Invention Grant
- Patent Title: Method for producing composite lithium iron phosphate material and composite lithium iron phosphate material produced by same
- Patent Title (中): 复合磷酸铁锂材料及复合磷酸铁锂材料的制造方法
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Application No.: US13120655Application Date: 2010-06-21
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Publication No.: US08815338B2Publication Date: 2014-08-26
- Inventor: Liguang Ye
- Applicant: Liguang Ye
- Applicant Address: CN Zaozhuang, Shandong
- Assignee: Haite Electronic Group Co., Ltd.
- Current Assignee: Haite Electronic Group Co., Ltd.
- Current Assignee Address: CN Zaozhuang, Shandong
- Agency: Global IP Services
- Agent Tianhua Gu
- Priority: CN200910016269 20090621
- International Application: PCT/CN2010/000906 WO 20100621
- International Announcement: WO2010/148638 WO 20101229
- Main IPC: B05D7/00
- IPC: B05D7/00 ; H01M4/00 ; C01B25/45 ; H01M4/58 ; H01M10/052

Abstract:
A method for producing a composite lithium iron phosphate material, which comprises formulating lithium iron phosphate material and purified water at a weight ratio of 1:5-15 into a suspension solution, slowly adjusting the pH value of the suspension solution to 1-3 with phosphoric acid at a concentration of 5-30% in weight, adding an analytically pure soluble chloride in an amount of 0.05-2% based on the molar amount of the lithium iron phosphate material; then adding ammonia water into the solution to adjust the pH value of the solution to 5-6 to obtain hydroxide colloid; drying liquid through spraying to prepare powder, and calcining at 300-450° C. for 3-6 hours under an inert atmosphere; coating the oxide with high conductivity obtained by thermally decomposing the hydroxide colloid on the surface of the lithium iron phosphate material grains; ball milling and sieving the calcined material into a finished product. Also disclosed is the composite lithium iron phosphate material produced by such a method.
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