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    METHOD FOR PRODUCING OXO-VINYL-IONOL AND O-PROTECTED DERIVATIVES THEREOF
    1.
    发明申请
    METHOD FOR PRODUCING OXO-VINYL-IONOL AND O-PROTECTED DERIVATIVES THEREOF 审中-公开
    用于生产OXOVINYLJONOL及其O型保护的衍生物

    公开(公告)号：WO2013068465A3

    公开(公告)日：2013-07-18

    申请号：PCT/EP2012072144

    申请日：2012-11-08

    Applicant: BASF SE

    Inventor： ERNST HANSGEORG ,  PUHL MICHAEL ,  BENSON STEFAN ,  SIEGEL WOLFGANG

    IPC: C07F9/54 ,  C07C403/06 ,  C07C403/08

    CPC classification number: C07C403/06 ,  C07C403/08 ,  C07F7/1856 ,  C07F9/5442 ,  Y02P20/55

    Abstract: The invention relates to the production of oxo-vinyl-ionol and O-protected derivatives thereof of formula (I), wherein R stands for hydrogen or an OH protecting group, for example a group Si(Ra)3, by reacting a compound of general formula (II), wherein R has the meanings previously specified for formula (I), i.e. beta-vinyl-ionol (formula (II), R = hydrogen) or an O-protected derivative thereof (formula (II), R = OH protecting group), with an oxidant in the presence of at least one transition metal, wherein the oxidant comprises at least one compound containing oxygen, which compound is selected from among hydrogen peroxide and organic hydroperoxides.

    Abstract translation: 本发明涉及Oxovinyljonol和式及其O-保护的衍生物（I）其中R是氢或OH-保护基团，例如基团的Si（Ra）为3，的制备由通式的化合物反应（II），其中 R具有式I，即上面给出的含义 SS-Vinyljonol（式（II）中，R =氢）或O-保护的衍生物（式（II），R = OH保护基团）与至少一种过渡金属，其中所述氧化剂包括至少一种含氧化合物的存在下的氧化剂， 从过氧化氢和有机氢过氧化物选择。

    METHOD FOR PRODUCING OXO-VINYL-IONOL AND O-PROTECTED DERIVATIVES THEREOF
    6.
    发明专利
    METHOD FOR PRODUCING OXO-VINYL-IONOL AND O-PROTECTED DERIVATIVES THEREOF 未知

    公开(公告)号：MY168427A

    公开(公告)日：2018-11-09

    申请号：MYPI2014001356

    申请日：2012-11-08

    Applicant: BASF SE

    Inventor： SIEGEL WOLFGANG ,  ERNST HANSGEORG ,  PUHL MICHAEL ,  BENSON STEFAN

    Abstract: The present invention relates to the preparation of oxovinylionol and its O-protected derivatives of the formula I (I) in which R is hydrogen or an OH protecting group, for example a group Si(Ra)3 by reacting a compound of the formula II (II) in which R have the meanings given above for formula I, i.e. ?-vinyl ionol (formula II, R = hydrogen) or an O-protected derivative thereof (formula II, R = OH protecting group) with an oxidant in the presence of at least one transition metal, where the oxidant comprises at least one oxygen-containing compound which is selected from among hydrogen peroxide and organic hydroperoxides. (No suitable figure)

    Method for producing astaxanthin esters
    7.
    发明专利
    Method for producing astaxanthin esters 未知

    公开(公告)号：AU2015314580A1

    公开(公告)日：2017-04-06

    申请号：AU2015314580

    申请日：2015-08-11

    Applicant: BASF SE

    Inventor： SCHAFER BERND ,  BENSON STEFAN ,  SIEGEL WOLFGANG

    IPC: C07C403/24 ,  A23L5/40 ,  A23L33/10 ,  A61K31/23

    Abstract: The invention relates to an environmentally friendly, resource-conserving, and economical method for producing astaxanthin esters of formula 1, wherein astaxanthin of formula 2 is doubly esterified with fatty acid chlorides of general formula 3. For this purpose, compounds 2 and 3 are reacted in an organic solvent in the presence of a nitrogen-containing base of general formula 4. The invention further relates to the non-therapeutic use of diester 1, wherein R stands for a residue that is selected from the group consisting of C13-C19 alkyl, C13-C19 alkenyl, C13-C19 alkdienyl, and C13-C19 alktrienyl, in the nourishment of humans or animals, and to diester 1 produced according to the method, for therapeutic use as a medication and as an ingredient for a medical preparation.

    Procedimiento para la preparación de oxo-vinil-ionol y sus derivados O-protegidos
    8.
    发明专利
    Procedimiento para la preparación de oxo-vinil-ionol y sus derivados O-protegidos 未知

    公开(公告)号：ES2681706T3

    公开(公告)日：2018-09-14

    申请号：ES12781343

    申请日：2012-11-08

    Applicant: BASF SE

    Inventor： ERNST HANSGEORG ,  PUHL MICHAEL ,  BENSON STEFAN ,  SIEGEL WOLFGANG

    IPC: C07C403/08 ,  C07C403/06 ,  C07F7/18 ,  C07F9/54

    Abstract: Procedimiento para la preparación de oxo-vinil-ionol y sus derivados O-protegidos de la fórmula I **(Ver fórmula)** en la cual R representa hidrógeno o un grupo protector de OH, caracterizado porque se hace reaccionar β-vinilionol o un derivado O-protegido del mismo de la fórmula II, en la cual R tiene los significados antes mencionados, con un agente de oxidación en presencia de al menos un metal de transición, el cual se selecciona entre Cu, Co, Fe y Mn y sus mezclas y comprendiendo el agente de oxidación al menos un compuesto que contiene oxígeno, el cual se selecciona entre peróxido de hidrógeno e hidroperóxidos orgánicos.

    METHOD FOR PREPARING ASTAXANTHIN ESTERS
    9.
    发明专利
    METHOD FOR PREPARING ASTAXANTHIN ESTERS 未知

    公开(公告)号：CA2958386A1

    公开(公告)日：2016-03-17

    申请号：CA2958386

    申请日：2015-08-11

    Applicant: BASF SE

    Inventor： SCHAFER BERND ,  BENSON STEFAN ,  SIEGEL WOLFGANG

    IPC: C07C403/24 ,  A61K31/23

    Abstract: The invention relates to an environmentally friendly, resource-conserving, and economical method for producing astaxanthin esters of formula 1, wherein astaxanthin of formula 2 is doubly esterified with fatty acid chlorides of general formula 3. For this purpose, compounds 2 and 3 are reacted in an organic solvent in the presence of a nitrogen-containing base of general formula 4. The invention further relates to the non-therapeutic use of diester 1, wherein R stands for a residue that is selected from the group consisting of C13-C19 alkyl, C13-C19 alkenyl, C13-C19 alkdienyl, and C13-C19 alktrienyl, in the nourishment of humans or animals, and to diester 1 produced according to the method, for therapeutic use as a medication and as an ingredient for a medical preparation.

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