Invention Grant
- Patent Title: Method for preparing sponge titanium from sodium fluotitanate by aluminothermic reduction
- Patent Title (中): 通过铝热还原从氟酸钠制备海绵钛的方法
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Application No.: US13585786Application Date: 2012-08-14
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Publication No.: US08864874B2Publication Date: 2014-10-21
- Inventor: Xuemin Chen , Jun Yang , Zhi Zhou
- Applicant: Xuemin Chen , Jun Yang , Zhi Zhou
- Applicant Address: CN Shenzhen, Guangdong
- Assignee: Shenzhen Sunxing Light Alloys Materials Co., Ltd.
- Current Assignee: Shenzhen Sunxing Light Alloys Materials Co., Ltd.
- Current Assignee Address: CN Shenzhen, Guangdong
- Agency: Jackson IPG PLLC
- Priority: CN201210014937 20120118
- Main IPC: C22B34/00
- IPC: C22B34/00 ; C22B34/12

Abstract:
The invention provides a method for preparing sponge titanium from sodium fluotitanate by aluminothermic reduction, comprising the following steps: a reaction step: aluminum and zinc are mixed under a vacuum state, and sodium fluotitanate is then added into the mixture for reaction; a separation step: the product resulting from the complete reaction stands still and is then introduced with inert gas, and NaF and AlF3 in upper-layer liquid phase are extracted; and a distillation step: Zn in the remaining product Zn—Ti is distilled out under a vacuum state, wherein the mass ratio of the aluminum to the zinc is 1:2 to 1:10.
Public/Granted literature
- US20120304826A1 METHOD FOR PREPARING SPONGE TITANIUM FROM SODIUM FLUOTITANATE BY ALUMINOTHERMIC REDUCTION Public/Granted day:2012-12-06
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