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    BORON TRIFLUORIDE-CATALYST COMPLEX AND PROCESS FOR PREPARING HIGH-REACTIVITY ISOBUTENE HOMOPOLYMERS
    4.
    发明申请
    BORON TRIFLUORIDE-CATALYST COMPLEX AND PROCESS FOR PREPARING HIGH-REACTIVITY ISOBUTENE HOMOPOLYMERS 有权
    硼三氟化物催化剂复合物和制备高反应性异丁烯共聚物的方法

    公开(公告)号：US20130217848A1

    公开(公告)日：2013-08-22

    申请号：US13768601

    申请日：2013-02-15

    Applicant: Thomas Wettling ,  Stefan Hirsch ,  Markus Brym ,  Markus Weis

    Inventor： Thomas Wettling ,  Stefan Hirsch ,  Markus Brym ,  Markus Weis

    IPC: C08F110/10

    CPC classification number: C08F110/10 ,  C08F4/14 ,  C08F2500/02

    Abstract: A catalyst complex composed of boron trifluoride and a cocatalyst mixture of 10 to 90% by weight of a monohydric primary C1- to C20-alcohol and 90 to 10% by weight of a monohydric secondary C3- to C20-alcohol, where the molar ratio of boron trifluoride to the sum of all alcohols is 2:1 to 1:10. This catalyst complex is used in the preparation of high-reactivity isobutene homopolymers having a number-average molecular weight of 300 to 50 000, using, as the feedstock, a C4 hydrocarbon mixture comprising at least 20% by weight of isobutene and a total of at least 10% by weight of other C4 olefins.

    Abstract translation: 由三氟化硼和10〜90重量％的一元一级C 1 -C 20醇和90〜10重量％的一元仲C 3〜C 20醇组成的催化剂络合物，其中摩尔比 的三氟化硼与所有醇的总和为2:1至1:10。 该催化剂络合物用于制备数均分子量为300至50 000的高反应异丁烯均聚物，其使用包含至少20重量％异丁烯的C 4烃混合物和总共为 至少10重量％的其它C4烯烃。

    PROCESS FOR PREPARING HIGHER MOLECULAR WEIGHT POLYISOBUTYLENE
    5.
    发明申请
    PROCESS FOR PREPARING HIGHER MOLECULAR WEIGHT POLYISOBUTYLENE 有权
    制备高分子量聚异丁烯的方法

    公开(公告)号：US20130217847A1

    公开(公告)日：2013-08-22

    申请号：US13765031

    申请日：2013-02-12

    Applicant: Thomas WETTLING ,  Stefan Hirsch ,  Markus Brym ,  Markus Weis

    Inventor： Thomas WETTLING ,  Stefan Hirsch ,  Markus Brym ,  Markus Weis

    IPC: C08F4/52 ,  C08F4/70

    CPC classification number: C08F4/52 ,  C08F4/70 ,  C08F110/10 ,  C08F4/14 ,  C08F2/06 ,  C08F2/38 ,  C08F2500/01 ,  C08F2500/04

    Abstract: Preparation of isobutene homopolymers having a weight-average molecular weight of 75 000 to 10 000 000 by polymerization of isobutene, by (a) performing the polymerization at −80° C. to −190° C., (b) using, as an inert solvent, optionally halogenated C1 to C5 hydrocarbons, (c) using, as a polymerization catalyst, a Lewis acid complex, (d) performing the polymerization in the presence of at least one reaction accelerator in the form of an ethylenically saturated hydrocarbon compound comprising one oxygen atom and no abstractable proton, and (e) performing the polymerization in the presence of at least one chain length regulator comprising one tertiary olefinic carbon atom.

    Abstract translation: 通过（a）在-80℃至-190℃下进行聚合，（b）使用，作为（a）），通过异丁烯的聚合制备重均分子量为75000至1000000的异丁烯均聚物 惰性溶剂，任选卤代的C1至C5烃，（c）使用路易斯酸配合物作为聚合催化剂，（d）在至少一种作为烯属饱和烃化合物形式的反应促进剂存在下进行聚合， 一个氧原子和不可抽出的质子，和（e）在至少一个包含一个三级烯烃碳原子的链长调节剂的存在下进行聚合。

    PROCESS FOR CONTINUOUSLY PREPARING POLYISOBUTYLENE
    6.
    发明申请
    PROCESS FOR CONTINUOUSLY PREPARING POLYISOBUTYLENE 审中-公开
    连续制备聚异丁烯的方法

    公开(公告)号：US20130178679A1

    公开(公告)日：2013-07-11

    申请号：US13735385

    申请日：2013-01-07

    Applicant: Thomas WETTLING ,  Stefan Hirsch ,  Markus Brym ,  Markus Weis

    Inventor： Thomas WETTLING ,  Stefan Hirsch ,  Markus Brym ,  Markus Weis

    IPC: C07C2/02

    CPC classification number: C07C2/02 ,  C08F110/10 ,  C08F4/12 ,  C08F4/14 ,  C08F2/00

    Abstract: Continuous preparation of polyisobutylene having a content of terminal double bonds of more than 50% by polymerizing isobutene in the presence of a polymerization catalyst customary therefor, by combining a technical 1-butene-, 2-butene- and isobutene-containing C4 hydrocarbon stream together with a stream of pure isobutene and feeding them into the reaction zone in such a way that the steady-state concentration of the isobutene in the combined stream at the feed point of the combined stream into the reaction zone has an average value of at least 40% by weight, and a polymerization plant therefor.

    Abstract translation: 通过在常规的聚合催化剂存在下，通过聚合异丁烯，连续制备末端双键含量大于50％的聚异丁烯，通过将工业的1-丁烯，2-丁烯和异丁烯的C4烃流合在一起 与纯异丁烯流并将其进料到反应区中，使得混合物流中的异丁烯在合并物流进入反应区的进料点的稳态浓度具有至少40的平均值 重量％，以及聚合装置。

    Boron trifluoride-catalyst complex and process for preparing high-reactivity isobutene homopolymers
    9.
    发明授权
    Boron trifluoride-catalyst complex and process for preparing high-reactivity isobutene homopolymers 有权
    三氟化硼 - 催化剂络合物和制备高反应性异丁烯均聚物的方法

    公开(公告)号：US08853336B2

    公开(公告)日：2014-10-07

    申请号：US13768601

    申请日：2013-02-15

    Applicant: Thomas Wettling ,  Stefan Hirsch ,  Markus Brym ,  Markus Weis

    Inventor： Thomas Wettling ,  Stefan Hirsch ,  Markus Brym ,  Markus Weis

    IPC: C08F4/00 ,  C08F10/00 ,  C08F110/10

    CPC classification number: C08F110/10 ,  C08F4/14 ,  C08F2500/02

    Abstract: A catalyst complex composed of boron trifluoride and a cocatalyst mixture of 10 to 90% by weight of a monohydric primary C1- to C20-alcohol and 90 to 10% by weight of a monohydric secondary C3- to C20-alcohol, where the molar ratio of boron trifluoride to the sum of all alcohols is 2:1 to 1:10. This catalyst complex is used in the preparation of high-reactivity isobutene homopolymers having a number-average molecular weight of 300 to 50 000, using, as the feedstock, a C4 hydrocarbon mixture comprising at least 20% by weight of isobutene and a total of at least 10% by weight of other C4 olefins.

    Abstract translation: 由三氟化硼和10〜90重量％的一元一级C 1 -C 20醇和90〜10重量％的一元仲C 3〜C 20醇组成的催化剂络合物，其中摩尔比 的三氟化硼与所有醇的总和为2:1至1:10。 该催化剂络合物用于制备数均分子量为300至50 000的高反应异丁烯均聚物，其使用包含至少20重量％异丁烯的C 4烃混合物和总共为 至少10重量％的其它C4烯烃。

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