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    FISCHER-TROPSCH CATALYST ACTIVATION
    1.
    发明申请
    FISCHER-TROPSCH CATALYST ACTIVATION 有权

    公开(公告)号：US20250059110A1

    公开(公告)日：2025-02-20

    申请号：US18722820

    申请日：2022-12-22

    Applicant: BP P.L.C. ,  Johnson Matthey Davy Technologies Limited

    Inventor： Alexander James Paterson ,  Jay Simon Clarkson ,  Andrew James Coe ,  Richard John Mercer ,  John West ,  Robert Miles Baker

    IPC: C07C1/04 ,  B01J21/06 ,  B01J23/889 ,  B01J37/18

    Abstract: The present disclosure relates generally to processes for activating Fischer-Tropsch synthesis catalysts. In particular, the application concerns a process for the activation of a Fischer-Tropsch synthesis catalyst, the process comprising: (i) contacting the catalyst with a first gaseous composition comprising at least 80% N2 at a pressure in the range of 2 barg to 20 barg at a temperature of no more than 150° C.; (ii) contacting the catalyst with a second gaseous composition comprising at least 80% H2 to form a H2/N2 gaseous composition with a H2:N2 molar ratio in the range of 0.2:1 to 2:1, resulting in a pressure in the range of 10 barg to 30 barg; (iii) increasing the temperature to a range of 220° C. to 260° C.; (iv) maintaining the catalyst at the conditions of step (iii) for a hold period in the range of 2 hr to 96 hr.

    Process for dehydrating methanol to dimethyl ether
    3.
    发明授权
    Process for dehydrating methanol to dimethyl ether 有权

    公开(公告)号：US12084410B2

    公开(公告)日：2024-09-10

    申请号：US17433135

    申请日：2019-02-22

    Applicant: BP P.L.C. ,  BP (CHINA) HOLDINGS LTD

    Inventor： Benjamin James Dennis-Smither ,  John Glenn Sunley ,  Zhiqiang Yang

    IPC: C07C41/09 ,  B01J29/06 ,  B01J29/08 ,  B01J29/18 ,  B01J29/40 ,  B01J29/70

    CPC classification number: C07C41/09 ,  B01J29/06 ,  B01J29/084 ,  B01J29/18 ,  B01J29/40 ,  B01J29/7007 ,  B01J29/7042 ,  B01J29/7046 ,  B01J2229/42

    Abstract: A process for dehydrating methanol to dimethyl ether product in the presence of a catalyst and a promoter, wherein the catalyst is at least one aluminosilicate zeolite, wherein: —the aluminosilicate zeolite is selected from: (i) a zeolite having a 2-dimensional framework structure comprising at least one channel having a 10-membered ring, and having a maximum free sphere diameter of at least 4.8 Angstroms; (ii) a zeolite having a 3-dimensional framework structure comprising at least one channel having a 10-membered ring; or (iii) a zeolite comprising at least one channel having a 12-membered ring; —the promoter is selected from one or more compounds of Formula I: (I) wherein Y is selected from a C1-C4 hydrocarbyl substituent, and wherein each of X and any or all of the Z's may independently be selected from hydrogen, halide, a substituted or unsubstituted hydrocarbyl substituent, or a compound of the formula —CHO, —CO2R, —COR, or —OR, where R is hydrogen or a substituted or unsubstituted hydrocarbyl substituent, and wherein the molar ratio of promoter to methanol is maintained at less than 1.

    Fischer-Tropsch Process, Supported Fischer-Tropsch Synthesis Catalyst and Uses Thereof
    5.
    发明申请
    Fischer-Tropsch Process, Supported Fischer-Tropsch Synthesis Catalyst and Uses Thereof 有权

    公开(公告)号：US20220186123A1

    公开(公告)日：2022-06-16

    申请号：US17554218

    申请日：2021-12-17

    Applicant: BP P.L.C.

    Inventor： Alexander James PATERSON

    IPC: C10G2/00 ,  B01J23/889 ,  B01J35/00 ,  B01J37/02

    Abstract: A process for converting a mixture of hydrogen and carbon monoxide gases to a composition comprising alcohols and liquid hydrocarbons by means of a Fischer-Tropsch synthesis reaction, said process comprising contacting a mixture of hydrogen and carbon monoxide gases, preferably in the form of synthesis gas mixture, with a supported Co—Mn Fischer-Tropsch synthesis catalyst, wherein: the support material of the supported Co—Mn Fischer-Tropsch synthesis catalyst comprises a material selected from titania, zinc oxide, zirconia, and ceria; the supported synthesis catalyst comprises at least 2.5 wt % of manganese, on an elemental basis, based on the total weight of the supported synthesis catalyst; the weight ratio of manganese to cobalt, on an elemental basis, is 0.2 or greater; the molar ratio of hydrogen to carbon monoxide is at least 1; and, the Fischer-Tropsch synthesis reaction is conducted at a pressure in the range of from 1.0 to 10.0 MPa absolute.

    PROCESS
    6.
    发明申请
    PROCESS 有权

    公开(公告)号：US20220098136A1

    公开(公告)日：2022-03-31

    申请号：US17433118

    申请日：2019-02-22

    Applicant: BP P.L.C. ,  BP (CHINA) HOLDINGS LTD

    Inventor： Benjamin James DENNIS-SMITHERS ,  John Glenn SUNLEY ,  Zhiqiang YANG

    IPC: C07C41/09 ,  B01J29/08 ,  B01J29/85 ,  B01J29/18 ,  B01J29/65 ,  B01J29/40 ,  B01J29/70

    Abstract: A process for dehydrating methanol to dimethyl ether product in the presence of a catalyst and a promoter, wherein the catalyst is at least one aluminosilicate zeolite, and the promoter is selected from one or more compounds of Formula I: (I) wherein each of X and any or all of the Y's may independently be selected from hydrogen, halide, a substituted or unsubstituted hydrocarbyl substituent, or a compound of the formula —CHO, —CO2R, —COR, or —OR, where R is hydrogen or a substituted or unsubstituted hydrocarbyl substituent, and wherein the molar ratio of promoter to methanol is maintained at less than 1.

    PROCESS
    9.
    发明申请
    PROCESS 审中-公开

    公开(公告)号：US20200262774A1

    公开(公告)日：2020-08-20

    申请号：US16645610

    申请日：2018-08-23

    Applicant: BP P.L.C. ,  BP (CHINA) HOLDINGS LTD

    Inventor： Benjamin James DENNIS-SMITHER ,  John Glenn SUNLEY ,  Zhiqiang YANG

    IPC: C07C41/09

    Abstract: A process for dehydrating methanol to dimethyl ether product in the presence of an aluminosilicate zeolite catalyst and a promoter selected from (i) aldehyde of formula R1CHO (Formula I) in which R1 is hydrogen, a C1-C11 alkyl group or a C3-C11 alkyl group in which 3 or more carbon atoms are joined to form a ring; or (ii) acetal derivative of an aldehyde of Formula I; and the molar ratio of promoter to methanol is maintained at 0.1 or less.

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