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公开(公告)号:US20210060604A1
公开(公告)日:2021-03-04
申请号:US17004082
申请日:2020-08-27
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Tyler Robert Hayes , James Robert Zimmerman
IPC: B05D1/20 , C01B32/194 , C01B32/21 , C01G39/06 , C01G41/00 , C08F38/00 , C09D149/00 , B05D3/06 , B22F1/00 , B22F9/24
Abstract: The present invention generally relates to a device and a process for performing large-scale noncovalent functionalization of 2D materials, with chemical pattern elements as small as a few nanometers, using thermally controlled rotary Langmuir-Schaefer conversion. In particular, the present invention discloses a device comprising a thermally regulated disc driven by a rotor with fine speed control configured to be operable with a Langmuir trough for performing large-scale noncovalent functionalization of 2D materials, achieving ordered domain areas up to nearly 10,000 μm2, with chemical pattern elements as small as a few nanometers. A process using the device for performing large-scale noncovalent functionalization of 2D materials with chemical pattern elements as small as a few nanometers is within the scope of this disclosure. The process we demonstrate would be readily extensible to roll-to-roll processing, addressing a longstanding challenge in scaling Langmuir-Schaefer transfer for practical applications.
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公开(公告)号:US20180229265A1
公开(公告)日:2018-08-16
申请号:US15875025
申请日:2018-01-19
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Shi Wah Choong , Jae Jin Bang , Shane Russell
IPC: B05D5/04 , C09D139/00 , B05D1/18 , B05D5/06
CPC classification number: B05D5/04 , B05D1/04 , B05D1/18 , B05D1/204 , B05D5/06 , B05D5/08 , B05D7/24 , B82Y30/00 , B82Y40/00 , C03C2217/75 , C09D139/00
Abstract: This invention discloses a method for controlling nanoscopic wetting near or at a molecular scale for synthetic material applications. In particular this invention relates to a method for preparing a monolayer or thin film with a patterned nanoscopic wetting surface using a ‘sitting’ phase of polymerizable amphiphile, wherein hydrophobic alkyl chains of the amphiphile extend along the supporting surface and the amphiphile molecules align side-to-side, effectively forming a repeating cross-section of bilayer with alternating hydrophilic and hydrophobic stripes of a ˜6 nm pitch tunable based on the chain length of the amphiphile. Products prepared according to the methods disclosed herein are within the scope of this invention. In some embodiments, monolayers or thin films so prepared are transferable.
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公开(公告)号:US11508917B2
公开(公告)日:2022-11-22
申请号:US16904716
申请日:2020-06-18
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Tyler Hayes , David McMillan
Abstract: This invention generally relates to a method for preparing and transferring a monolayer or thin film. In particular this present invention is an improved version of the Langmuir-Schaefer technique for preparing and transferring a monolayer or thin film, incorporating in situ thermal control of the substrate during the transfer process.
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公开(公告)号:US20220064586A1
公开(公告)日:2022-03-03
申请号:US17466048
申请日:2021-09-03
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Tyson C. Davis , Sarah Calve , Alita Miller , Anamika Singh
Abstract: This present disclosure relates to a designed material surface mimicking properties of an extracellular matrix or matrisome, as a means for modulating cell adhesion, spreading, proliferation, differentiation, or reprogramming; and for controllable, directional cell adhesion, spreading, proliferation, differentiation, or reprogramming. In particular, this present disclosure relates to a designed material surface mimicking properties of large polysaccharides for modulating cell adhesion, proliferation, differentiation, or reprogramming of a cell, and to materials for scaffolding cell growth. Processes and composition matters are within the scope of this patent application.
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公开(公告)号:US11031268B2
公开(公告)日:2021-06-08
申请号:US16038232
申请日:2018-07-18
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Tyler Hayes , David McMillan
Abstract: This invention generally relates to a device for preparing and transferring a monolayer or thin film. In particular this present invention is a device for preparing and transferring a monolayer or thin film to a substrate using an improved version of the Langmuir-Schaefer technique, which incorporates in situ thermal control, for instance to heat the supporting substrate before and/or during the transfer process.
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公开(公告)号:US20190027697A1
公开(公告)日:2019-01-24
申请号:US16038231
申请日:2018-07-18
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Tyler Hayes , David McMillan
CPC classification number: H01L51/0075 , B05D1/204 , B05D1/208 , H01L51/0012 , H01L51/0026
Abstract: This invention generally relates to a method for preparing and transferring a monolayer or thin film. In particular this present invention is an improved version of the Langmuir-Schaefer technique for preparing and transferring a monolayer or thin film, incorporating in situ thermal control of the substrate during the transfer process.
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公开(公告)号:US20200321542A1
公开(公告)日:2020-10-08
申请号:US16904716
申请日:2020-06-18
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Tyler Hayes , David McMillan
Abstract: This invention generally relates to a method for preparing and transferring a monolayer or thin film. In particular this present invention is an improved version of the Langmuir-Schaefer technique for preparing and transferring a monolayer or thin film, incorporating in situ thermal control of the substrate during the transfer process.
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8.
公开(公告)号:US20200299542A1
公开(公告)日:2020-09-24
申请号:US16820786
申请日:2020-03-17
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Tyson Clinton Davis
IPC: C09D191/00 , B05D1/28
Abstract: The present invention generally relates to a method for creating a chemically structured surface with structural elements as small as 1 nm, on a material that does not itself display a high degree of ordering, using thin molecular layers that minimize the material added through the coating. In particular, the present invention discloses a method for assembling a chemical pattern on a surface, comprising pattern elements with scales that can be as small as 1 nm, and then transferring that pattern to another substrate, on which the pattern would not form natively. In the described method, the patterned monolayer is comprised of polymerizable amphiphiles such as diyne phospholipids or diynoic acids, which are transferred from the ordering substrate using a transferring material such as poly(dimethylsiloxane).
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公开(公告)号:US20190092885A1
公开(公告)日:2019-03-28
申请号:US16145279
申请日:2018-09-28
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Jae Jin Bang , Shane Richard Russell , Terry Angelo Villarreal
IPC: C08F138/00 , C08J5/18 , H01L51/00
Abstract: This invention generally relates to a method for modulating interfacial wettability of a noncovalent nanoscopic monolayer or thin film. Particularly, this invention relates to a method for modulating interfacial wettability of a two-dimensional (2D) material using a molecular layer prepared from a polymerizable amphiphilic monomer having a hydrophilic head and a hydrophobic tail, wherein enhanced or decreased wettability of said 2D material is achieved by proper allocating the position of polymerizable group relative to the hydrophilic head and the hydrophobic tail.
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公开(公告)号:US20190027387A1
公开(公告)日:2019-01-24
申请号:US16038232
申请日:2018-07-18
Applicant: Purdue Research Foundation
Inventor: Shelley A. Claridge , Tyler Hayes , David McMillan
IPC: H01L21/677 , H01L51/00 , B05D1/20
Abstract: This invention generally relates to a device for preparing and transferring a monolayer or thin film. In particular this present invention is a device for preparing and transferring a monolayer or thin film to a substrate using an improved version of the Langmuir-Schaefer technique, which incorporates in situ thermal control, for instance to heat the supporting substrate before and/or during the transfer process.
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