Method for obtaining synthetic diamonds from saccharose and an equipment for carrying out said method

    公开(公告)号:US12090472B2

    公开(公告)日:2024-09-17

    申请号:US16977326

    申请日:2019-01-28

    Abstract: The invention relates to a method for obtaining synthetic diamonds from sucrose, and to a device for carrying out said method, the method comprising: introducing sucrose or a solution of water and sucrose into a hermetic capsule without air, which is surrounded by an external container that keeps the volume of the capsule constant during the entire process; increasing the pressure inside the capsule by breaking down the sucrose inside the capsule, either by increasing the temperature or by combining the sucrose with sulfuric acid, until the carbon resulting from said pressure conditions of the capsule is transformed into diamond; and controlling the pressure generated inside the capsule, using containing means that apply pressure externally around the container of the capsule. In addition, extra carbon is added, increasing the dimensions of the diamond.

    COMBINED FIELD ASSISTED SINTERING TECHNIQUES AND HTHP SINTERING TECHNIQUES FOR FORMING POLYCRYSTALLINE DIAMOND COMPACTS AND EARTH-BORING TOOLS
    77.
    发明申请
    COMBINED FIELD ASSISTED SINTERING TECHNIQUES AND HTHP SINTERING TECHNIQUES FOR FORMING POLYCRYSTALLINE DIAMOND COMPACTS AND EARTH-BORING TOOLS 审中-公开
    用于形成多晶金刚石复合材料和接地工具的组合现场辅助烧结技术和HTHP烧结技术

    公开(公告)号:US20150367310A1

    公开(公告)日:2015-12-24

    申请号:US14837747

    申请日:2015-08-27

    Abstract: Methods of forming polycrystalline diamond compacts include employing field assisted sintering techniques with high temperature and high pressure sintering techniques. For example, a particle mixture that includes diamond particles may be sintered by subjecting the particle mixture to a high temperature and high pressure sintering cycle, and pulsing direct electrical current through the particle mixture during at least a portion of the high temperature and high pressure sintering cycle. The polycrystalline diamond compacts may be used to form cutting elements for earth-boring tools. Sintering systems are configured to perform such sintering processes.

    Abstract translation: 形成多晶金刚石压块的方法包括使用具有高温和高压烧结技术的场辅助烧结技术。 例如,包括金刚石颗粒的颗粒混合物可以通过使颗粒混合物经受高温和高压烧结循环而烧结,并且在高温和高压烧结的至少一部分期间脉动直接电流通过颗粒混合物 周期。 多晶金刚石压块可用于形成用于钻孔工具的切割元件。 烧结系统被配置为执行这样的烧结过程。

    High pressure apparatus and method for nitride crystal growth
    78.
    发明授权
    High pressure apparatus and method for nitride crystal growth 有权
    用于氮化物晶体生长的高压装置和方法

    公开(公告)号:US08986447B2

    公开(公告)日:2015-03-24

    申请号:US13343563

    申请日:2012-01-04

    Inventor: Mark P. D'Evelyn

    Abstract: A high pressure apparatus and related methods for processing supercritical fluids. In a specific embodiment, the present apparatus includes a capsule, a heater, at least one ceramic ring but can be multiple rings, optionally, with one or more scribe marks and/or cracks present. In a specific embodiment, the apparatus optionally has a metal sleeve containing each ceramic ring. The apparatus also has a high-strength enclosure, end flanges with associated insulation, and a power control system. In a specific embodiment, the apparatus is capable of accessing pressures and temperatures of 0.2-2 GPa and 400-1200° C., respectively.

    Abstract translation: 一种用于加工超临界流体的高压装置及相关方法。 在具体实施例中,本装置包括胶囊,加热器,至少一个陶瓷环,但可以是多个环,任选地,存在一个或多个划痕和/或裂纹。 在具体实施例中,该装置可选地具有包含每个陶瓷环的金属套筒。 该设备还具有高强度外壳,具有相关绝缘的端部法兰和电源控制系统。 在具体实施例中,该装置能够分别访问0.2-2GPa和400-1200℃的压力和温度。

    COMPOUND HIGH PRESSURE, HIGH TEMPERATURE TOOL
    79.
    发明申请
    COMPOUND HIGH PRESSURE, HIGH TEMPERATURE TOOL 审中-公开
    复合高压,高温工具

    公开(公告)号:US20150079416A1

    公开(公告)日:2015-03-19

    申请号:US14484287

    申请日:2014-09-12

    Abstract: A tool for a high temperature, high pressure apparatus includes a working layer of a first hard metal composition of material and at least one supporting layer of a second hard metal composition of material attached to the working layer. The first hard metal composition has a mean linear intercept of less than about 0.4 μm of a binder phase. The working layer has a top and bottom surface. At least one supporting layer of a second hard metal composition of material is attached to the working layer. The at least one supporting layer includes an upper portion. An interface region is formed by the bottom surface of the working layer and the upper portion of the at least one supporting layer. The bottom surface and upper portion have a corresponding shape, wherein the bottom surface and upper portion are bonded to form the corresponding shape in the interface region.

    Abstract translation: 用于高温高压装置的工具包括第一硬质合金材料组合物的工作层和连接到工作层的材料的第二硬金属组合物的至少一个支撑层。 第一硬质合金组合物的粘结相的平均线性截距小于约0.4μm。 工作层具有顶面和底面。 至少一个第二硬质合金材料组合物的支撑层附着在工作层上。 所述至少一个支撑层包括上部。 界面区域由工作层的底表面和至少一个支撑层的上部形成。 底表面和上部具有对应的形状,其中底部表面和上部被接合以在界面区域中形成相应的形状。

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