• Patent Title: Method for obtaining raw-1,3-butadiene
  • Application No.: AU2005210003
    Application Date: 2005-02-04
  • Publication No.: AU2005210003A1
    Publication Date: 2005-08-18
  • Inventor: HEIDA BERND
  • Applicant: BASF AG
  • Assignee: BASF AG
  • Current Assignee: BASF AG
  • Priority: DE102004005930 2004-02-06
  • Main IPC: C07C7/08
  • IPC: C07C7/08
Method for obtaining raw-1,3-butadiene
Abstract:
1,3-butadiene is obtained by extractive distillation with a selective solvent from a C4 cut comprising C4 acetylenes as secondary components in a dividing wall column having a bottom evaporator, in which a dividing wall is disposed in the longitudinal direction of the column to form a first subregion, a second subregion and a lower combined column region. The column is disposed upstream of an extractive wash column. The energy input into the dividing wall column via the bottom evaporator is controlled in such a way that a bottom stream containing solvent, C4 acetylenes and 1,3-butadiene restricted such that the loss of 1,3-butadiene is economically acceptable, is drawn off and fed to an acetylenes outgasser where the C4 acetylenes are stripped out overhead and purified solvent is obtained as the bottom stream.
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