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    High temperature high pressure apparatus
    51.
    发明授权
    High temperature high pressure apparatus 失效
    高温高压装置

    公开(公告)号：US4518334A

    公开(公告)日：1985-05-21

    申请号：US644362

    申请日：1984-08-27

    Applicant: Hiroshi Ishizuka

    Inventor： Hiroshi Ishizuka

    IPC: B01J3/06

    CPC classification number: B01J3/06 ,  B01J3/065 ,  Y10S425/026

    Abstract: A high temperature high pressure apparatus which comprises: an annular die having a straight cylindrical bore and a substantially conical face in adjacency outwards with each end thereof, a pair of tapered punches which are in opposed and axial alignment with the die so that a conical face of each punch is substantially in parallel with that of the die, a pair of inner gaskets, each of which is made of fired refractory and is arranged in direct abutment on the conical face of the punch and the bore of the die, a pair of outer gaskets, which are made of material of intermediate hardness level and is arranged in adjacency outside the inner gasket, and a pair of stopper rings of readily deformable but highly tough material and arranged in adjacency outwards to the outer gaskets.

    Abstract translation: 一种高温高压装置，包括：环形模具，其具有直的圆柱形孔和与其每端相邻的基本上圆锥形的表面，一对与模具相对且轴向对准的锥形冲头，使得圆锥形面 每个冲头基本上与模具平行，一对内垫圈，每个内垫圈由耐火材料制成，并且直接邻接在冲头的锥形表面和模具的孔上，一对 外部垫圈由中间硬度水平的材料制成，并且在内部垫圈外侧相邻地布置，以及一对容易变形但非常坚韧的材料的止动环，并且邻近地布置在外部垫圈上。

    High pressure reaction vessel for growing diamond on diamond seed and method therefor
    52.
    发明授权
    High pressure reaction vessel for growing diamond on diamond seed and method therefor 失效
    用于在钻石种子上生长钻石的高压反应容器及其方法

    公开(公告)号：US4322396A

    公开(公告)日：1982-03-30

    申请号：US148213

    申请日：1980-05-09

    Applicant: Herbert M. Strong

    Inventor： Herbert M. Strong

    IPC: B01J3/06 ,  C01B31/06

    CPC classification number: B01J3/065 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068

    Abstract: Reaction vessel construction is described for suppressing spontaneous diamond nucleation and simultaneously reducing the flaw content in the main body of diamond grown from diamond seed material by the process broadly disclosed in U.S. Pat. No. 3,297,407 to Wentorf, Jr.In the reaction vessel construction the body of catalyst-solvent metal is formed with at least one small tip projecting from the underside thereof. A single diamond seed is placed in contact with this (or each) tip. The underside of the plug of catalyst-solvent metal is in contact with a nucleation-suppressing disc, or layer, of a material different from the catalyst-solvent and selected from a specific group of materials. In each case the tip of catalyst-solvent metal projects through a hole in the disc or layer to make contact with the diamond seed material.

    Abstract translation: 描述了用于抑制自发金刚石成核并同时降低由金刚石种子材料生长的金刚石的主体中的缺陷含量的反应容器结构，这通过美国专利中广泛公开的方法。 在Wentorf，Jr.的第3,297,407号中，在反应容器结构中，催化剂 - 溶剂金属体形成有从其下侧突出的至少一个小尖端。 单个金刚石种子与该（或每个）尖端接触。 催化剂 - 溶剂金属的塞子的下侧与不同于催化剂 - 溶剂并选自特定材料组的材料与成核抑制盘或层接触。 在每种情况下，催化剂 - 溶剂金属的尖端通过盘或层中的孔突出以与金刚石种子材料接触。

    Apparatus for making diamonds
    54.
    发明授权
    Apparatus for making diamonds 失效
    用于制作钻石的装置

    公开(公告)号：US4197066A

    公开(公告)日：1980-04-08

    申请号：US8485

    申请日：1979-02-02

    Applicant: George C. Kennedy

    Inventor： George C. Kennedy

    IPC: B01J3/06 ,  B30B11/32

    CPC classification number: B01J3/065 ,  B30B11/004

    Abstract: A piston type system for forming industrial diamonds is provided with a pressure vessel which includes a tungsten carbide member having a central opening which has a tapered mouth at one end, and which is lined with a salt bushing. A charge including invar and graphite to be converted to diamond is inserted within the pressure chamber inside the salt bushing. An end load plate has a central opening of substantially the same diameter as the opening in the salt bushing and has a tapered flange which fits into the tapered mouth in the tungsten carbide pressure vessel. A tungsten carbide piston which has a diameter about 0.003 inch less than the diameter of the opening in the end plate, and which has a lead gasket between its surface and that of the opening in the end plate, is forced through the end plate and applies high pressure at high temperatures to the charge, thereby converting the graphite to diamond after the passage of a suitable period of time. The tungsten carbide piston need only have the diameter of the inner diameter of the salt bushing, instead of a diameter equal to the full I.D. of the tungsten carbide pressure vessel.

    Abstract translation: 用于形成工业金刚石的活塞式系统设置有压力容器，该压力容器包括具有中心开口的碳化钨构件，该中心开口在一端具有锥形口，并且内衬有盐套管。 将含有金刚石和石墨的电荷插入盐套内的压力室内。 端部装载板具有与盐套管中的开口基本相同的直径的中心开口，并具有与碳化钨压力容器中的锥形口部相配合的锥形凸缘。 具有比端板中的开口直径大约0.003英寸并且在其表面和端板中的开口之间具有引线垫圈的直径约为0.003英寸的碳化钨活塞被迫通过端板并施加 在高温下对电荷施加高压，从而在经过合适的时间后将石墨转化为金刚石。 碳化钨活塞仅需具有盐套内径的直径，而不是直径等于完整的I.D. 的碳化钨压力容器。

    High pressure apparatus
    56.
    发明授权
    High pressure apparatus 失效
    高压设备

    公开(公告)号：US3988087A

    公开(公告)日：1976-10-26

    申请号：US651755

    申请日：1976-01-23

    Applicant: Hiroshi Ishizuka

    Inventor： Hiroshi Ishizuka

    IPC: B01J3/06 ,  B30B11/32

    CPC classification number: B01J3/065 ,  Y10S425/026 ,  Y10S425/115

    Abstract: A high pressure apparatus for synthesizing diamonds which comprises a pair of opposed tapered pistons each having a truncated end surface, a pair of hollow truncated-conical piston protectors each of which is made of a ductile metal and arranged on the tapered piston surface, and annular die member having a substantially cylindrical wall of a diameter larger than that of each piston truncated end surface, a hollow cylindrical body made of less compressibility coefficient material than the die material and having an outer diameter substantially same or slightly smaller than the diameter of said truncated end surface of each pistons and positioned coaxially within the die cylindrical wall, and gaskets placed respectively at the ends of said cylindrical body.

    Abstract translation: 一种用于合成金刚石的高压装置，其包括一对具有截头端面的相对的锥形活塞，一对中空截锥形活塞保护器，每个都由延性金属制成，并设置在锥形活塞表面上，环形 模具构件具有直径大于每个活塞截头端面的直径的基本上圆柱形的壁;中空圆柱体，由比模具材料更小的压缩系数材料制成，并具有与所述截顶端的直径基本相同或略小的外径 每个活塞的端面并且同轴地定位在模具圆筒壁内，并且垫圈分别放置在所述圆柱体的端部。

    Device for generating high pressures and temperatures
    57.
    发明授权
    Device for generating high pressures and temperatures 失效
    用于产生高压和高温的装置

    公开(公告)号：US3895894A

    公开(公告)日：1975-07-22

    申请号：US35373873

    申请日：1973-04-23

    Applicant: KRUPP GMBH

    Inventor： BIERMANN KLAUS ,  BURBACH JURGEN ,  GIMPEL HORST ,  ZIRPINS BURCKHARD

    IPC: B01J3/06 ,  B29C11/00 ,  B29F5/00

    CPC classification number: B01J3/065

    Abstract: A device for generating high pressures and temperatures, in which in the pressure chamber of a high strength metallic pressure container, a charge of material laterally surrounded by electrically insulating material by means of two piston rams movable in opposite direction with regard to each other and sealed relative to the pressure container is subjected to pressure while being electrically heated. The pressure container comprises at least two axially aligned metallic ring members of high strength hard metal which define a pressure chamber, while between the rings and between the rings and a matrix surrounding the rings, pressure resistant electrically insulating material is provided. Outside the pressure chamber, sealing means of plastically deformable strong metallic material are provided between the piston rams and the rings.

    Abstract translation: 一种用于产生高压和高温的装置，其中在高强度金属压力容器的压力室中，由电绝缘材料横向包围的材料的电荷通过相对于彼此相反方向可移动的两个活塞凸起而密封 相对于压力容器在电加热的同时承受压力。 压力容器包括高强度硬金属的至少两个轴向排列的金属环构件，其限定了压力室，同时在环之间和环之间以及围绕环的基体之间提供耐压电绝缘材料。 在压力室外面，在活塞杆和环之间提供可塑性变强的金属材料的密封装置。

    Method and device for providing high pressure and high temperature
    58.
    发明授权
    Method and device for providing high pressure and high temperature 失效
    用于提供高压和高温的方法和装置

    公开(公告)号：US3695797A

    公开(公告)日：1972-10-03

    申请号：US3695797D

    申请日：1970-08-26

    Applicant: UK NI KONSHUKTORSKO T I SINT S

    Inventor： BAKUL VALENTIN NIKOLAEVICH ,  PRIKHNA ALEXEI IOSIFOVICH ALEX ,  SHULZHENKO ALEXANDR ALEXANDROV ,  GERASIMOVICH ALEXEI VLADIMIROV

    IPC: B01J3/06 ,  B30B11/32

    CPC classification number: B01J3/065 ,  Y10S425/026

    Abstract: A die pair for use in high temperature high pressure apparatus for use in the synthesis of super hard materials such as diamonds, cubic boron nitride or the like in which the dies include an annular step structure on confronting cooperating faces of the dies to afford over an extended period of time stable, repetitive temperatures in the order of thousands of degrees centigrade and pressures in the order of 60 thousand atmospheres; the confronting die faces having recesses forming a pressure chamber and step structure cooperating with a deformable container of a thermo-and-electro-insulating material such as lithographic stone etc. which deforms as heated and has pressure applied thereto to form an annular sealing ''''burr'''' of a greater volume than an outer surrounding annular slot filled with a porous plastic, electro-insulating material such as ''''technical rubber'''' etc.; the deformable container being of a volume to fill the space both inwardly and outwardly of the material being treated up to the confronting edge of annular surrounding steps; the outer steps having radial, transverse slots; staggered in confronting relation; for readily accommodating the porous plastic outer seal.

    Abstract translation: 用于合成超硬材料如金刚石，立方氮化硼等的高温高压装置中的模具对，其中模具包括在模具的配合面上面的环状台阶结构，以提供超过 延长的时间段稳定，重复温度在数千摄氏度，压力在6万个大气压的数量级; 相对的模具面具有形成压力室的凹部和与诸如平版印刷石等的热电绝缘材料的可变形容器配合的阶梯结构，其在加热时变形并施加压力以形成环形密封“毛刺 “比填充有多孔塑料的外围环形槽更大的体积，诸如”技术橡胶“之类的电绝缘材料; 所述可变形容器具有一个体积，以便将被处理的材料的内部和外部填充到环形围绕步骤的相对边缘; 所述外部台阶具有径向横向狭槽; 交错对立; 用于容易地容纳多孔塑料外部密封件。

    High-pressure device
    59.
    发明授权
    High-pressure device 失效
    高压设备

    公开(公告)号：US3642412A

    公开(公告)日：1972-02-15

    申请号：US3642412D

    申请日：1969-09-30

    Applicant: ADAMANT LAB PROPRIETARY LTD

    Inventor： POPE NOEL C ,  KEMPIS EDWARD B ,  O'DONOVAN KEVIN H J

    IPC: B01J3/06 ,  B29C3/00

    CPC classification number: B01J3/065 ,  B30B11/004 ,  Y10S425/026

    Abstract: This invention relates to high-pressure dies normally used for use in the synthesis of diamonds. The die comprises a die ring having a through cavity within which there is formed a pressure chamber that is lined with a pyrophyllite sleeve. Respectively entering the ends of the sleeve are two plungers. These plungers are capable of sliding in the sleeve until near the end of their compressive strokes so that little or no axial pressure is applied to the ends of the sleeve.

    Abstract translation: 本发明涉及通常用于合成钻石的高压模具。 模具包括具有通孔的模具环，在该模腔中形成有与叶蜡石套筒相衬的压力室。 分别进入套筒的端部是两个柱塞。 这些柱塞能够在套筒中滑动直到接近其压缩冲程的结束，使得很少或没有轴向压力施加到套筒的端部。

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