粘土是具有平均斯托克斯当量粒径至少为3.0微米的颗粒粘土，而本发明中具有通用效用的粗颗粒ATH填料是BET表面积值小于5.0m 2 / g 。 用本发明的硅烷/醇处理处理的粘土或ATH在热固性聚合物中提供了独特的降粘效果，不可以通过单独使用任何一种处理添加剂来达到。 这种低粘度特性允许经处理的矿物产品以高负荷使用于各种热固性化合物作为填料或增量剂，这在降低成本和/或获得某些性能性能方面是有利的，例如物理强化，复合表面光滑度或 阻燃性

    Zirconium modified synthetic alkali metal silicate pigment and method of making
    22.
    发明授权
    Zirconium modified synthetic alkali metal silicate pigment and method of making 失效
    锆改性合成碱金属硅酸盐颜料及其制法

    公开(公告)号：US5814143A

    公开(公告)日：1998-09-29

    申请号：US976230

    申请日：1997-11-21

    Applicant: Gary M. Freeman ,  Richard C. Zielke

    Inventor： Gary M. Freeman ,  Richard C. Zielke

    IPC: C09C1/28 ,  C09C1/40 ,  C09C3/06 ,  C08K3/00

    CPC classification number: C09C1/28 ,  C09C1/405 ,  C09C3/063 ,  C01P2002/02 ,  C01P2004/62 ,  C01P2004/82 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/16 ,  C01P2006/17 ,  C01P2006/19 ,  C01P2006/60

    Abstract: A synthetic alkali metal silicate pigment is modified with a source of a water soluble zirconium ion to form an oxy-hydroxy zirconium species precipitate on the pigment surface. The surface modified pigment is made by slurrying the pigment and reacting it with the source of a water soluble zirconium ion. The surface modified pigment provides improvements over conventional synthetic alkali metal silicate pigments in terms of optical properties, particularly in paper applications, and physical properties, particularly in rubber applications. The surface modified pigment is also useful as an extender or replacement for TiO.sub.2, a conventional synthetic alkali metal silicate such as a sodium-aluminosilicate pigment, a clay, a calcined clay or the like.

    Abstract translation: 合成的碱金属硅酸盐颜料用水溶性锆离子源改性以在颜料表面上形成氧 - 羟基锆类沉淀物。 表面改性颜料通过将颜料浆化并使其与水溶性锆离子源反应而制备。 表面改性颜料在光学性能，特别是纸张应用和物理性能方面，特别是在橡胶应用方面，提供了优于常规合成碱金属硅酸盐颜料的改进。 表面改性颜料也可用作TiO 2的增量剂或替代物，TiO 2是常规的合成碱金属硅酸盐，例如钠 - 硅铝酸盐颜料，粘土，煅烧粘土等。

    Pigment system for paints
    24.
    发明授权
    Pigment system for paints 失效
    油漆颜料系统

    公开(公告)号：US5112402A

    公开(公告)日：1992-05-12

    申请号：US753545

    申请日：1991-09-03

    Applicant: Gary M. Freeman ,  Thad T. Broome

    Inventor： Gary M. Freeman ,  Thad T. Broome

    IPC: C09C1/40

    CPC classification number: C09C1/405 ,  C09C1/402 ,  C09C1/42 ,  C01P2004/20 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2004/82 ,  C01P2006/19 ,  C01P2006/22 ,  C01P2006/60

    Abstract: The present invention relates to slurries of synthetic alkali metal silicates with fine particles kaolin clay. The slurries consists of at least 50% solids which solids comprise an approximately 50:50 combination of the fine kaolin clay and the synthetic alkali metal silicate (SAMS). The integrated composition of the SAMS products is an entity having an overall composition ofxM.sub.2 O:Al.sub.2 O.sub.3 :ySiO.sub.2 Owhere x is the number of moles of alkali metal oxide and is an integer from 0.01 to 2.0, M is an alkali metal, y is the number of miles of SiO.sub.2 in the unique SAMS composition, and z is the number of moles of bound water and is an integer ranging from 1.0 to 5.0. The composition essentially comprises altered kaolin clay platelets with an integral rim or protuberance of essentially amorphous alkali metal silicate-kaolin reaction product. The slurry is useful in latex paint systems.

    Abstract translation: 本发明涉及合成碱金属硅酸盐与细颗粒高岭土的浆料。 浆料由至少50％的固体组成，其中固体包含细高岭土和合成的碱金属硅酸盐（SAMS）的约50:50的组合。 SAMS产品的整体组成是具有xM 2 O：Al 2 O 3：ySiO 2的总体组成的实体，其中x是碱金属氧化物的摩尔数，为0.01-2.0的整数，M是碱金属，y是数 的独特SAMS组合物中的英里的SiO 2，z是结合水的摩尔数，为1.0至5.0的整数。 组合物基本上包括具有基本上无定形的碱金属硅酸盐 - 高岭土反应产物的整体边缘或突起的改变的高岭土血小板。 该浆料可用于乳胶漆系统。

    Flow monitoring device
    25.
    发明授权
    Flow monitoring device 失效
    流量监测装置

    公开(公告)号：US4480467A

    公开(公告)日：1984-11-06

    申请号：US444999

    申请日：1982-11-29

    Applicant: James R. Harter ,  Gary M. Freeman

    Inventor： James R. Harter ,  Gary M. Freeman

    IPC: G01F1/684 ,  G01F1/698 ,  G01F1/68 ,  G01F15/14

    CPC classification number: G01F1/684 ,  G01F1/6842 ,  G01F1/698

    Abstract: The flow monitoring device comprises a housing having a passageway therethrough for liquid flow through the housing. The passageway has an inlet opening and an outlet opening. A first thermistor is provided for sensing the temperature of the liquid in the passageway at a place near the inlet opening. A heating resistor is provided for heating the liquid at a place near the outlet opening and a second thermistor is provided for sensing the temperature of the liquid at the place near the outlet opening. A control circuit controls the input of heat energy to the heating resistor for heating the liquid just enough to maintain a predetermined temperature differential between the first and second thermistors. The passageway has a first larger-in-cross-section passageway portion at the place of the first thermistor for enhancing temperature sensing, a second larger-in-cross-section passageway portion at the place of the second thermistor for enhancing temperature sensing and a smaller-in-cross-section passage between the first and second larger passageway portions to cause a higher flow rate between those portions to thermally isolate those portions thereby to minimize, if not altogether eliminate, thermal pollution between those portions. The first and second passageway portions gradually widen from their inlet and outlet ends to the larger-in-cross-section portions to minimize turbulent flow through said first and second portions.

    Abstract translation: 流量监测装置包括具有通过其的液体流过壳体的通道的壳体。 通道具有入口开口和出口开口。 提供第一热敏电阻用于感测在入口附近的通道处的液体的温度。 提供加热电阻器用于在出口附近的位置处加热液体，并且提供第二热敏电阻器用于感测在出口附近的位置处的液体的温度。 控制电路控制加热电阻器的热能输入，以加热液体足以保持第一和第二热敏电阻之间的预定温度差。 通道具有第一大截面通道部分，位于第一热敏电阻位置，用于增强温度感测，第二大截面通道部分位于第二热敏电阻的位置，用于增强温度感测和 第一和第二较大通道部分之间的较小的横截面通道，以在这些部分之间产生更高的流速，以使这些部分热隔离，从而最小化（如果不是完全消除）这些部分之间的热污染。 第一和第二通道部分从其入口端和出口端逐渐变宽到较大的横截面部分，以使通过所述第一和第二部分的湍流最小化。

    Low visibility landing system and method
    26.
    发明授权
    Low visibility landing system and method 有权
    低能见度着陆系统和方法

    公开(公告)号：US08374737B2

    公开(公告)日：2013-02-12

    申请号：US13243698

    申请日：2011-09-23

    Applicant: Robert S. Takacs ,  Gary M. Freeman ,  Glenn L. Connor

    Inventor： Robert S. Takacs ,  Gary M. Freeman ,  Glenn L. Connor

    IPC: G06F19/00

    CPC classification number: G05D1/0676 ,  G08G5/0021 ,  G08G5/025

    Abstract: A low visibility landing system is provided for guiding aircraft on landing approaches. The low visibility landing system may aid a pilot during landing in low visibility conditions such that an aircraft may descend to lower altitudes without visual contact with the runway than is possible with other landing systems. The system may use various navigational systems to produce a hybrid signal that may be more stable than individual signals of those navigational systems. The hybrid signal is compared to a predetermined landing approach plan to determine the deviation of the aircraft from the landing approach plan and to provide guidance to the pilot to get the aircraft back onto the landing approach plan. The system may also use multiple navigational systems to perform checks on an operation of a primary navigational system to ensure that the primary navigational system is operating accurately.

    Abstract translation: 提供低能见度的着陆系统，用于在着陆进近时引导飞机。 低能见度着陆系统可以在低能见度条件下着陆时帮助飞行员，使得飞行器可以下降到较低的高度，而不是与跑道的视觉接触，而不是与其他着陆系统相同。 该系统可以使用各种导航系统来产生可能比那些导航系统的单个信号更稳定的混合信号。 将混合信号与预定的着陆方法计划进行比较，以确定飞机与着陆进近计划的偏差，并向飞行员提供指导以使飞机返回到着陆进近计划。 该系统还可以使用多个导航系统对主导航系统的操作执行检查，以确保主导航系统准确地操作。

    Silane-treated clay production method, silane-treated clay and composition containing same
    29.
    发明授权
    Silane-treated clay production method, silane-treated clay and composition containing same 失效
    硅烷处理粘土生产方法，硅烷处理粘土和含有它们的组合物

    公开(公告)号：US6013699A

    公开(公告)日：2000-01-11

    申请号：US185641

    申请日：1998-11-04

    Applicant: Gary M. Freeman ,  Carl J. Marshall, Jr. ,  Walter O. Lackey ,  Masao Onizawa

    Inventor： Gary M. Freeman ,  Carl J. Marshall, Jr. ,  Walter O. Lackey ,  Masao Onizawa

    IPC: B60C1/00 ,  B60C13/04 ,  C04B20/10 ,  C08K9/06 ,  C09C1/42 ,  C08K3/34

    CPC classification number: C09C1/42 ,  B60C1/00 ,  B60C1/0025 ,  B60C13/04 ,  C04B20/1051 ,  C08K9/06 ,  C01P2004/54 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2006/12 ,  C01P2006/19 ,  C01P2006/22 ,  C01P2006/60 ,  Y10S152/12

    Abstract: An effective production method for silane-treated clays having exceptional reinforcing effects with respect to rubber, and compositions using these silane-treated clays are offered. With the silane-treated clay production method, a functional silane is predispersed or emulsified in water by means of a surfactant in order to mix the functional silane with kaolin clay and thereby uniformly surface-treat the kaolin clay with the functional silane. The surfactant should preferably be a non-ionic surfactant with an HLB value in the range of 8-18. The silane-treated clay formed by surface-treating kaolin clay by means of these functional silanes characteristically contains low residual levels of the non-ionic surfactants. The functional silanes can be either vinyl or sulfur functional silanes. The silane treated clays are useful as fillers or extenders in rubber compositions, particularly those employing silicas and/or carbon blacks.

    Abstract translation: 提供了对于橡胶具有优异的增强效果的硅烷处理粘土的有效制备方法，以及使用这些硅烷处理的粘土的组合物。 通过硅烷处理的粘土生产方法，通过表面活性剂将功能性硅烷预先分散或在水中乳化，以将功能性硅烷与高岭土混合，从而用功能性硅烷均匀地表面处理高岭土。 表面活性剂应优选为HLB值在8-18范围内的非离子表面活性剂。 通过这些功能性硅烷表面处理高岭土形成的硅烷处理粘土特征在于含有低残留水平的非离子表面活性剂。 功能硅烷可以是乙烯基或硫官能硅烷。 硅烷处理的粘土可用作橡胶组合物中的填料或增量剂，特别是使用二氧化硅和/或炭黑的那些。

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