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公开(公告)号:US10369086B2
公开(公告)日:2019-08-06
申请号:US15552751
申请日:2016-03-01
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Bradley D. Craig , Gregory A. Kobussen
Abstract: The present disclosure provides a composite material, a method of making and using the composite material and dental products made by hardening the composite material. The composite material includes a polymerizable component, ceramic fibers and nanoclusters. Each of the ceramic fibers of the composite material has a length and where the length of fifty percent of the ceramic fibers, based on a total number of the ceramic fibers, is at least 50 micrometers and the length of ninety percent of the ceramic fibers, based on the total number of the ceramic fibers, is no greater than 500 micrometers. The composite material can also include discrete non-fumed metal oxide nanoparticles. The composite material can be hardened to become any one of a dental restorative, a dental adhesive, a dental mill blank, a dental cement, a dental prostheses, an orthodontic device, an orthodontic adhesive, a dental casting material or a dental coating.
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公开(公告)号:US10350297B2
公开(公告)日:2019-07-16
申请号:US15521913
申请日:2015-10-16
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Bradley D. Craig
Abstract: The present application is directed to a dental material and a method of using the dental material. The dental material can include a hardenable resin; an initiator system; a filler; and from about 1 wt % to about 20 wt % zinc compound, based on the weight of the hardenable resin. The contrast ratio of the cured dental material increases by at least about 10 units after continuous exposure to an aqueous solution for 21 days.
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33.
公开(公告)号:US20190201296A1
公开(公告)日:2019-07-04
申请号:US16301211
申请日:2017-05-15
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Yizhong Wang , Zhisheng Yun , Eric S. Hansen , Joel D. Oxman , James D. Hansen , Bradley D. Craig , Tao Gong
CPC classification number: A61K6/002 , A61C9/0053 , A61K6/0017 , A61K6/10
Abstract: Disclosed herein are aqueous dental coating compositions and methods for enhancing contrast of intraoral surfaces for 3-dimensional digital scanning. The compositions include: an aqueous solvent system; a water soluble polymer present at no greater than 5 wt. %, based on the total weight of the aqueous dental coating composition; hydrophilic particles; and hydrophobic particles, wherein the aqueous dental coating composition is a dispersion or a dispersion of the hydrophilic particles and hydrophobic particles in the aqueous solvent system can be formed by shaking the composition for 30 seconds.
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34.
公开(公告)号:US20190000723A1
公开(公告)日:2019-01-03
申请号:US15775040
申请日:2016-10-11
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Michael Jahns , Markus Mikulla , Robert F. Peez , Adrian S. Eckert , Rainer A. Guggenberger , Simone Raynoschek , Afshin Falsafi , Bradley D. Craig , Jimmie R. Baran, JR. , Joel D. Oxman
Abstract: The invention relates to a kit of parts for preparing a glass ionomer composition for dental use, the kit of parts comprising a Powder Part P and a Liquid Part L, Powder Part P comprising: acid-reactive inorganic filler, Liquid Part L comprising: water, complexing agent, polyacid, either the Powder Part P or the Liquid Part L or the Powder Part P and the Liquid Part L comprising non-aggregated nano-sized particles based on silica or alumina, the composition obtained by combining the components of Powder Part P and Liquid Part L before hardening comprising the components in the following amounts: non-aggregated nano-sized particles: from 0.1 to 15 wt.-%, acid-reactive filler in an amount from 50 to 75 wt.-%, polyacid: 7 to 20 wt.-%, complexing agent: 0.5 to 3 wt.-%, water: 5 to 18 wt.-%, wt.-% with respect to the weight of the whole composition.
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公开(公告)号:US20230372161A1
公开(公告)日:2023-11-23
申请号:US18031228
申请日:2021-10-15
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Bradley D. Craig , Saurabh Batra , Paul J. Homnick , Jamie Vadnais , Satinder K. Nayar
CPC classification number: A61F13/36 , A61F13/2008 , A61F13/15203 , A61F15/001 , A61C17/08
Abstract: An absorbent article includes at least two absorbent pads spaced apart from each other. The absorbent article further includes an interconnect member. Each absorbent pad includes an absorbent material configured to absorb a liquid. Each absorbent pad further includes an outer surface. The interconnect member joins the outer surfaces of the at least two absorbent pads. The interconnect member is stretchable.
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公开(公告)号:US11207246B2
公开(公告)日:2021-12-28
申请号:US16485952
申请日:2018-03-02
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Mark B. Agre , Bradley D. Craig , Michael Jahns , William V. Chiu
Abstract: Disclosed herein are curable glass ionomer compositions that include a first paste and a second paste, and methods for using the disclosed compositions. The first paste includes water, a polyacid, and a non acid-reactive filler. The second paste includes water and an acid-reactive filler. At least one of the first paste and the second paste further includes substantially crystalline inorganic fibers. In some embodiments, the water content of the first paste and the second paste of the paste/paste GI composition disclosed herein is less than 20% by weight, based on the total weight of the composition.
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公开(公告)号:US11111320B2
公开(公告)日:2021-09-07
申请号:US16591055
申请日:2019-10-02
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: William H. Moser , Ann R. Fornof , Guy D. Joly , Serkan Yurt , Larry R. Krepski , Ahmed S. Abuelyaman , Afshin Falsafi , Bradley D. Craig , Joel D. Oxman , Babu N. Gaddam
IPC: C08F22/10 , C07F7/18 , C09J4/06 , C08F292/00 , A61K6/62 , A61K6/71 , A61K6/887 , C09D7/61 , C07C69/602 , C07F9/09 , C09D4/00 , C08K3/36
Abstract: Novel stress-reducing crosslinking oligomers that have application in dental restoratives, thin films, hardcoats, composites, adhesives, and other uses subject to stress reduction are described. The addition-fragmentation process of crosslinking results in a chain-transfer event that provides novel polymers that may be further functionalized. In addition, the addition-fragmentation oligomer comprises pendent functional groups that bond to a substrate by forming an ionic or covalent bond, or etch the substrate by chemically removing some material from the substrate.
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公开(公告)号:US11103425B2
公开(公告)日:2021-08-31
申请号:US16954742
申请日:2018-12-18
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Bradley D. Craig , Paul J. Homnick , Ahmed S. Abuelyaman , Thomas P. Klun
Abstract: The present disclosure provides an inorganic dental filler including a surface treated with at least one silane. Exemplary silanes described in the present disclosure for the surface treatment of the inorganic filler include silanes of Formula I and/or Formula II: (RSi)—(CR1R2)n—(NH—C(O)—O—CH2—CH2)q—N(R5)—C(O)—NH—(CH2—CH2—O)t—CR3R4—CH2-(A) Formula I (RSi)—(CR1R2)n—NH—C(O)—O—CR3R4-(L)q-CH2-(A) Formula II, wherein: RSi is a silane-containing group of the formula —Si(Yp)(R6)3-p, wherein Y is a hydrolysable group, R6 is a monovalent alkyl or aryl group, and p is 1, 2, or 3. Methods of making and using the surface treated inorganic dental fillers are also disclosed.
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公开(公告)号:US10751264B2
公开(公告)日:2020-08-25
申请号:US15315530
申请日:2015-06-08
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Bradley D. Craig , Joel D. Oxman , Thomas P. Klun , Richard B. Ross
Abstract: The present application is directed to a curable composition and a method for isolating a working area in a patient's mouth. The curable composition can include a borate-crosslinked polysiloxane, at least one ethylenically unsaturated monomer comprising at least two polymerizable groups, and an initiator.
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公开(公告)号:US20200230029A1
公开(公告)日:2020-07-23
申请号:US16485952
申请日:2018-03-02
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Mark B. Agre , Bradley D. Craig , Michael Jahns , William V. Chiu
Abstract: Disclosed herein are curable glass ionomer compositions that include a first paste and a second paste, and methods for using the disclosed compositions. The first paste includes water, a polyacid, and a non acid-reactive filler. The second paste includes water and an acid-reactive filler. At least one of the first paste and the second paste further includes substantially crystalline inorganic fibers. In some embodiments, the water content of the first paste and the second paste of the paste/paste GI composition disclosed herein is less than 20% by weight, based on the total weight of the composition.
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