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    MULTI-TUBE FIXED-BED REACTOR, ESPECIALLY FOR CATALYTIC GAS PHASE REACTIONS
    1.
    发明申请
    MULTI-TUBE FIXED-BED REACTOR, ESPECIALLY FOR CATALYTIC GAS PHASE REACTIONS 审中-公开
    管式反应器，尤其气相催化反应的

    公开(公告)号：WO0054877A3

    公开(公告)日：2001-04-05

    申请号：PCT/EP0002304

    申请日：2000-03-15

    Applicant: BASF AG ,  OLBERT GERHARD ,  CORR FRANZ ,  REUTER PETER ,  WAMBACH LUDWIG ,  HAMMON ULRICH

    Inventor： OLBERT GERHARD ,  CORR FRANZ ,  REUTER PETER ,  WAMBACH LUDWIG ,  HAMMON ULRICH

    IPC: B01J8/06 ,  B01J19/00 ,  B01J19/24 ,  C07C45/35 ,  C07C45/38

    CPC classification number: C07C45/35 ,  B01J8/067 ,  B01J19/0013 ,  B01J19/2425 ,  B01J2208/00212 ,  B01J2208/00221 ,  B01J2208/00256 ,  B01J2219/00094 ,  B01J2219/00103 ,  C07C45/38 ,  C07C47/22 ,  C07C47/127

    Abstract: The invention relates to a multi-tube fixed-bed reactor and to the use of a reactor of this type for carrying out catalytic gas phase reactions, especially for carrying out exothermic or endothermic catalytic gas phase reactions such as producing phthalic anhydride (PSA), acrylic acid (AA), methacrylic acid (MAA), acrolein, maleic anhydride (MSA), glyoxal, phosgene, hydrogen cyanide or vinyl formamide (VFA). According to the invention, in the case of larger reactors where a considerable reaction heat is produced or required and must be dissipated as a result of the numerous reaction tubes (17), the ratio of tube distribution t to tube outer diameter d?a? is made dependant on the reactor diameter or the tube bundle diameter d?RBa?. If the outer diameter of the reaction tube bundle (18) is more than 4 metres, a ratio of tube distribution t to tube outer diameter d?a? of at least 1.3 is preferred.

    Abstract translation: 本发明涉及一种管束反应器和用于进行气相催化反应，特别是用于进行放热或吸热催化气相反应如生产Phthalsälureanhydrid（PSA），丙烯酸（AA），甲基丙烯酸（MAA），丙烯醛，马来酸酐的使用这样的反应器中的（ MSA），乙二醛，光气，氢氰酸或乙烯基甲酰胺（VFA）。 根据本发明，在较大的反应器，其中，这是因为许多反应管（17）的已被获得的反应的高的热或需要，管间距的比率管外径d·A· 在反应器直径或管束外径d？RBA？ 让他们依赖。 具有大于4米反应管束（18）的外直径，管间距吨到管外径d的比·A· 优选为至少1.3。

    3.
    发明专利
    未知

    公开(公告)号：BR0009000A

    公开(公告)日：2002-01-02

    申请号：BR0009000

    申请日：2000-03-15

    Applicant: BASF AG

    Inventor： OLBERT GERHARD ,  CORR FRANZ ,  REUTER PETER ,  WAMBACH LUDWIG ,  HAMMON ULRICH

    IPC: B01J8/06 ,  B01J19/00 ,  B01J19/24 ,  C07C45/35 ,  C07C45/38 ,  H01Q21/08 ,  B01J8/00

    Abstract: A multitube fixed bed reactor and the use of such a reactor for carrying out catalytic gas-phase reactions, in particular for carrying out exothermic and endothermic catalytic gas-phase reactions such as the preparation of phthalic anhydride (PA), acrylic acid, methacrylic acid (MAA), acrolein, maleic anhydride (MA), glyoxal, phosgene, hydrocyanic acid or vinyl formamide (VFA). In a relatively large multitube reactor in which a large amount of heat of reaction is generated owing to the numerous catalyst tubes ( 17 ) and has to be removed, it is proposed that the ratio of tube spacing t to external tube diameter d a be made dependent on the reactor diameter or on the external tube bundle diameter d RBa . At an external diameter of the catalyst tube bundle ( 18 ) of more than 4 meters, a ratio of tube spacing d to external tube diameter d a of at least 1.3 is preferred.

    Multi-tube fixed-bed reactor, especially for catalytic gas phase reactions
    4.
    发明专利
    Multi-tube fixed-bed reactor, especially for catalytic gas phase reactions 未知

    公开(公告)号：AU4538700A

    公开(公告)日：2000-10-04

    申请号：AU4538700

    申请日：2000-03-15

    Applicant: BASF AG

    Inventor： OLBERT GERHARD ,  CORR FRANZ ,  REUTER PETER ,  WAMBACH LUDWIG ,  HAMMON ULRICH

    IPC: B01J8/06 ,  B01J19/00 ,  B01J19/24 ,  C07C45/35 ,  C07C45/38 ,  H01Q21/08 ,  B01J8/00

    Abstract: A multitube fixed bed reactor and the use of such a reactor for carrying out catalytic gas-phase reactions, in particular for carrying out exothermic and endothermic catalytic gas-phase reactions such as the preparation of phthalic anhydride (PA), acrylic acid, methacrylic acid (MAA), acrolein, maleic anhydride (MA), glyoxal, phosgene, hydrocyanic acid or vinyl formamide (VFA). In a relatively large multitube reactor in which a large amount of heat of reaction is generated owing to the numerous catalyst tubes ( 17 ) and has to be removed, it is proposed that the ratio of tube spacing t to external tube diameter d a be made dependent on the reactor diameter or on the external tube bundle diameter d RBa . At an external diameter of the catalyst tube bundle ( 18 ) of more than 4 meters, a ratio of tube spacing d to external tube diameter d a of at least 1.3 is preferred.

    6.
    发明专利
    未知

    公开(公告)号：DE3774378D1

    公开(公告)日：1991-12-12

    申请号：DE3774378

    申请日：1987-09-15

    Applicant: BASF AG

    Inventor： WAMBACH LUDWIG

    IPC: B01D53/14 ,  C07D207/22 ,  C07D207/26 ,  C07D207/267 ,  C07D209/54

    Abstract: 2-Pyrrolidone derivs. of formula (Ia) are new, where R'1 and R'2 = 1-4C alkyl, or CR'1R'2 is a ring, esp. with 4-7 ring C atoms; R''3 = Me ot t-Bu. Prodn. of 2-pyrrolidone derivs. of formula (I) is effected by reacting an amine of formula (II) with an alpha,beta-unsatd. carboxylic acid or nitrile deriv. of formula (III) in the presence of a radical initiator, and opt. alkylating the prod. when R'3 = H. R1 and R2 = 1-8C alkyl, 1-8C alkoxy, 3-10C cycloalkyl or 3-10C cycloalkoxy, or CR1R2 is a ring, esp. with 4-7 ring C atoms; R3 = H, 1-6C alkyl, phenyl or naphthyl; R4 and R5 = H or 1-4C alkyl; R'3 = H, t-Bu, phenyl or napthyl; Q = COX or CN; X = OR', NR'R'', NHR' or NH2; R'= 1-8C alkyl, 3-8C cycloalkyl or phenyl; Z = O or NH. Use of cpds. (I; Z = O) as basic absorbents for scrubbing gas mixts. to remove acid gases is also new. The reaction is effected at 50-200 deg.C and 1-200 bar in the presence of an alkyl perester, dialkyl peroxide, diaryl peroxide or azo cpd. Excess (II) is used as solvent.

    Multi-tube fixed-bed reactor, especially for catalytic gas phase reactions
    7.
    发明专利
    Multi-tube fixed-bed reactor, especially for catalytic gas phase reactions 未知

    公开(公告)号：MX220474B

    公开(公告)日：2004-05-20

    申请号：MXPA01009012

    申请日：2001-09-06

    Applicant: BASF AG

    Inventor： OLBERT GERHARD ,  CORR FRANZ ,  REUTER PETER ,  WAMBACH LUDWIG ,  HAMMON ULRICH

    IPC: B01J8/06 ,  B01J19/00 ,  B01J19/24 ,  C07C45/35 ,  C07C45/38 ,  H01Q21/08

    Abstract: A multitube fixed bed reactor and the use of such a reactor for carrying out catalytic gas-phase reactions, in particular for carrying out exothermic and endothermic catalytic gas-phase reactions such as the preparation of phthalic anhydride (PA), acrylic acid, methacrylic acid (MAA), acrolein, maleic anhydride (MA), glyoxal, phosgene, hydrocyanic acid or vinyl formamide (VFA). In a relatively large multitube reactor in which a large amount of heat of reaction is generated owing to the numerous catalyst tubes ( 17 ) and has to be removed, it is proposed that the ratio of tube spacing t to external tube diameter d a be made dependent on the reactor diameter or on the external tube bundle diameter d RBa . At an external diameter of the catalyst tube bundle ( 18 ) of more than 4 meters, a ratio of tube spacing d to external tube diameter d a of at least 1.3 is preferred.

    8.
    发明专利
    未知

    公开(公告)号：AT251944T

    公开(公告)日：2003-11-15

    申请号：AT00926738

    申请日：2000-03-15

    Applicant: BASF AG

    Inventor： OLBERT GERHARD ,  CORR FRANZ ,  REUTER PETER ,  WAMBACH LUDWIG ,  HAMMON ULRICH

    IPC: B01J8/06 ,  B01J19/00 ,  B01J19/24 ,  C07C45/35 ,  C07C45/38 ,  H01Q21/08

    Abstract: A multitube fixed bed reactor and the use of such a reactor for carrying out catalytic gas-phase reactions, in particular for carrying out exothermic and endothermic catalytic gas-phase reactions such as the preparation of phthalic anhydride (PA), acrylic acid, methacrylic acid (MAA), acrolein, maleic anhydride (MA), glyoxal, phosgene, hydrocyanic acid or vinyl formamide (VFA). In a relatively large multitube reactor in which a large amount of heat of reaction is generated owing to the numerous catalyst tubes ( 17 ) and has to be removed, it is proposed that the ratio of tube spacing t to external tube diameter d a be made dependent on the reactor diameter or on the external tube bundle diameter d RBa . At an external diameter of the catalyst tube bundle ( 18 ) of more than 4 meters, a ratio of tube spacing d to external tube diameter d a of at least 1.3 is preferred.

    10.
    发明专利
    未知

    公开(公告)号：DE59909810D1

    公开(公告)日：2004-07-29

    申请号：DE59909810

    申请日：1999-02-25

    Applicant: BASF AG

    Inventor： DEMUTH DIRK ,  FETZER THOMAS ,  PRATSCH VOLKER ,  WENDRICH THOMAS ,  MENIG HELMUTH ,  WAMBACH LUDWIG ,  HARTH KLAUS

    IPC: C07B61/00 ,  C07C45/38 ,  C07C45/39 ,  C07C47/04 ,  C07C47/127 ,  C07C47/19

    Abstract: Carbonyl compounds of the formulawhere R1 is a hydrogen atom or an alkyl radical having from 1 to 3 carbon atoms, R2 is a hydrogen atom, an unsubstituted or C1-C3-alkyl-monosubstituted to -trisubstituted C2-C4-alkenyl radical or a radical of the formulawhere R3 is a hydrogen atom or together with R4 is an oxygen atom, R4 is the radical OR6 or together with R3 is an oxygen atom, R5 is a hydrogen atom, an alkyl radical having from 1 to 8 carbon atoms, an unsubstituted or C1-C3-alkyl-monosubstituted to -trisubstituted C2-C4-alkenyl radical or a cyclohexyl or cyclopentyl radical and R6 is an alkyl radical having from 1 to 4 carbon atoms, a cyclohexyl or cyclopentyl radical or a radical of the formula -CH2-CHO or -CH2-CH2-O-CH2-CHO, are prepared by gas-phase oxidation of methanol or alcohols of the formulawhere R1 and R5 are as defined above, by means of an oxygen-containing gas in the presence of copper- and/or silver-containing catalysts, the catalyst system used comprising at least one phosphorus-containing copper- and/or silver-containing catalyst.

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