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公开(公告)号:US11378719B2
公开(公告)日:2022-07-05
申请号:US17004562
申请日:2020-08-27
Applicant: Corning Incorporated
Inventor: Jaymin Amin , Shandon Dee Hart , Karl William Koch, III , Carlo Anthony Kosik Williams , Thien An Thi Nguyen
IPC: G02F1/13357 , G02B1/00 , G02F1/1335
Abstract: An article is described herein that includes: a translucent substrate comprising opposing major surfaces; and an optical film structure disposed on a first major surface of the substrate, the optical film structure comprising an outer surface and a plurality of periods such that each period comprises an alternating low refractive index layer and high refractive index layer. The article exhibits a hardness of 10 GPa or greater measured at an indentation depth of about 100 nm by a Berkovich Indenter Hardness Test. Further, the article exhibits a single side average photopic light reflectance of at least 50% of non-polarized light as measured at the outer surface from near-normal incidence to an incident angle of 60 degrees over a portion of at least 10 nm within the visible spectrum. In addition, each low refractive index layer comprises SiO2 or doped-SiO2 and each high refractive index layer comprises AlOxNy, SiOxNy, SiuAlvOxNy, SiNx or ZrO2.
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公开(公告)号:US11267973B2
公开(公告)日:2022-03-08
申请号:US14707106
申请日:2015-05-08
Applicant: CORNING INCORPORATED
Inventor: Jaymin Amin , Shandon Dee Hart , Karl William Koch, III , Eric Louis Null , Xu Ouyang , Charles Andrew Paulson , James Joseph Price
Abstract: Embodiments of durable, anti-reflective articles are described. In one or more embodiments, the article includes a substrate and an anti-reflective coating disposed on the major surface. The article exhibits an average light transmittance of about 94% or greater over an optical wavelength regime and/or an average light reflectance of about 2% or less over the optical wavelength regime, as measured from an anti-reflective surface. In some embodiments, the article exhibits a maximum hardness of about 8 GPa or greater as measured by a Berkovich Indenter Hardness Test along an indentation depth of about 50 nm or greater and a b* value, in reflectance, in the range from about −5 to about 1 as measured on the anti-reflective surface only at all incidence illumination angles in the range from about 0 degrees to about 60 degrees under an International Commission on Illumination illuminant.
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公开(公告)号:US20210168957A1
公开(公告)日:2021-06-03
申请号:US17170147
申请日:2021-02-08
Applicant: CORNING INCORPORATED
Inventor: Jaymin Amin , Joshua Michael Jacobs , Jonathan David Pesansky , Kevin Barry Reiman , Ananthanarayanan Subramanian
Abstract: Disclosed are device display screen protectors comprising a first strengthened substrate sized to cover a display screen of an electronic device, the first strengthened substrate having a central tension value in the range greater than 0 MPa and less than 20 MPa, a surface having a Knoop lateral cracking scratch threshold of at least 3 N.
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公开(公告)号:US20210063607A1
公开(公告)日:2021-03-04
申请号:US17004562
申请日:2020-08-27
Applicant: Corning Incorporated
Inventor: Jaymin Amin , Shandon Dee Hart , Karl William Koch, III , Carlo Anthony Kosik Williams , Thien An Thi Nguyen
IPC: G02B1/00 , G02F1/13357
Abstract: An article is described herein that includes: a translucent substrate comprising opposing major surfaces; and an optical film structure disposed on a first major surface of the substrate, the optical film structure comprising an outer surface and a plurality of periods such that each period comprises an alternating low refractive index layer and high refractive index layer. The article exhibits a hardness of 10 GPa or greater measured at an indentation depth of about 100 nm by a Berkovich Indenter Hardness Test. Further, the article exhibits a single side average photopic light reflectance of at least 50% of non-polarized light as measured at the outer surface from near-normal incidence to an incident angle of 60 degrees over a portion of at least 10 nm within the visible spectrum. In addition, each low refractive index layer comprises SiO2 or doped-SiO2 and each high refractive index layer comprises AlOxNy, SiOxNy, SiuAlvOxNy, SiNx or ZrO2.
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公开(公告)号:USRE48200E1
公开(公告)日:2020-09-08
申请号:US16045438
申请日:2018-07-25
Applicant: Corning Incorporated
Inventor: Jaymin Amin , George Halsey Beall , Charlene Marie Smith
Abstract: The invention relates to glass articles suitable for use as electronic device housing/cover glass which comprise a glass ceramic material. Particularly, a cover glass comprising an ion-exchanged glass ceramic exhibiting the following attributes (1) optical transparency, as defined by greater than 90% transmission at 400-750 nm; (2) a fracture toughness of greater than 0.6 MPa·m1/2; (3) a 4-point bend strength of greater than 350 MPa; (4) a Vickers hardness of at least 450 kgf/mm2 and a Vickers median/radial crack initiation threshold of at least 5 kgf; (5) a Young's Modulus ranging between about 50 to 100 GPa; (6) a thermal conductivity of less than 2.0 W/m° C., and (7) and at least one of the following attributes: (i) a compressive surface layer having a depth of layer (DOL) greater and a compressive stress greater than 400 MPa, or, (ii) a central tension of more than 20 MPa.
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公开(公告)号:US20190223309A1
公开(公告)日:2019-07-18
申请号:US16363208
申请日:2019-03-25
Applicant: CORNING INCORPORATED
Inventor: Jaymin Amin , Joshua Michael Jocobs , Jonathan David Pesansky , Kevin Barry Reiman , Ananthanarayanan Subramanian
CPC classification number: H05K5/03 , B32B7/12 , B32B17/06 , B32B17/10036 , B32B17/10091 , B32B17/10119 , B32B17/10137 , B32B17/10743 , B32B17/10761 , B32B17/1077 , B32B17/10788 , B32B17/10798 , B32B2307/584 , B32B2457/20 , C03C3/093 , C03C21/002 , C03C21/005 , C03C23/007 , H05K5/0017
Abstract: Disclosed are device display screen protectors comprising a first strengthened substrate sized to cover a display screen of an electronic device, the first strengthened substrate having a central tension value in the range greater than 0 MPa and less than 20 MPa, a surface having a Knoop lateral cracking scratch threshold of at least 3 N.
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公开(公告)号:US10244648B2
公开(公告)日:2019-03-26
申请号:US15711379
申请日:2017-09-21
Applicant: CORNING INCORPORATED
Inventor: Jaymin Amin , Joshua Michael Jacobs , Jonathan David Pesansky , Kevin Barry Reiman , Ananthanarayanan Subramanian
Abstract: Disclosed are device display screen protectors comprising a first strengthened substrate sized to cover a display screen of an electronic device, the first strengthened substrate having a central tension value in the range greater than 0 MPa and less than 20 MPa, a surface having a Knoop lateral cracking scratch threshold of at least 3 N.
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公开(公告)号:US20190047909A1
公开(公告)日:2019-02-14
申请号:US16165312
申请日:2018-10-19
Applicant: CORNING INCORPORATED
Inventor: Jaymin Amin , Benedict Osobomen Egboiyi , Jonathan David Pesansky , Kevin Barry Reiman , Rostislav Vatchev Roussev , Brian Paul Strines
IPC: C03C21/00 , C03C3/097 , C03C3/04 , C03C3/085 , C03C3/087 , G06F1/16 , C03C4/18 , C03C3/095 , C03C3/093 , C03C3/091 , H04B1/3827
Abstract: Chemically strengthened glass articles having at least one deep compressive layer extending from a surface of the article to a depth of at least about 45 μm within the article are provided. In one embodiment, the compressive stress profile includes a single linear segment extending from the surface to the depth of compression DOC. Alternatively, the compressive stress profile includes two linear portions: the first portion extending from the surface to a relatively shallow depth and having a steep slope; and a second portion extending from the shallow depth to the depth of compression. The strengthened glass has a 60% survival rate when dropped from a height of 80 cm in an inverted ball drop test and a peak load at failure of at least 10 kgf as determined by abraded ring-on-ring testing. Methods of achieving such stress profiles are also described.
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公开(公告)号:US10160688B2
公开(公告)日:2018-12-25
申请号:US14482250
申请日:2014-09-10
Applicant: CORNING INCORPORATED
Inventor: Jaymin Amin , Alexandre Michel Mayolet , Charles Andrew Paulson , James Joseph Price , Kevin Barry Reiman
IPC: B32B15/04 , B32B17/06 , C03C17/34 , C01B21/068 , C01B21/072 , C01B21/082 , C03C17/22 , C03C21/00 , C03C3/091 , G01N3/42 , H04M1/18
Abstract: Embodiments of a layered-substrate comprising a substrate and a layer disposed thereon, wherein the layered-substrate is able to withstand fracture when assembled with a device that is dropped from a height of at least 100 cm onto a drop surface, are disclosed. The layered-substrate may exhibit a hardness of at least about 10 GPa or at least about 20 GPa. The substrate may include an amorphous substrate or a crystalline substrate. Examples of amorphous substrates include glass, which is optionally chemically strengthened. Examples of crystalline substrates include single crystal substrates (e.g. sapphire) and glass ceramics. Articles and/or devices including such layered-substrate and methods for making such devices are also disclosed.
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公开(公告)号:US20180362399A1
公开(公告)日:2018-12-20
申请号:US15777422
申请日:2016-11-18
Applicant: CORNING INCORPORATED
Inventor: Jaymin Amin , Xiaoju Guo , Todd LeRoy Heck , Hongmei Hu , Yuhui Jin , Pascale Oram , Ljerka Ukrainczyk
CPC classification number: C03C21/002 , B01J39/02 , B01J39/14 , C03C3/097 , C03C4/18 , C03C2204/00
Abstract: Methods for regenerating poisoned salt bath comprising providing a salt bath comprising at least one of KNO3 and NaNO3, providing an ion-exchangeable substrate comprising lithium cations, contacting at least a portion of the ion-exchangeable substrate with the salt bath, whereby lithium cations in the salt bath diffuse from the ion-exchangeable substrate and are dissolved in the salt bath, and selectively precipitating dissolved lithium cations from the salt bath using phosphate salt. The methods further include preventing or reducing the formation of surface defects in the ion-exchangeable substrate by preventing or reducing the formation of crystals on the surface of the ion-exchangeable substrate upon removal from the salt bath.
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