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    COMPOSITION FOR IMPROVED NICKEL-LIGAND SOLUBILITY
    42.
    发明申请
    COMPOSITION FOR IMPROVED NICKEL-LIGAND SOLUBILITY 审中-公开
    用于改善镍基配体溶解性的组合物

    公开(公告)号：WO2014089492A1

    公开(公告)日：2014-06-12

    申请号：PCT/US2013/073688

    申请日：2013-12-06

    Applicant: INVISTA NORTH AMERICA S.A.R.L.

    Inventor： VOS, Thomas E.

    IPC: B01J31/18 ,  C07C253/10 ,  C07C53/10

    CPC classification number: B01J31/185 ,  B01J37/00 ,  B01J2231/322 ,  B01J2531/847 ,  B01J2531/90 ,  C07C253/10 ,  C07C255/07 ,  C07C255/04

    Abstract: In the hydrocyanation reaction of butadiene proceeding through pentenenitriles to adiponitrile, catalysis by complexes of zerovalent nickel with bidentate phosphorus-based ligands of the NiL 2 A type wherein L 2 is a bidentate ligand and A is an unsaturated compound, can be rate-limited by the solubility of the catalytic complex. The present invention concerns solvent compositions for the nickel-ligand complex comprising mixtures of unsaturated nitriles that provide for increased metal solubility, particularly in the absence of a Lewis acid promoter, resulting in higher hydrocyanation reaction rates in an industrial-scale process for production of important nylon manufacturing intermediates. The mixed nitrile solvent compositions can include mixtures of pentenenitriles and/or methylbutenenitriles. The mixtures of mixed unsaturated nitriles can be, at least in part, from recycle streams from the hydrocyanation reaction for which the nickel-bidentate ligand complexes are used as catalysts.

    Abstract translation: 在通过戊烯腈进行己二腈的丁二烯的氢化反应中，通过与零价镍的络合物与NiL2A型的二齿磷系配体的催化作用，其中L2是二齿配体，A是不饱和化合物，可以通过溶解度 催化复合物。 本发明涉及用于镍 - 配体络合物的溶剂组合物，其包括提供金属溶解度增加的不饱和腈的混合物，特别是在不存在路易斯酸促进剂的情况下，导致在工业规模生产过程中较高的氢氰化反应速率 尼龙制造中间体。 混合的腈溶剂组合物可以包括戊烯腈和/或甲基丁烯腈的混合物。 混合的不饱和腈的混合物可以至少部分地来自使用镍二齿配位体配合物作为催化剂的氢化氰化反应的再循环流。

    AMMONIA RECOVERY WITH PURGE FOR CORROSION CONTROL
    44.
    发明申请
    AMMONIA RECOVERY WITH PURGE FOR CORROSION CONTROL 审中-公开
    奥斯陆恢复与腐蚀控制

    公开(公告)号：WO2014014620A1

    公开(公告)日：2014-01-23

    申请号：PCT/US2013/047355

    申请日：2013-06-24

    Applicant: INVISTA NORTH AMERICA S.A R.L.

    Inventor： MICKA, Thomas, A. ,  RENNER, Martin, J.

    IPC: C01C1/12 ,  C01C3/02 ,  B01D53/14 ,  B01D53/58 ,  B01D53/96 ,  C07C253/34

    CPC classification number: C01C1/02 ,  B01D53/14 ,  B01D53/1425 ,  B01D53/58 ,  B01D53/96 ,  B01D2251/61 ,  B01D2257/406 ,  C01C1/12 ,  C01C3/0212 ,  C01C3/022

    Abstract: The present invention relates to reduction of corrosion. The present invention includes a method of decreasing corrosion during ammonia extraction. The method includes performing a process to extract ammonia using ammonia extraction equipment. The ammonia extraction equipment includes an ammonia absorber, an ammonia desorber, and an aqueous solution. The aqueous solution includes an acid or an ammonium salt thereof. The method also includes purging at least part of the aqueous solution. The purged part of the aqueous solution includes at least one corrosion-promoting ion. The method also includes adding a replacement aqueous solution to the aqueous solution. The replacement aqueous solution has a reduced concentration of the at least one corrosion-promoting ion as compared to the purged part of the aqueous solution. The invention also provides a system that can perform the method.

    Abstract translation: 本发明涉及减少腐蚀。 本发明包括在氨提取期间减少腐蚀的方法。 该方法包括执行使用氨提取设备提取氨的方法。 氨提取设备包括氨吸收器，氨解吸器和水溶液。 水溶液包含酸或其铵盐。 该方法还包括清洗至少部分水溶液。 水溶液的吹扫部分包括至少一种腐蚀促进离子。 该方法还包括向水溶液中加入替代水溶液。 与水溶液的清洗部分相比，替代水溶液的至少一种腐蚀促进离子的浓度降低。 本发明还提供一种可以执行该方法的系统。

    CORROSION CONTROL IN AMMONIA EXTRACTION BY AIR SPARGING
    45.
    发明申请
    CORROSION CONTROL IN AMMONIA EXTRACTION BY AIR SPARGING 审中-公开
    通过空气分配提取氨氮的腐蚀控制

    公开(公告)号：WO2014014619A1

    公开(公告)日：2014-01-23

    申请号：PCT/US2013/047349

    申请日：2013-06-24

    Applicant: INVISTA NORTH AMERICA S.A.R.L.

    Inventor： MICKA, Thomas, A. ,  RENNER, Martin, J.

    IPC: C01C1/12 ,  C01C3/02 ,  B01D53/14 ,  B01D53/58 ,  B01D53/96

    CPC classification number: C01C1/12 ,  B01D53/14 ,  B01D53/1425 ,  B01D53/18 ,  B01D53/58 ,  B01D53/96 ,  B01D2251/60 ,  B01D2251/608 ,  B01D2251/61 ,  B01D2257/406 ,  C01C3/0212 ,  C01C3/022

    Abstract: The present invention relates to reduction of corrosion. The present invention includes a method of decreasing corrosion during ammonia extraction. The method includes performing a process to extract ammonia using ammonia extraction equipment. The ammonia extraction equipment includes an ammonia absorber, an ammonia desorber, and an aqueous solution. The aqueous solution includes an acid or an ammonium salt thereof. The method also includes sparging an oxygen-containing gas into the solution in the ammonia absorber, the ammonia desorber, or therebetween. The invention also provides a system that can perform the method.

    Abstract translation: 本发明涉及减少腐蚀。 本发明包括在氨提取期间减少腐蚀的方法。 该方法包括执行使用氨提取设备提取氨的方法。 氨提取设备包括氨吸收器，氨解吸器和水溶液。 水溶液包含酸或其铵盐。 该方法还包括将含氧气体喷射到氨吸收器，氨解吸器中或其间的溶液中。 本发明还提供一种可以执行该方法的系统。

    PROCESS FOR THE PREPARATION OF POLYAMIDES
    48.
    发明申请
    PROCESS FOR THE PREPARATION OF POLYAMIDES 审中-公开
    制备聚氨酯的方法

    公开(公告)号：WO2013085747A1

    公开(公告)日：2013-06-13

    申请号：PCT/US2012/066603

    申请日：2012-11-27

    Applicant: INVISTA NORTH AMERICA S.A. R.L.

    Inventor： KAUSHIVA, Bryan, Dinesh

    IPC: C08G69/28 ,  C08L77/06 ,  C07C231/02

    CPC classification number: C08G69/04 ,  C08G69/28 ,  C08L77/06

    Abstract: The disclosures herein relate to a process for making polyamides from stoichiometrically imbalanced mixtures. This process includes the production and subsequent use of solidified stoichiometrically imbalanced components comprising mixtures of diacids and diamines. This stoichiometric imbalance is defined by a component molar ratio equal to moles of dicarboxylic acid units divided by moles of diamine units; and wherein this molar ratio is different from unity. This process com¬ prises steps of: a) forming an acid-rich solidified first component in a dry or moisture containing state by; b) contacting at least a dicar¬ boxylic acid with at least a diamine in a molar ratio of greater than 1:1; c) forming an amine-rich solidified second component in a dry or moisture containing state by; d) contacting at least a dicarboxylic acid with at least a diamine in a molar ratio of less than 1:1; e) contacting the acid-rich first component with the amine-rich second component in a molten state or a solution state and f) forming a first composition having a composition molar ratio g) such that a total dicarboxylic acid content and a total diamine content, supplied by said first and second components, is from about 0.95 to about 1.05; h) heating the first composition with agitation in the molten state and under pressure to a sufficiently high temperature for a polyamidation reaction to and subsequently, i) forming a second composition comprising a polyamide.

    Abstract translation: 本文的公开内容涉及由化学计量不平衡混合物制备聚酰胺的方法。 该方法包括生产和随后使用包含二酸和二胺的混合物的固化化学计量不平衡组分。 该化学计量不平衡由等于二羧酸单元摩尔数除以二胺单元摩尔数的组分摩尔比定义; 并且其中该摩尔比不同于1。 该方法包括以下步骤：a）通过以下方式形成富含干燥或含水的状态的富酸固化的第一组分： b）使至少二羧酸与摩尔比大于1:1的至少二胺接触; c）通过以下方式形成干燥或含水状态的富含胺的固化的第二组分; d）使至少二羧酸与摩尔比小于1:1的二胺接触; e）使富酸的第一组分与富含胺的第二组分以熔融状态或溶液状态接触，以及f）形成具有组成摩尔比g）的第一组合物，使得总二羧酸含量和总二胺含量 由所述第一和第二组分提供的是约0.95至约1.05; h）在熔融状态和压力下搅拌加热第一组合物至足够高的温度进行聚酰胺化反应，随后，i）形成包含聚酰胺的第二组合物。

    MOLDABLE COMPOSITE ARTICLE
    50.
    发明申请
    MOLDABLE COMPOSITE ARTICLE 审中-公开
    可模压复合材料制品

    公开(公告)号：WO2005104812A3

    公开(公告)日：2005-12-15

    申请号：PCT/US2005003683

    申请日：2005-02-04

    Applicant: INVISTA NORTH AMERICA SARL ,  NGUYEN HUNG MANH

    Inventor： NGUYEN HUNG MANH

    IPC: C08G63/91 ,  C08K5/00 ,  C08K5/15 ,  C08L37/00 ,  C08L51/06 ,  C08L73/02

    CPC classification number: C08G63/916 ,  C08G69/48 ,  C08J5/047 ,  C08K5/0008 ,  C08K5/15 ,  C08L67/00 ,  C08L67/02 ,  D04H1/425 ,  D04H1/4291 ,  D04H1/4334 ,  D04H1/435 ,  D04H1/4382 ,  Y10T428/237 ,  C08L77/00 ,  C08L2666/24

    Abstract: The present invention relates to moldable composite articles, and particularly to a molded nonwoven fibrous article, and specifically to an automobile headliner that has improved physical properties at low weight. There is a need to minimize the weight of the headliner and the critical parameter is minimum sag. For a molded non-needlepunched batt in the weight range of 1000 to 1200 grams per square meter (gsm), the sag at 91°C must be less than 10 mm, when cantilevering a distance of 28cm. The stiffness, strength and toughness of the batt should be greater than 2 N/mm, 17N and 70% respectively. In the first embodiment, the thermoplastic binder is a bicomponent fiber with an adhesion promoted polyolefin sheath and a polyester core. In the second embodiment, the matrix fiber is a synthetic fiber with a modulus greater than 10 cN/tex. In the third embodiment the matrix fiber is a natural fiber. In the fourth embodiment the bicomponent fiber contains a filler such as carbon black or titanium dioxide.

    Abstract translation: 本发明涉及可模制复合制品，特别涉及模制非织造纤维制品，并且具体涉及在重量轻的情况下具有改善的物理性能的汽车顶蓬。 有必要尽量减少顶篷的重量，关键参数是最小下垂。 对于重量范围为1000至1200克/平方米（gsm）的模制非针刺棉胎，当悬臂距离为28厘米时，91°C下垂度必须小于10毫米。 棉胎的刚度，强度和韧性应分别大于2N / mm，17N和70％。 在第一实施例中，热塑性粘合剂是具有粘合促进的聚烯烃护套和聚酯芯的双组分纤维。 在第二实施例中，基质纤维是模量大于10cN / tex的合成纤维。 在第三实施例中，基质纤维是天然纤维。 在第四实施方案中，双组分纤维含有填料如炭黑或二氧化钛。

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