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    Fipronyl crystalline transformation
    1.
    发明专利
    Fipronyl crystalline transformation 审中-公开
    FIPRONYL晶体转化

    公开(公告)号：JP2014139190A

    公开(公告)日：2014-07-31

    申请号：JP2014031226

    申请日：2014-02-21

    Applicant: Basf Se ,  ビーエーエスエフ ソシエタス・ヨーロピアBasf Se

    Inventor： HEIDI EMILIA SAXELL ,  ERK PETER ,  CLAUDE TARANTA ,  KROEHL THOMAS ,  COX GERHARD ,  DESIRAJU GAUTAM R ,  RAHUL BANERJEE ,  BHATT PRASHANT M

    IPC: C07D231/44 ,  A01N25/00 ,  A01N25/04 ,  A01N25/14 ,  A01N47/02 ,  A01P5/00 ,  A01P7/00 ,  A01P7/04 ,  A61K31/415 ,  A61P33/10 ,  A61P33/14

    CPC classification number: A01N47/02 ,  A01N2300/00

    Abstract: PROBLEM TO BE SOLVED: To provide a novel crystalline transformation of fipronyl, and a method for producing said crystalline transformation, and also a composition for combating pests and parasites.SOLUTION: Use of a novel crystalline transformation IV of fipronyl of formula I below that exists in a triclinic crystalline system having center symmetric space group P-1. Said fipronyl is dissolved into acetone and crystallized to obtain crystalline transformation IV, and which is used, as it is (crystalline transformation IV), as a composition for controlling pests. High purity fipronyl of said crystalline transformation IV is a raw material for converting to crystalline transformation IV by further tempering the crystalline transformation IV at 90 to 100°C, or to crystalline transformation V by tempering at 100 to 130°C.

    Abstract translation: 要解决的问题：提供呋喃尼基的新型结晶转化及其生产所述结晶转化的方法，以及用于防治害虫和寄生虫的组合物。解决方案：使用存在下述式I的呋喃基的新结晶转化IV 具有中心对称空间群P-1的三斜晶系​​。 将所述氟虫酰基溶于丙酮中并结晶，得到结晶转化IV，并将其作为（结晶转化IV）用作防治害虫的组合物。 所述结晶转变IV的高纯度fipronyl是通过在90至100℃进一步回火结晶转变IV或通过在100至130℃回火的结晶转变V而转化为结晶转变IV的原料。

    Fipronyl crystalline transformation
    2.
    发明专利
    Fipronyl crystalline transformation 审中-公开
    FIPRONYL晶体转化

    公开(公告)号：JP2014139188A

    公开(公告)日：2014-07-31

    申请号：JP2014031221

    申请日：2014-02-21

    Applicant: Basf Se ,  ビーエーエスエフ ソシエタス・ヨーロピアBasf Se

    Inventor： HEIDI EMILIA SAXELL ,  ERK PETER ,  CLAUDE TARANTA ,  KROEHL THOMAS ,  COX GERHARD ,  GAUTAM R DESIRAJU ,  RAHUL BANERJEE ,  PRASHANT M BHATT

    IPC: C07D231/44 ,  A01G13/00 ,  A01M1/20 ,  A01N25/04 ,  A01N25/12 ,  A01N47/02 ,  A01P7/04 ,  A23K1/16

    CPC classification number: A01N47/02 ,  A01N2300/00

    Abstract: PROBLEM TO BE SOLVED: To provide a novel crystalline transformation of fipronyl of the formula below that was found and of which characteristics were determined, and a novel method for producing said crystalline transformation with high yield while excluding the production of other crystalline transformed forms, also a mixture and composition for killing insects and parasites comprising said crystalline transformation, and a method of their use for combating pests and parasites.SOLUTION: A crystalline transformation of fipronyl that has a particular X-ray powder diffraction chart, and undergoes, at 105°C to 145°C, phase transformation to two other crystalline transformations respectively having melting points of 196 to 197°C and 202 to 203°C.

    Abstract translation: 要解决的问题：为了提供下面所公开的下列式子基的新型结晶转变，其特征是确定的，以及一种新的制备高产率的结晶转化同时排除其它结晶转化形式的生产的新方法 用于杀死昆虫和包含所述结晶转化的寄生虫的混合物和组合物及其用于防治害虫和寄生虫的方法。解决方案：具有特定X射线粉末衍射图的fipronyl的结晶转化并在105° C至145℃，相转变为分别具有196至197℃和202至203℃的熔点的两个其它结晶转化。

    Crystal transformation of fipronyl
    3.
    发明专利
    Crystal transformation of fipronyl 审中-公开
    FIPRONYL的晶体转化

    公开(公告)号：JP2014141494A

    公开(公告)日：2014-08-07

    申请号：JP2014031217

    申请日：2014-02-21

    Applicant: Basf Se ,  ビーエーエスエフ ソシエタス・ヨーロピアBasf Se

    Inventor： HEIDI EMILIA SAXELL ,  ERK PETER ,  CLAUDE TARANTA ,  KROEHL THOMAS ,  COX GERHARD ,  MARTIN SUKOPP ,  STEFAN SCHERER ,  ANTTI OJALA ,  GAUTAM R DESIRAJU ,  RAHUL BANERJEE ,  PRASHANT M BHATT

    IPC: C07D231/38 ,  A01N47/02 ,  A01P7/04 ,  A61K9/10 ,  A61K31/415 ,  A61P33/00 ,  A61P33/10 ,  A61P33/14

    CPC classification number: A01N43/56 ,  A01N47/02 ,  A01N2300/00

    Abstract: PROBLEM TO BE SOLVED: To provide a fipronyl crystal allowing easy filtration and drying with less dust in a production procedure and a composition which is blended with the crystal, has formulation stability and is for insecticidal and parasiticidal mixtures.SOLUTION: A solid fipronyl is present as a monoclinic system having a center-symmetry space group C2/c, shows a specific reflection in an X-ray powder diffraction diagram recorded at 25°C by using Cu-Kα radiation rays and contains at least 85 wt.% of a crystal transformation I of fipronyl. A method of producing the crystal transformation I comprises dissolving a solid fipronyl different from the crystal transformation I in a solvent selected from one or more of alcohols, acetonitrile(AN), dimethylsulfoxide(DMSO), one or more of benzene derivatives, etc. and crystallizing from the resultant solution. When the solvent is AN, crystallization is carried out at 40°C or lower. When the solvent is DMSO, crystallization is carried out at 80°C or lower.

    Abstract translation: 要解决的问题：提供一种氟虫腈基晶体，其允许在制备方法中容易地过滤和干燥较少的粉尘，并且与晶体混合的组合物具有制剂的稳定性，并且是杀虫剂和杀寄生虫剂的混合物。解决方案：存在固体氟虫基 作为具有中心对称空间群C2 / c的单斜晶系，通过使用Cu-Kα射线在25℃记录的X射线粉末衍射图中显示特定的反射，并含有至少85重量％的结晶 氟吡酮的转化I。 制造晶体转变I的方法包括将不同于晶体转变I的固体氟虫酰基溶解在选自醇，乙腈（AN），二甲基亚砜（DMSO），一种或多种苯衍生物等中的一种或多种的溶剂中，以及 从所得溶液中结晶。 当溶剂为AN时，在40℃或更低温度下进行结晶。 当溶剂为DMSO时，在80℃或更低温度下进行结晶。

    COMPOUNDS WITH TERMINAL HETEROARYLCYANOVINYLENE GROUPS AND THEIR USE IN ORGANIC SOLAR CELLS
    6.
    发明申请
    COMPOUNDS WITH TERMINAL HETEROARYLCYANOVINYLENE GROUPS AND THEIR USE IN ORGANIC SOLAR CELLS 审中-公开
    具有末端杂环亚氨基的组合物及其在有机太阳能电池中的使用

    公开(公告)号：WO2015024848A4

    公开(公告)日：2015-05-14

    申请号：PCT/EP2014067390

    申请日：2014-08-14

    Applicant: BASF SE

    Inventor： SUNDARRAJ SUDHAKAR ,  EICKHOFF CHRISTIAN ,  BAHULAYAN SHEEJA ,  SEND ROBERT ,  NISHIMAE YUICHI ,  REICHELT HELMUT ,  TANABE JUNICHI ,  ERK PETER

    IPC: C09K11/06 ,  H05B33/10

    CPC classification number: H01L51/0068 ,  C09K11/06 ,  C09K2211/1007 ,  C09K2211/1011 ,  C09K2211/1029 ,  C09K2211/1037 ,  C09K2211/104 ,  C09K2211/1088 ,  C09K2211/1092 ,  H01L51/0046 ,  H01L51/0052 ,  H01L51/0053 ,  H01L51/0065 ,  H01L51/0067 ,  H01L51/0069 ,  H01L51/0071 ,  H01L51/0072 ,  H01L51/0074 ,  H01L51/424 ,  H05B33/10

    Abstract: The present invention relates to a photoactive material comprising a donor substance and an acceptor substance, wherein the donor substance comprises or consists of one or more compounds of formula (I) described herein, or the acceptor substance comprises or consists of one or more compounds of formula (I) described herein, or the donor sub¬ stance comprises or consists of a first compound of formula (I) described herein and the acceptor substance comprises a second compound of formula (I) described herein with the proviso that the first and second compound are not the same, as well as to an organic solar cell comprising said photoactive material. The present invention also relates to a photoelectric conversion device comprising or consisting of two or more organic solar cells comprising said photoactive material and to compounds of formula (I) as described herein for use as donor substance or as acceptor substance in a photoactive material. Further, the present invention relates to the use of a compound of formula (III) as described herein in the synthesis of a compound of formula (I) as described herein.

    Abstract translation: 本发明涉及包含施主物质和受体物质的光活性物质，其中供体物质包含一种或多种本文所述的式（I）化合物或由其组成，或受体物质包含或由一种或多种 本文所述的式（I）或供体方案包含本文所述的第一式（I）化合物或由其组成，受体物质包含本文所述的第二式（I）化合物，条件是第一和第二 化合物不同，以及包含所述光活性材料的有机太阳能电池。 本发明还涉及一种光电转换装置，其包含两种或更多种包含所述光活性材料的有机太阳能电池或由本文所述的式（I）化合物或用作光活性材料中的受体物质或作为受体物质的化合物。 此外，本发明涉及本文所述的式（III）化合物在合成如本文所述的式（I）化合物中的用途。

    DYE SOLAR CELL WITH IMPROVED STABILITY
    8.
    发明申请
    DYE SOLAR CELL WITH IMPROVED STABILITY 审中-公开
    DYE太阳能电池具有改善的稳定性

    公开(公告)号：WO2012011023A3

    公开(公告)日：2012-03-15

    申请号：PCT/IB2011053121

    申请日：2011-07-13

    Applicant: BASF SE ,  BASF CHINA CO LTD ,  PSCHIRER NEIL GREGORY ,  BRUDER INGMAR ,  SENS RUEDIGER ,  ERK PETER

    Inventor： PSCHIRER NEIL GREGORY ,  BRUDER INGMAR ,  SENS RUEDIGER ,  ERK PETER

    IPC: H01G9/20 ,  H01L27/30 ,  H01L51/42 ,  H01L51/46

    CPC classification number: H01L51/422 ,  C09B57/007 ,  H01L51/002 ,  H01L2251/303 ,  Y02E10/549 ,  Y02P70/521

    Abstract: A photovoltaic element (110) is proposed for conversion of electromagnetic radiation to electrical energy. The photovoltaic element (1 10) may especially be a dye solar cell (1 12). The photovoltaic element (110) has at least one first electrode (1 16), at least one n-semiconductive metal oxide (120), at least one electromagnetic radiation-absorbing dye (122), at least one solid organic p-semiconductor (126) and at least one second electrode (132). The p-semiconductor (126) comprises at least one metal oxide (130).

    Abstract translation: 光伏元件（110）被提出用于将电磁辐射转换成电能。 光伏元件（110）尤其可以是染料太阳能电池（112）。 光伏元件（110）具有至少一个第一电极（116），至少一个n-半导体金属氧化物（120），至少一个电磁辐射吸收染料（122），至少一个固体有机p-半导体 126）和至少一个第二电极（132）。 p-半导体（126）包含至少一种金属氧化物（130）。

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