Invention Grant
- Patent Title: Method for preparing high-melting-point metal powder through multi-stage deep reduction
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Application No.: US16498151Application Date: 2018-05-21
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Publication No.: US11241740B2Publication Date: 2022-02-08
- Inventor: Ting An Zhang , Zhihe Dou , Yan Liu , Zimu Zhang , Guozhi Lv , Qiuyue Zhao , Liping Niu , Daxue Fu , Weiguang Zhang
- Applicant: NORTHEASTERN UNIVERSITY
- Applicant Address: CN Shenyang
- Assignee: NORTHEASTERN UNIVERSITY
- Current Assignee: NORTHEASTERN UNIVERSITY
- Current Assignee Address: CN Shenyang
- Agency: Muncy, Geissler, Olds & Lowe, P.C.
- Priority: CN201710365992.1 20170523
- International Application: PCT/CN2018/087587 WO 20180521
- International Announcement: WO2018/214830 WO 20181129
- Main IPC: B22F9/24
- IPC: B22F9/24 ; C22B34/00

Abstract:
The invention relates to a method for preparing high-melting-point metal powder through multi-stage deep reduction, and belongs to the technical field of preparation of powder. The method includes the following steps of mixing dried high-melting-point metal oxide powder with magnesium powder and performing a self-propagating reaction, placing an intermediate product into a closed reaction kettle, leaching the intermediate product with hydrochloric acid as a leaching solution so as to obtain a low-valence oxide MexO precursor of the low-valence high-melting-point metal; uniformly mixing the precursor with calcium powder, pressing the mixture, placing the pressed mixture into a vacuum reduction furnace, heating the vacuum reduction furnace to 700-1200° C., performing deep reduction for 1-6 h, leaching a deep reduction product with hydrochloric acid as a leaching solution and performing treatment, so as to obtain the high-melting-point metal powder.
Public/Granted literature
- US20200276648A1 METHOD FOR PREPARING HIGH-MELTING-POINT METAL POWDER THROUGH MULTI-STAGE DEEP REDUCTION Public/Granted day:2020-09-03
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